Determining the Occurrence of Oil in Micro/Nanopores of Tight Sand: A New Approach Using Environmental Scanning Electron Microscopy Combined with Energy-Dispersive Spectrometry

2018 ◽  
Vol 32 (4) ◽  
pp. 4885-4893 ◽  
Author(s):  
Yanjie Gong ◽  
Keyu Liu ◽  
Shaobo Liu
2001 ◽  
Vol 711 ◽  
Author(s):  
Athene M Donald

ABSTRACTThe environmental scanning electron microscope (ESEM) offers a new approach for the examination of biological samples at rather high resolution. It permits samples to be imaged without extensive specimen preparation, and specifically requires neither drying nor coating. This implies that organic samples can be looked at in their native state, without the danger of artefacts being introduced. A few specific examples both of static imaging, and also images obtained during dynamic mechanical testing are given in this article to illustrate the power of the technique.


Author(s):  
Howard S. Kaufman ◽  
Keith D. Lillemoe ◽  
John T. Mastovich ◽  
Henry A. Pitt

Gallstones contain precipitated cholesterol, calcium salts, and proteins. Calcium (Ca) bilirubinate, palmitate, phosphate, and carbonate occurring in gallstones have variable morphologies but characteristic windowless energy dispersive x-ray (EDX) spectra. Previous studies of gallstone microstructure and composition using scanning electron microscopy (SEM) with EDX have been limited to dehydrated samples. In this state, Ca bilirubinates appear as either glassy masses, which predominate in black pigment stones, or as clusters, which are found mostly in cholesterol gallstones. The three polymorphs of Ca carbonate, calcite, vaterite, and aragonite, have been identified in gallstones by x-ray diffraction, however; the morphologies of these crystals vary in the literature. The purpose of this experiment was to study fresh gallstones by environmental SEM (ESEM) to determine if dehydration affects gallstone Ca salt morphology.Gallstones and bile were obtained fresh at cholecystectomy from 6 patients. To prevent dehydration, stones were stored in bile at 37°C. All samples were studied within 4 days of procurement.


2001 ◽  
Vol 707 ◽  
Author(s):  
Ian C. Bache ◽  
Catherine M. Ramsdale ◽  
D. Steve Thomas ◽  
Ana-Claudia Arias ◽  
J. Devin MacKenzie ◽  
...  

ABSTRACTCharacterising the morphology of thin films for use in device applications requires the ability to study both the structure within the plane of the film, and also through its thickness. Environmental scanning electron microscopy has proved to be a fruitful technique for the study of such films both because contrast can be seen within the film without the need for staining (as is conventionally done for electron microscopy), and because cross-sectional images can be obtained without charging artefacts. The application of ESEM to a particular blend of relevance to photovoltaics is described.


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