Effects of Coagulation Bath Temperature on the Separation Performance and Antifouling Property of Poly(ether sulfone) Ultrafiltration Membranes

2010 ◽  
Vol 49 (10) ◽  
pp. 4858-4864 ◽  
Author(s):  
Jinming Peng ◽  
Yanlei Su ◽  
Wenjuan Chen ◽  
Qing Shi ◽  
Zhongyi Jiang
Keyword(s):  
Bath Temperature ◽  
Coagulation Bath ◽  
Separation Performance ◽  
Ultrafiltration Membranes ◽  
Antifouling Property ◽  
Coagulation Bath Temperature

scholarly journals Effect of Precipitation Temperature on the Properties of Cellulose Ultrafiltration Membranes Prepared via Immersion Precipitation with Ionic Liquid as Solvent

Membranes ◽  
2018 ◽  
Vol 8 (4) ◽  
pp. 87 ◽  
Author(s):  
Daria Nevstrueva ◽  
Arto Pihlajamäki ◽  
Juha Nikkola ◽  
Mika Mänttäri
Keyword(s):  
Ionic Liquid ◽  
Pure Water ◽  
Polymer Concentration ◽  
Water Flux ◽  
Bath Temperature ◽  
Liquid Solution ◽  
Coagulation Bath ◽  
Fouling Resistance ◽  
Ultrafiltration Membranes ◽  
Coagulation Bath Temperature

Supported cellulose ultrafiltration membranes are cast from a cellulose-ionic liquid solution by the immersion precipitation technique. The effects of coagulation bath temperature and polymer concentration in the casting solution on the membrane morphology, wettability, pure water flux, molecular weight cut-off, and fouling resistance are studied. Scanning electron microscopy, contact angle measurements, atomic force microscopy, and filtration experiments are carried out in order to characterise the obtained ultrafiltration cellulose membranes. The results show the effect of coagulation bath temperature and polymer concentration on the surface morphology and properties of cellulose ultrafiltration membranes. Optimisation of the two parameters leads to the creation of dense membranes with good pure water fluxes and proven fouling resistance towards humic acid water solutions.

Preparation and Characterizations of Polysulfone Flat Ultrafiltration Membranes

2011 ◽  
Vol 418-420 ◽  
pp. 169-172
Author(s):  
Shan Zhang ◽  
Zhen Liu
Keyword(s):  
Pure Water ◽  
Water Flux ◽  
Bath Temperature ◽  
Coagulation Bath ◽  
Egg Rejection ◽  
Evaporation Time ◽  
Ultrafiltration Membranes ◽  
Pure Water Flux ◽  
Coagulation Bath Temperature

The Polysulfone Flat ultrafiltration membranes were prepared with dimethylacetamide (DMAc) as solvent and polyvinypyrrolidone (PVP) as pore forming additive. Performance of PSF membrane such as pure water flux, albumin egg rejection were investigated. In addition, the same investigations were conducted with different coagulation bath temperature and evaporation time. The results show that there were a maximum of pure water flux and a minimum of the retention of Albumin when PVP content reach 14%.

Preparation of hydrophilic modified polyvinylidene fluoride (PVDF) ultrafiltration membranes by polymer/non-solvent co-induced phase separation: effect of coagulation bath temperature

2022 ◽  
Vol 0 (0) ◽  
Author(s):  
Xiaoming Zhang ◽  
Qingchen Lu ◽  
Nana Li
Keyword(s):  
Phase Separation ◽  
Membrane Fouling ◽  
Membrane Structure ◽  
Polyvinylidene Fluoride ◽  
Membrane Surface ◽  
Pure Water ◽  
Bath Temperature ◽  
Coagulation Bath ◽  
Separation Performance ◽  
Coagulation Bath Temperature

Abstract Membrane separation technology is widely used in wastewater purification, but the issue of membrane fouling could not be ignored. Hydrophilic modification is an effective method to reduce membrane fouling. Therefore, in this work, a hydrophilic modified polyvinylidene fluoride (PVDF) ultrafiltration membrane was prepared by polymer/non-solvent co-induced phase separation, and the effect of coagulation bath temperature on the membrane structure and performance was systematically investigated based on the previous study. With the increased of the coagulation bath temperature, the phase separation process changed from delayed to instantaneous, and the membrane surface changed from porous to dense, while the macropore structures and sponge-like pores appeared on the cross-section. Meanwhile, the pure water flux decreased from 229.3 L/(m2·h) to 2.08 L/(m2·h), the protein rejection rate increased from 83.87% to 100%, and the surface water contact angle increased from 63° to 90°. Thus, excessively high coagulation bath temperature adversely affected the permeate and separation performance, as well as antifouling performance of the membrane. This study enriched the research for preparing separation membranes by polymer/non-solvent co-induced phase separation and provided a practical and theoretical reference for controlling the membrane structure and properties by changing the coagulation bath temperature.

scholarly journals Temperature Coagulant Tub Variation Effect on the Characteristic of Hollow Fiber Dialyser from Cellulose Acetate Composite D-Glucose Monohydrate

2017 ◽  
Vol 31 ◽  
pp. 53-60
Author(s):  
Rizki Firsta Wahyuliswari ◽  
Siswanto ◽  
Prihartini Widiyanti
Keyword(s):  
Tensile Strength ◽  
Creatinine Clearance ◽  
Cellulose Acetate ◽  
Hollow Fiber ◽  
Bath Temperature ◽  
Hollow Fibers ◽  
Coagulation Bath ◽  
Temperature Variations ◽  
Swelling Rate ◽  
Coagulation Bath Temperature

Polysulfone is synthetic polymer widely used as basic material for dialyzer membrane and hydrophobic so it tends to cause fouling. Cellulose acetate is non-synthetic, hydrophilic polymer which has low tendency of fouling and has good thermal stability and permeability so it is considered as alternative material for hollow fiber dialyzer. A proper hollow fiber can be achieved by setting a proper temperature of coagulation bath along the spinning process. This research aims to understand the effect of coagulation bath temperature variations on the physical characteristic such as pore size, tensile strength, swelling rate and creatinine clearance of cellulose acetate – D-glucose monohydrate hollow fibers. Hollow fibers were fabricated using spinneret at temperature variations 5°C, 10°C, 15°C dan 20°C. Physical characteristics were estimated by doing morphology test using SEM, tensile test, swelling test towards Simulated Body Fluid (SBF) and filtration test towards creatinine. Result revealed that the hollow fibers from 5°C coagulation bath temperature gives the best characteristic and performance with tensile strength 27,421 N mm-2, pore size 0,0295–0,0858 nm, swelling rate 4,18%, elongation rate 4,4 %, flux rate 1,6032–1,7956 mL cm-2 min-1 and creatinine clearance rate 40,14–48,30% so it is potential to be applied as dialyzer membrane.

scholarly journals Effect of coagulation bath temperature during preparation of PES hollow fiber supported liquid membrane for acetic acid removal

2017 ◽  
Vol 19 ◽  
pp. 118 ◽  
Author(s):  
Sathiya Sanmugam ◽  
Norlisa Harruddin ◽  
Syed M Saufi
Keyword(s):  
Aqueous Solution ◽  
Acetic Acid ◽  
Hollow Fiber ◽  
Liquid Membrane ◽  
Hollow Fiber Membrane ◽  
Bath Temperature ◽  
Supported Liquid Membrane ◽  
Coagulation Bath ◽  
Fiber Membrane ◽  
Coagulation Bath Temperature

<p>Acetic acid is a byproduct of acid hydrolysis of biomass during sugar recovery step in biofuel production. Acetic acid can inhibit the enzyme used during fermentation of sugar to the ethanol. Hollow fiber supported liquid membrane (SLM) was used in this study to remove acetic acid from aqueous solution. Liquid membrane was formulated using trioctylamine and 2-ethyl hexanol as a carrier and solvent, respectively. The hollow fiber membrane support was prepared from 15 wt.% polyethersulfone, 42.5 wt.% polyethyleneglycol 200 and 42.5 wt.% dimethylacetamide. The effect of coagulation bath temperature (CBT) at 30<sup>º</sup>C, 40<sup>º</sup>C and 50<sup>º</sup>C during hollow fiber membrane spinning process was investigated. The porosity of the membrane increased as the CBT increased. The porosity of the membrane prepared using CBT of 30ºC, 40<sup>º</sup>C and 50<sup>º</sup>C were 35.7%, 46.7% and 61.6%, respectively. SLM process using hollow fiber membrane prepared at 50ºC of coagulation bath was able to remove 52% of acetic acid from the aqueous solution.</p><p>Chemical Engineering Research Bulletin 19(2017) 118-122</p>

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