High-Resolution Analysis of (Sc3C2)@C80Metallofullerene by Third Generation Synchrotron Radiation X-ray Powder Diffraction

2006 ◽  
Vol 110 (39) ◽  
pp. 19215-19219 ◽  
Author(s):  
Eiji Nishibori ◽  
Ikuya Terauchi ◽  
Makoto Sakata ◽  
Masaki Takata ◽  
Yasuhiro Ito ◽  
...  
2007 ◽  
Vol 130 ◽  
pp. 7-14 ◽  
Author(s):  
Andrew N. Fitch

The highly-collimated, intense X-rays produced by a synchrotron radiation source can be harnessed to build high-resolution powder diffraction instruments with a wide variety of applications. The general advantages of using synchrotron radiation for powder diffraction are discussed and illustrated with reference to the structural characterisation of crystalline materials, atomic PDF analysis, in-situ and high-throughput studies where the structure is evolving between successive scans, and the measurement of residual strain in engineering components.


2012 ◽  
Vol 415 (1) ◽  
pp. 102-117 ◽  
Author(s):  
Elena Bobyr ◽  
Jonathan K. Lassila ◽  
Helen I. Wiersma-Koch ◽  
Timothy D. Fenn ◽  
Jason J. Lee ◽  
...  

Archaeometry ◽  
2010 ◽  
Vol 52 (2) ◽  
pp. 286-307 ◽  
Author(s):  
A. DURAN ◽  
M. C. JIMENEZ DE HARO ◽  
J. L. PEREZ-RODRIGUEZ ◽  
M. L. FRANQUELO ◽  
L. K. HERRERA ◽  
...  

2016 ◽  
Vol 49 (5) ◽  
pp. 1443-1453 ◽  
Author(s):  
Marcelo Goncalves Honnicke ◽  
Leonardo M. Bianco ◽  
Sergio A. Ceppi ◽  
Cesar Cusatis ◽  
XianRong Huang ◽  
...  

The construction and characterization of a focusing X-ray spherical analyzer based on α-quartz 4{\bar 4}04 are presented. The performance of the analyzer was demonstrated by applying it to a high-resolution X-ray spectroscopy study of theKα1,2emission spectrum of Ni. An analytical representation based on physical grounds was assumed to model the shape of the X-ray emission lines. Satellite structures assigned to 3dspectator hole transitions were resolved and determined as well as their relative contribution to the emission spectrum. The present results on 1s−13d−1shake probabilities support a recently proposed calculation framework based on a multi-configuration atomic model.


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