In situ microcalorimetry study of ZnFe2O4 nanoparticle formation under solvothermal conditions

2015 ◽  
Vol 44 (39) ◽  
pp. 17293-17301 ◽  
Author(s):  
Jun Liu ◽  
Zhaodong Nan ◽  
Shengli Gao
Keyword(s):  
Formation Mechanism ◽  
Solvothermal Method ◽  
Nanoparticle Formation ◽  
Model Sample ◽  
One Step ◽  
Solvothermal Conditions ◽  
In Situ Microcalorimetry

In situ microcalorimetry is used to investigate the formation mechanism for the solvothermal method, where ZnFe2O4 nanoparticles synthesized via a one-step solvothermal method are selected as the model sample.

In situ time-resolved DXAFS study of Rh nanoparticle formation mechanism in ethylene glycol at elevated temperature

2012 ◽  
Vol 14 (9) ◽  
pp. 2983 ◽  
Author(s):  
Hiroyuki Asakura ◽  
Kentaro Teramura ◽  
Tetsuya Shishido ◽  
Tsunehiro Tanaka ◽  
Ning Yan ◽  
...  
Keyword(s):  
Elevated Temperature ◽  
Ethylene Glycol ◽  
Formation Mechanism ◽  
Time Resolved ◽  
Nanoparticle Formation

Elucidation of the Formation Mechanism of Metal–Organic Frameworks via in-Situ Raman and FTIR Spectroscopy under Solvothermal Conditions

2018 ◽  
Vol 122 (23) ◽  
pp. 12267-12278 ◽  
Author(s):  
Heidemarie Embrechts ◽  
Martin Kriesten ◽  
Kilian Hoffmann ◽  
Wolfgang Peukert ◽  
Martin Hartmann ◽  
...  
Keyword(s):  
Ftir Spectroscopy ◽  
Formation Mechanism ◽  
Metal Organic Frameworks ◽  
In Situ Raman ◽  
Metal Organic ◽  
Solvothermal Conditions

One-step in situ synthesis of BiOCl/(BiO)2CO3 composite photocatalysts with exposed high-energy {001} facets

CrystEngComm ◽  
2018 ◽  
Vol 20 (48) ◽  
pp. 7838-7850 ◽  
Author(s):  
Yingying Chen ◽  
Yan Zhou ◽  
Qimei Dong ◽  
Hanming Ding
Keyword(s):  
Photocatalytic Activity ◽  
Synergistic Effect ◽  
Solvothermal Method ◽  
High Energy ◽  
In Situ Synthesis ◽  
Band Alignment ◽  
Type Ii ◽  
Composite Photocatalysts ◽  
One Step

BiOCl/(BiO)2CO3 composites with reactive exposed {001} facets have been synthesized by a one-step in situ solvothermal method. The synergistic effect of type-II band alignment and exposed high-energy facets enhances photocatalytic activity.

In situ formed Bi/BiOBrxI1−x heterojunction of hierarchical microspheres for efficient visible-light photocatalytic activity

2015 ◽  
Vol 17 (20) ◽  
pp. 13347-13354 ◽  
Author(s):  
Chunrui Zheng ◽  
Chuanbao Cao ◽  
Zulfiqar Ali
Keyword(s):  
Photocatalytic Activity ◽  
Visible Light ◽  
Solvothermal Method ◽  
Visible Light Photocatalytic Activity ◽  
Hierarchical Microspheres ◽  
One Step ◽  
Visible Light Photocatalytic

Bi/BiOBrxI1−x heterojunction of hierarchical microspheres formed in situ with efficient visible-light photocatalytic activity were synthesized by a facile one-step solvothermal method.

scholarly journals In-situ construction of ZnIn2S4/CdIn2S4 2D/3D nano hetero-structure for enhanced visible-light-driven hydrogen production

2021 ◽  
Author(s):  
Xinyu Dang ◽  
Mingsen Xie ◽  
Fangfang Dai ◽  
Jin-Na Guo ◽  
Jia Liu ◽  
...  
Keyword(s):  
Hydrogen Production ◽  
Visible Light ◽  
Solvothermal Method ◽  
Nano Composites ◽  
Hetero Structure ◽  
In Situ Modification ◽  
Visible Light Driven ◽  
One Step ◽  
Interface Contact

Through in-situ modification of CdIn2S4 nano-octahedron on the surface of ZnIn2S4 nanosheets, ZnIn2S4/CdIn2S4 nano-composites with tight interface contact are obtained by one-step solvothermal method. Due to ZnIn2S4/CdIn2S4 nano-heterostructure, the optimized...

Synthesis of Titania Microshperes with Controllable Diameter Under Solvothermal Conditions

2012 ◽  
Vol 476-478 ◽  
pp. 1678-1681
Author(s):  
Dong Bo Guo ◽  
Yan Ping Wang ◽  
Xiao Chao Zhang ◽  
Jia Wang ◽  
Yi Min Wang
Keyword(s):  
Titanium Dioxide ◽  
Diblock Copolymers ◽  
Solvothermal Method ◽  
Structure Directing Agent ◽  
X Ray ◽  
One Step ◽  
Poly Ethylene Oxide ◽  
Poly Ethylene ◽  
Xrd Patterns ◽  
Solvothermal Conditions

Bead-structured titanium dioxide microspheres were successfully prepared by a facile one-step solvothermal method using diblock copolymers poly(ethylene oxide)-block-polystyene (PEO-b-PS) as the structure-directing agent. The products were characterized by scanning electron microscopy, thermogravimetic analysis and X-ray powder diffraction (XRD) technique. The XRD patterns show that the products synthesized with low content of HCl are anatase titanium dioxide and the products synthesized with low content of HCl are rulite titanium dioxide.

Preparation of high-refractive-index PMMA/TiO2 nanocomposites by one-step in situ solvothermal method

2013 ◽  
Vol 22 (10) ◽  
pp. 767-774 ◽  
Author(s):  
Jieyu Jin ◽  
Rongrong Qi ◽  
Yuezeng Su ◽  
Mingkang Tong ◽  
Jian Zhu
Keyword(s):  
Refractive Index ◽  
Solvothermal Method ◽  
High Refractive Index ◽  
One Step

Phase Structure of Nanocrystalline BaTiO3 Powders via One-Step Solvothermal Route

2013 ◽  
Vol 833 ◽  
pp. 8-12 ◽  
Author(s):  
Hui Zhang ◽  
Xiao Hui Wang ◽  
Zheng Bo Shen ◽  
Ya Nan Hao
Keyword(s):  
Phase Transition ◽  
Grain Size ◽  
Solvothermal Method ◽  
One Step ◽  
In Situ Heating ◽  
The One ◽  
Different Grain Size ◽  
Similar Phase ◽  
Dispersive Phase

5 nm BaTiO3 powder has been successfully prepared by the one-step solvothermal method. The different grain size BaTiO3 powders have been achieved after calcining the 5 nm Nanocrystalline BaTiO3 powders at 700°C, 850°C and 950°C for 3 h. In-situ heating Raman spectroscopy revealed the dispersive phase transition character in the nanocrystalline BaTiO3 powders. As the BaTiO3 grain size decreases, wider phase transition temperature and the Raman intensity becomes weak. The BaTiO3 powders of the 5 nm nanocrystalline exhibited the similar phase transformations from rhombohedral to orthorhombic to tetragonal to cubic transitions as those in the coarse BaTiO3 ceramics.

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