A bifunctional NiCo2S4/reduced graphene oxide@polyaniline nanocomposite as a highly-efficient electrode for glucose and rutin detection

2018 ◽  
Vol 42 (12) ◽  
pp. 9398-9409 ◽  
Author(s):  
Yanying Wang ◽  
Ji Zhong ◽  
Fang Ding ◽  
Qingbiao Zhao ◽  
Zhaoyi Zhang ◽  
...  

A novel NiCo2S4/reduced graphene oxide@polyaniline (NiCo2S4/rGO@PANI) composite was synthesized by a facile two-step hydrothermal treatment and calcination, which was coupled with an in situ polymerization process.

RSC Advances ◽  
2017 ◽  
Vol 7 (85) ◽  
pp. 54031-54038 ◽  
Author(s):  
Yuefang Zhang ◽  
Jia Liu ◽  
Yahong Zhang ◽  
Jin Liu ◽  
Yuping Duan

Hierarchical nanocomposites of aligned polyaniline nanorods on reduced graphene oxide nanosheets are synthesized in an in situ polymerization process.


RSC Advances ◽  
2015 ◽  
Vol 5 (66) ◽  
pp. 53935-53939 ◽  
Author(s):  
Sheng Wang ◽  
Donghua Hu ◽  
Wenwen Hua ◽  
Jiangjiang Gu ◽  
Qiuhong Zhang ◽  
...  

A simple scheme of Pd2+ fixed on FRGO as a highly efficient coupling catalyst.


2018 ◽  
Vol 2018 ◽  
pp. 1-9 ◽  
Author(s):  
Xiaochao Duan ◽  
Bin Yu ◽  
Tonghui Yang ◽  
Yanpeng Wu ◽  
Hao Yu ◽  
...  

A one-step method of in situ polymerization of nylon 66/reduced graphene oxide (PA66/rGO) nanocomposites is first proposed, simply by introducing graphene oxide (GO) into PA66 salt with the existence of ammonium hydroxide. The GO is prereduced by the ammonium hydroxide at an early stage of the polymerization process and then grafted on the PA66 chains, accompanied with the thermal reduction of GO. The PA66 chains were grafted onto the GO nanosheets through the condensation between the oxygen-containing functional groups of the GO and the terminal amino ends of the PA66 chains. The effect of GO on the mechanical properties, especially tensile strength, of nanocomposites was investigated. The results revealed that the incorporation of a very small amount (about 1 wt%) of GO caused a significant improvement in ultimate tensile strength (about 17%). The SEM of the fracture surface of composites indicated a good dispersion of rGO in the matrix. Raman spectroscopy, thermogravimetric analysis (TGA), scanning electron microscope (SEM), Fourier transformed infrared spectroscopy (FTIR), and XRD patterns of rGO, which was isolated from nanocomposites, revealed that the GO nanolayers were simultaneously reduced and PA66 chains were grafted on the rGO nanosheet during the polymerization process. The rGO grafted with the PA66 chain increases its compatibility in the PA66 matrix and effectively enhanced the interfacial energy of the composites.


ACS Omega ◽  
2020 ◽  
Vol 5 (49) ◽  
pp. 31535-31542
Author(s):  
Weijun Miao ◽  
Feng Wu ◽  
Shiman Zhou ◽  
Guibin Yao ◽  
Yiguo Li ◽  
...  

2020 ◽  
Vol 59 (1) ◽  
pp. 477-487 ◽  
Author(s):  
Zhuang Liu ◽  
Haiyang Fu ◽  
Bo Gao ◽  
Yixuan Wang ◽  
Kui Li ◽  
...  

AbstractThis paper studies in-situ synthesis of Fe2O3/reduced graphene oxide (rGO) anode materials by different hydrothermal process.Scanning Electron Microscopy (SEM) analysis has found that different processes can control the morphology of graphene and Fe2O3. The morphologies of Fe2O3 prepared by the hydrothermal in-situ and oleic acid-assisted hydrothermal in-situ methods are mainly composed of fine spheres, while PVP assists The thermal in-situ law presents porous ellipsoids. Graphene exhibits typical folds and small lumps. X-ray diffraction analysis (XRD) analysis results show that Fe2O3/reduced graphene oxide (rGO) is generated in different ways. Also, the material has good crystallinity, and the crystal form of the iron oxide has not been changed after adding GO. It has been reduced, and a characteristic peak appears around 25°, indicating that a large amount of reduced graphene exists. The results of the electrochemical performance tests have found that the active materials prepared in different processes have different effects on the cycle performance of lithium ion batteries. By comprehensive comparison for these three processes, the electro-chemical performance of the Fe2O3/rGO prepared by the oleic acid-assisted hydrothermal method is best.


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