Crystal structures and electronic properties of Sn3N4 polymorphs synthesized via high-pressure nitridation of tin

CrystEngComm ◽  
2020 ◽  
Vol 22 (20) ◽  
pp. 3531-3538
Author(s):  
Ken Niwa ◽  
Tomoya Inagaki ◽  
Tetsu Ohsuna ◽  
Zheng Liu ◽  
Takuya Sasaki ◽  
...  
Keyword(s):  
High Pressure ◽  
Electronic Properties ◽  
Crystal Structures ◽  
Crystal Chemistry ◽  
Diamond Anvil Cell ◽  
Functional Materials ◽  
Group Iva ◽  
Diamond Anvil ◽  
Laser Heated ◽  
Insight Into

Sn3N4 polymorphs were synthesized via high-pressure nitridation of tin by means of laser-heated diamond anvil cell technique. This implies new insight into the crystal chemistry and functional materials of group IVA nitrides.

High Pressure in situ Micro-Raman Spectroscopy of Ge-Sn System Synthesized in a Laser Heated Diamond Anvil Cell

2011 ◽  
Author(s):  
Y. A. Sorb ◽  
N. Subramanian ◽  
T. R. Ravindran ◽  
P. Ch. Sahu ◽  
Alka B. Garg ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
High Pressure ◽  
Diamond Anvil Cell ◽  
Micro Raman Spectroscopy ◽  
Diamond Anvil ◽  
Laser Heated

scholarly journals The Bridgmanite–Akimotoite–Majorite Triple Point Determined in Large Volume Press and Laser-Heated Diamond Anvil Cell

Minerals ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 67
Author(s):  
Britany L. Kulka ◽  
Jonathan D. Dolinschi ◽  
Kurt D. Leinenweber ◽  
Vitali B. Prakapenka ◽  
Sang-Heon Shim
Keyword(s):  
High Pressure ◽  
Triple Point ◽  
Large Volume ◽  
Diamond Anvil Cell ◽  
Experimental Methods ◽  
Diamond Anvil ◽  
Laser Heated ◽  
Good Agreement

The bridgmanite–akimotoite–majorite (Bm–Ak–Mj or BAM) triple point in MgSiO3 has been measured in large-volume press (LVP; COMPRES 8/3 assembly) and laser-heated diamond anvil cell (LHDAC). For the LVP data, we calculated pressures from the calibration provided for the assembly. For the LHDAC data, we conducted in situ determination of pressure at high temperature using the Pt scale at synchrotron. The measured temperatures of the triple point are in good agreement between LVP and LHDAC at 1990–2000 K. However, the pressure for the triple point determined from the LVP is 3.9 ± 0.6 GPa lower than that from the LHDAC dataset. The BAM triple point determined through these experiments will provide an important reference point in the pressure–temperature space for future high-pressure experiments and will allow mineral physicists to compare the pressure–temperature conditions measured in these two different experimental methods.

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