A total consumption (up to 75 μL min−1) infrared-heated sample introduction system for inductively coupled plasma optical emission spectrometry

2020 ◽  
Vol 35 (6) ◽  
pp. 1125-1130 ◽  
Author(s):  
Ahmed Al Hejami ◽  
Mirah J. Burgener ◽  
John Burgener ◽  
Diane Beauchemin
Keyword(s):  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Analytical Performance ◽  
Sample Introduction ◽  
Emission Spectrometry ◽  
Total Consumption ◽  
Heated Sample ◽  
Inductively Coupled ◽  
Sample Introduction System ◽  
Plasma Optical Emission Spectrometry

A compact infrared-heated sample introduction system provides similar analytical performance with higher robustness and faster washout than commercially available nebulization systems.

New infrared-heated sample introduction system for enhanced analytical performance of inductively coupled plasma optical emission spectrometry

2018 ◽  
Vol 33 (5) ◽  
pp. 738-744 ◽  
Author(s):  
Ahmed Al Hejami ◽  
Diane Beauchemin
Keyword(s):  
Inductively Coupled Plasma ◽  
Detection Limits ◽  
Optical Emission ◽  
Analytical Performance ◽  
Sample Introduction ◽  
Emission Spectrometry ◽  
Spray Chamber ◽  
Heated Sample ◽  
Inductively Coupled ◽  
Plasma Optical Emission Spectrometry

A cyclonic spray chamber was modified to allow the insertion of an infrared lamp to improve detection limits and robustness.

Improvement of analytical performance in inductively coupled plasma optical emission spectrometry without compromising robustness using an infrared-heated sample introduction system with a pneumatic nebulizer

2015 ◽  
Vol 30 (1) ◽  
pp. 214-224 ◽  
Author(s):  
Yoseif Makonnen ◽  
John Burgener ◽  
Diane Beauchemin
Keyword(s):  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Sample Introduction ◽  
Infrared Heating ◽  
Emission Spectrometry ◽  
Heated Sample ◽  
Inductively Coupled ◽  
Line Intensity Ratio ◽  
Plasma Optical Emission Spectrometry ◽  
Pneumatic Nebulizer

Infrared-heating the spray chamber and bottom of the torch significantly improves sensitivity and detection limit for 38 elements, as well as robustness, resulting in a Mg II 280.270 nm/Mg I 285.213 nm line intensity ratio of 13.

Analytical Performance in Flow Injection—Simultaneous Multielement—Inductively Coupled Plasma—Optical Emission Spectrometry Employing a Cyclonic Spray Chamber

1996 ◽  
Vol 50 (8) ◽  
pp. 1015-1022 ◽  
Author(s):  
Terrance D. Hettipathirana ◽  
David E. Davey
Keyword(s):  
Flow Rate ◽  
Flow Injection ◽  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Analytical Performance ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Spray Chamber ◽  
Inductively Coupled ◽  
Plasma Optical Emission Spectrometry

Simultaneous multielement–inductively coupled plasma–optical emission spectrometry (ICP-OES) with flow injection (FI) and a small-volume cyclonic spray chamber is described. Analytical performance of FI-ICP-OES was studied with the use of a concentric nebulizer and the cyclonic spray chamber for carrier nebulization. A noise study using Fourier transformation analysis was also carried out to identify the factors that affect the analytical figures of merit of FI-ICP-OES. At a carrier flow rate of 1.0 mL/min, the major source of noise, between 0 and 15 Hz, was the peristaltic pump's roller rotation; this pump noise disappeared at a flow rate of 3.5 mL/min. A number of other discrete low-frequency noise sources were also observed at flow rates below 2.5 mL/min, with resultant degradation of precision and detection limit.

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