Facile preparation of polyoxometalate nanoparticles via a solid-state chemical reaction for aerobic oxidative desulfurization catalysis

2021 ◽  
Author(s):  
Hang Yu ◽  
Wenwen Bu ◽  
Zijia Wang ◽  
Zhuoyue Zhao ◽  
Mehwish Jadoon ◽  
...  
Keyword(s):  
Solid State ◽  
Silver Nitrate ◽  
Chemical Reaction ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Oxidative Desulfurization ◽  
Solid State Reaction Method ◽  
Reaction Method ◽  
State Chemical ◽  
Facile Preparation

Polyoxometalate nanoparticles were synthesized via a concise solid-state reaction method by directly grinding silver nitrate and the polyoxometalate (NH4)5H6PMo4V8O40 at room temperature without the assistance of a surfactant.

Study of thermoelectric properties of Ca-doped LaCoO3

2015 ◽  
Vol 29 (06n07) ◽  
pp. 1540026 ◽  
Author(s):  
Kei-Ichiro Murai ◽  
Ken Nagai ◽  
Masaru Takahashi ◽  
Shosuke Takakusa ◽  
Toshihiro Moriga
Keyword(s):  
Electrical Conductivity ◽  
Solid State ◽  
Seebeck Coefficient ◽  
Thermoelectric Properties ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Solid State Reaction Method ◽  
Reaction Method ◽  
Ca Substitution

The samples of La 1-x Ca x CoO 3 (x = 0, 0.05, 0.10, 0.15) were synthesized by solid state reaction method for studying thermoelectric properties. The properties of electrical conductivity and Seebeck coefficient were measured in the temperature ranging from room temperature to 573 K. The results of electrical conductivity was increasing Ca substitution. The highest value of electrical conductivity is 1574 S/cm. It is concluded that Ca 2+ doping in LaCoO 3 has the effect to inhibit Seebeck coefficient from decreasing.

Photoluminescence at room temperature in polycrystalline BaxSr1−xTiO3 ceramics obtained by solid-state reaction method

2008 ◽  
Vol 128 (8) ◽  
pp. 1359-1362 ◽  
Author(s):  
Wanhui Zhang ◽  
Haiyan Wang ◽  
Jian Chen ◽  
Weihong Zhang ◽  
Xiaomin Xiong ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Solid State Reaction Method ◽  
Reaction Method

Phase relations in the Ba–Sr–Co–Fe–O system at 1273 K in air

2009 ◽  
Vol 42 (2) ◽  
pp. 153-160 ◽  
Author(s):  
Zhèn Yáng ◽  
Ashley S. Harvey ◽  
Anna Infortuna ◽  
Ludwig J. Gauckler
Keyword(s):  
High Temperature ◽  
Solid State ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Solid State Reaction Method ◽  
Cubic Phase ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray

Selected compositions of the Ba–Sr–Co–Fe–O system were synthesized from powders by the solid-state reaction method. Samples were equilibrated at 1273 K for 36 000 s in air. The resulting powders were characterized by X-ray diffraction (XRD) at room temperature and by high-temperaturein situXRD. The phases present in the BaxSr1−xCoyFe1−yO3−δsystem are outlined for 1273 K in air. For most of the quaternary compositions, the cubic perovskite is formed, except for the compositions withx= 1 (excludingy= 0.4),y= 1 andx,y= 0.8, where the phases mainly show hexagonal distortions, andx, y= 0, for which a predominant cubic phase is mixed with other phases.

Application of Impedance Spectroscopy for Bi1−xNdxFeO3 Ceramics Characterization

2012 ◽  
Vol 730-732 ◽  
pp. 71-75
Author(s):  
Beata Wodecka-Dus ◽  
Jolanta Dzik ◽  
Henryk Bernard ◽  
Katarzyna Osinska ◽  
Agata Lisińska-Czekaj ◽  
...  
Keyword(s):  
Solid State ◽  
Impedance Spectroscopy ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Single Phase ◽  
Solid State Reaction Method ◽  
Frequency Range ◽  
Reaction Method ◽  
Synthesis Conditions

In the present paper the synthesis conditions for fabrication of Bi1−xNdxFeO3ceramics are reported. The single phase polycrystalline samples of Bi1−xNdxFeO3 were prepared by standard solid state reaction method from the mixture of oxides viz.: Bi2O3, Fe2O3and Nd2O3. The samples were characterized by impedance spectroscopy in the frequency range 10Hz – 1MHz at room temperature.

A simple, room temperature, solid-state synthesis route for metal oxide nanostructures

2014 ◽  
Vol 2 (33) ◽  
pp. 13519-13526 ◽  
Author(s):  
Supriya A. Patil ◽  
Dipak V. Shinde ◽  
Do Young Ahn ◽  
Dilip V. Patil ◽  
Kailas K. Tehare ◽  
...  
Keyword(s):  
Solid State ◽  
Metal Oxides ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Solid State Reaction Method ◽  
Effective Strategy ◽  
Reaction Method ◽  
Oxide Nanostructures ◽  
Metal Oxide Nanostructures ◽  
Functional Metal Oxides

In this work, we demonstrate an extremely simple but highly effective strategy for the synthesis of various functional metal oxides (MOs) such as ZnO, In2O3, Bi2O3, and SnO2nanoparticles with various distinct shapes at room temperatureviaa solid-state reaction method.

Synthesis and Electromagnetic Properties of Ca2MTeO6 (M = Mn, Co, Mg)

2006 ◽  
Vol 45 ◽  
pp. 2572-2575 ◽  
Author(s):  
Yue Jin Shan ◽  
Yoko Kanai ◽  
Keitaro Tezuka ◽  
Hideo Imoto
Keyword(s):  
Solid State ◽  
Solid State Reaction ◽  
Effective Magnetic Moment ◽  
Room Temperature ◽  
Solid State Reaction Method ◽  
Electromagnetic Properties ◽  
Reaction Method ◽  
Manganese Ion ◽  
Electronic Conductivities ◽  
Perovskite Type

Ordered perovskite-type oxides, Ca2MTeO6 (M = Mn, Co, Mg), were synthesized by a solid-state reaction method. All of samples belonged to space group P21/n and were insulators at room temperature. However, their electronic conductivities tended large gradually with a rise of temperature. Ca2MnTeO6 and Ca2CoTeO6 showed anti-ferromagnetism, and their Neel temperatures were 10 K and 7 K, respectively. The effective magnetic moment of manganese ion was 5.8 μB while its valence was bivalence in Ca2MnTeO6.

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