scholarly journals Development verification of coatings made from porous ceramic-matrix composite materials

2018 ◽  
Vol 224 ◽  
pp. 03019 ◽  
Author(s):  
Sergey Reznik ◽  
Pavel Prosuntsov ◽  
Konstantin Mikhaylovskiy

The paper presents methodology and results of tests conducted for porous carbon ceramic specimens on a high-temperature gas dynamic facility to simulate real operating conditions for heat shields. The structure of the materials before and after tests is compared.

2000 ◽  
Vol 122 (2) ◽  
pp. 212-218 ◽  
Author(s):  
Karren L. More ◽  
Peter F. Tortorelli ◽  
Mattison K. Ferber ◽  
Larry R. Walker ◽  
James R. Keiser ◽  
...  

A high-temperature, high-pressure, tube furnace has been used to evaluate the long term stability of different monolithic ceramic and ceramic matrix composite materials in a simulated combustor environment. All of the tests have been run at 150 psia, 1204°C, and 15 percent steam in incremental 500 h runs. The major advantage of this system is the high sample throughput; >20 samples can be exposed in each tube at the same time under similar exposure conditions. Microstructural evaluations of the samples were conducted after each 500 h exposure to characterize the extent of surface damage, to calculate surface recession rates, and to determine degradation mechanisms for the different materials. The validity of this exposure rig for simulating real combustor environments was established by comparing materials exposed in the test rig and combustor liner materials exposed for similar times in an actual gas turbine combustor under commercial operating conditions. [S0742-4795(00)02402-9]


Author(s):  
Michael J. Walock ◽  
Vann Heng ◽  
Andy Nieto ◽  
Anindya Ghoshal ◽  
Muthuvel Murugan ◽  
...  

Future gas turbine engines will operate at significantly higher temperatures (∼1800 °C) than current engines (∼1400 °C) for improved efficiency and power density. As a result, the current set of metallic components (titanium-based and nickel-based superalloys) will be replaced with ceramics and ceramic matrix composites (CMCs). These materials can survive the higher operating temperatures of future engines at significant weight savings over the current metallic components, i.e., advanced ceramic components will facilitate more powerful engines. While oxide-based CMCs may not be suitable candidates for hot-section components, they may be suitable for structural and/or exhaust components. However, a more thorough understanding of the performance under relevant environment of these materials is needed. To this end, this work investigates the high-temperature durability of a family of oxide–oxide CMCs (Ox–Ox CMCs) under an engine-relevant environment. Flat Ox–Ox CMC panels were cyclically exposed to temperatures up to 1150 °C, within 240 m/s (∼0.3 M) gas flows and hot sand impingement. Front and backside surface temperatures were monitored by a single-wavelength (SW) pyrometer and thermocouple, respectively. In addition, an infrared (IR) camera was used to evaluate the damage evolution of the samples during testing. Flash thermography nondestructive evaluation (NDE) was used to elucidate defects present before and after thermal exposure.


Author(s):  
K. Elliott Cramer ◽  
William P. Winfree ◽  
Edward R. Generazio ◽  
Ramakrishna Bhatt ◽  
Dennis S. Fox ◽  
...  

Strong, tough, high temperature ceramic matrix composites are currently being developed for application in advanced heat engines. One of the most promising of these new materials is a SiC fiber-reinforced silicon nitride ceramic matrix composite (SiCf/Si3N4). The interfacial shear strength in such composites is dependant on the integrity of the fiber’s carbon coating at the fiber-matrix interface. The integrity of the carbon rich interface can be significantly reduced if the carbon is oxidized. Since the thermal diffusivity of the fiber is greater than that of the matrix material, the removal of carbon increases the contact resistance at the interface reducing the thermal diffusivity of the composite. Therefore thermal diffusivity images can be used to characterize the progression of carbon depletion and degradation of the composite. A new thermal imaging technique has been developed to provide rapid large area measurements of the thermal diffusivity perpendicular to the fiber direction in these composites. Results of diffusivity measurements will be presented for a series of SiCf/Si3N4 (reaction bonded silicon nitride) composite samples heat-treated under various conditions. Additionally, the ability of this technique to characterize damage in both ceramic and other high temperature composites will be shown.


Author(s):  
Todd Engel

Ceramic Matrix Composite (CMC) materials are an attractive design option for various high-temperature structural applications. In particular, the use of CMC materials as a replacement for state-of-the-art nickel-based superalloys in hot gas path turbomachinery components offers the potential for significant increases in turbine system efficiencies, due largely to reductions in cooling requirements afforded by the increased temperature capabilities inherent to the ceramic material. However, two-dimensional fabric-laminated CMCs typically exhibit low tensile strengths in the thru-thickness (interlaminar) direction, and interply delamination is a concern for some targeted applications. Currently, standardized test methods only address the characterization of interlaminar tensile strengths at ambient temperatures; this is problematic given that nearly all CMCs are slated for service in high-temperature operating environments. This work addresses the development of a new test technique for the high-temperature measurement of interlaminar tensile properties in CMCs, allowing for the characterization of material properties under conditions more analogous to anticipated service environments in order to yield more robust component designs.


Author(s):  
V.A. Tovstonog

In modern technology, gas dynamic facilities with a flow path of a high-temperature working fluid are widely used. Their effectiveness largely depends on the maximum achievable temperature, which is to a great extent determined by the heat resistance of structural materials and thermal protection systems of the most heat-stressed structural units. Most often, mass transfer thermal protection methods using the coolant of fuel components are used in such plants. However, in some gas dynamic facilities, such as high-speed ramjet engines, the use of such methods is only sufficient to maintain an acceptable temperature level for the elements of the flow path itself. As for the thermal protection of the enclosing structural elements which are adjacent to the path, it can be provided with either uncooled screens or heat-insulating linings. The study gives a comparative assessment of the temperature regime and characteristics of alternative types of heat shields


Author(s):  
David Brewer ◽  
Greg Ojard ◽  
Martin Gibler

The NASA High Speed Research (HSR)/Enabling Propulsion Materials (EPM) program was charged with the responsibility for developing the materials and technologies necessary to meet the High Speed Civil Transport (HSCT) engine requirements. The combustor liner was identified as a critical component for meeting the efficiency and environmental acceptability goals of the HSCT engine. The EPM Ceramic Matrix Composite (CMC) Combustor liner program was tasked with developing and demonstrating a material system and design concept that meets the HSCT environmental, thermal, structural, economic, and durability requirements. Melt Infiltration (MI) SiC/SiC composites were ultimately selected for the combustor liner application. The culmination of this development effort was the delivery and testing of a CMC combustor liner. Testing was performed at NASA Glenn Research Center in the Sector Rig under HSCT operating conditions. The initial results of the rig testing are presented.


Author(s):  
Karren L. More ◽  
Peter F. Tortorelli ◽  
Mattison K. Ferber ◽  
Larry R. Walker ◽  
James R. Keiser ◽  
...  

A high-temperature, high-pressure, tube furnace has been used to evaluate the long term stability of different monolithic ceramic and ceramic matrix composite materials in a simulated combustor environment. All of the tests have been run at 150 psia, 1204°C, and 15% steam in incremental 500 h runs. The major advantage of this system is the high sample throughput; >20 samples can be exposed in each tube at the same time under similar exposure conditions. Microstructural evaluations of the samples were conducted after each 500 h exposure to characterize the extent of surface damage, to calculate surface recession rates, and to determine degradation mechanisms for the different materials. The validity of this exposure rig for simulating real combustor environments was established by comparing materials exposed in the test rig and combustor liner materials exposed for similar times in an actual gas turbine combustor under commercial operating conditions.


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