The effect of pretreatment by titanium ion beam on the internal stresses and microstructure of the TiAlN coating obtained by magnetron sputtering

Author(s):  
Olga Perevalova ◽  
Aleksej Panin ◽  
Mark Kalashnikov ◽  
Viktor Sergeev
2014 ◽  
Vol 601 (1) ◽  
pp. 57-63 ◽  
Author(s):  
Kyong Chan Heo ◽  
Phil Kook Son ◽  
Youngku Sohn ◽  
Jonghoon Yi ◽  
Jin Hyuk Kwon ◽  
...  

2018 ◽  
Vol 25 (07) ◽  
pp. 1950011
Author(s):  
YU. M. BOROVIN ◽  
E. V. LUKYANENKO ◽  
V. V. OVCHINNIKOV ◽  
T. YU. SKAKOVA ◽  
N. V. UCHEVATKINA ◽  
...  

Electron microscopy studies were conducted for the fine structure of ion-doped layer on 30ChGSN2A steel obtained by ion implantation of monotectic tin-doped copper–lead alloy Cu64Pb36[Formula: see text]Sn. Formation of a multi-level hierarchical structure was detected. The features of formation of each layer were analyzed, and it was found that the main mechanism of formation of these structures is diffusion and relaxation resulting in the occurrence of internal stresses both in the surface layer and in the sheet of 30ChGSN2A steel. Relaxation of elastic stress fields results in translational–rotational deformation forming various vortex structures.


2011 ◽  
Vol 17 (6) ◽  
pp. 983-990 ◽  
Author(s):  
Hosni Idrissi ◽  
Stuart Turner ◽  
Masatoshi Mitsuhara ◽  
Binjie Wang ◽  
Satoshi Hata ◽  
...  

AbstractFocused ion beam (FIB) induced damage in nanocrystalline Al thin films has been characterized using advanced transmission electron microscopy techniques. Electron tomography was used to analyze the three-dimensional distribution of point defect clusters induced by FIB milling, as well as their interaction with preexisting dislocations generated by internal stresses in the Al films. The atomic structure of interstitial Frank loops induced by irradiation, as well as the core structure of Frank dislocations, has been resolved with aberration-corrected high-resolution annular dark-field scanning TEM. The combination of both techniques constitutes a powerful tool for the study of the intrinsic structural properties of point defect clusters as well as the interaction of these defects with preexisting or deformation dislocations in irradiated bulk or nanostructured materials.


2015 ◽  
Vol 1084 ◽  
pp. 11-15
Author(s):  
Sergey P. Umnov ◽  
Oleg Kh. Asainov ◽  
Svetlana N. Popova ◽  
Aleksey N. Lemachko

High-reflectance aluminum films are widely used in applied optics. As part of this work, we deposited aluminum films on glass substrates by magnetron sputtering using argon ion beam assistance. The reflectivity of the films obtained was measured on the SF-256 spectrophotometer. The microstructure and topology of the films were examined with a transmission electron microscope (TEM), X-ray diffraction (XRD) and atomic force microscope (AFM). The studies have shown that the aluminum films deposited with ion assistance have higher reflectance in the UV range than the films formed by magnetron sputtering alone. The results of TEM and AFM measurements show that the geometric factor (crystallite size, surface roughness) is not the reason for the increase of reflectivity. X-ray diffraction analyses have shown a significant increase in microstress in the aluminum films deposited with ion assistance, which is caused by an increase in the defect density of the vacancy-type crystal structure. The results have shown that the increase in the density of crystal defects leads to an increase in reflectance in the UV range.


2014 ◽  
Vol 488-489 ◽  
pp. 48-52
Author(s):  
Zhi Qiang Fu ◽  
Yi Ren ◽  
Cheng Biao Wang ◽  
Wen Yue ◽  
Song Sheng Lin

The influence of sputtering power, N2 flow rate, ion current and substrate temperature on the monolayer TiN films deposited by ion beam assisted magnetron sputtering and the effect of the on-off ratio and deposition period on the multilayered Ti/TiN films was studied. It was found that the key factors affecting surface defects of monolayer TiN films are sputtering power and N2 flow rate while ion current is the most significant factor affecting the hardness of monolayer TiN films. The surface defects can be greatly inhibited by pulsed gas feeding. The adhesion and hardness of the multilayered Ti/TiN films is improved with increasing on-off ratio or decreasing deposition period; the on-off ratio has a negligible effect on the surface defects of the multilayered Ti/TiN films while the surface defects of the multilayered Ti/TiN films become more obvious at a long deposition period.


2019 ◽  
Vol 53 (11) ◽  
pp. 1457-1464
Author(s):  
P. N. Krylov ◽  
A. S. Alalykin ◽  
E. A. Durman ◽  
R. M. Zakirova ◽  
I. V. Fedotova

Vacuum ◽  
2004 ◽  
Vol 76 (2-3) ◽  
pp. 329-333
Author(s):  
P. Hrkút ◽  
M. Držík ◽  
M. Mozolík ◽  
P. Kováč ◽  
Š. Haščík ◽  
...  

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