Rapid and Inexpensive Steam Distillation Method for Routine Analysis of Inorganic Nitrogen in Alkaline Calcareous Soils

2011 ◽  
Vol 42 (8) ◽  
pp. 920-931 ◽  
Author(s):  
Muhammad Akhtar ◽  
F. Hussain ◽  
T. M. Qureshi ◽  
M. Y. Ashraf ◽  
J. Akhter ◽  
...  
Keyword(s):  
Steam Distillation ◽  
Inorganic Nitrogen ◽  
Calcareous Soils ◽  
Routine Analysis ◽  
Distillation Method

scholarly journals Chemical composition and content of essential oil from the bud of cultivated Turkish clove (Syzygium aromaticum L.)

BioResources ◽  
2007 ◽  
Vol 2 (2) ◽  
pp. 265-269 ◽  
Author(s):  
M. Hakki Alma ◽  
Murat Ertaş ◽  
Siegfrie Nitz ◽  
Hubert Kollmannsberger
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Essential Oils ◽  
Mediterranean Region ◽  
Steam Distillation ◽  
Syzygium Aromaticum ◽  
Distillation Method ◽  
Eugenyl Acetate ◽  
Clove Bud Oil ◽  
Oil Company

In this study, clove bud oil, which was cultivated in the Mediterranean region of Turkey, was provided from a private essential oil company in Turkey. Essential oil from clove (Syzygium aromaticum L.) was obtained from steam-distillation method, and its chemical composition was analyzed by GC and GC-MS. The results showed that the essential oils mainly contained about 87.00% eugenol, 8.01% eugenyl acetate and 3.56% β-Caryophyllene. The chemical composition of the Turkish clove bud oil was comparable to those of trees naturally grown in their native regions.

scholarly journals Essential Oil from Lemon (Citrus aurantifolia) Grown in Ben Tre Province, Vietnam: Condition Extraction, Chemical Composition and Antibacterial Properties

2020 ◽  
Vol 32 (4) ◽  
pp. 965-969
Author(s):  
Ngo Thi To Quyen ◽  
Nguyen Thi Ngoc Quyen ◽  
Huynh Thi Kieu Linh ◽  
Thuy Trang Le Ngoc ◽  
Hoang Le Tuan Anh ◽  
...  
Keyword(s):  
Essential Oil ◽  
Steam Distillation ◽  
Antibacterial Properties ◽  
Antibacterial Activities ◽  
Oil Yield ◽  
Distillation Method ◽  
Bioactive Components ◽  
Citrus Aurantifolia ◽  
Physico Chemical ◽  
Essential Oil Yield

In present study, a steam distillation method has been adopted for extraction of the essential oil from Vietnamese lemon (Citrus aurantifolia) peel harvested from Tien Giang Province, Vietnam. Various extraction conditions influencing the oil yield were investigated. The resulting essential oil was evaluated for physico-chemical characteristics and antibacterial activities. The chemic al composition of oil was investigated by GC-MS. The results showed that with grinded lemon peel, a ratio of water and lemon peels of 3:1 (mL/g), extraction time of 90 min at 120 ºC, the highest essential oil yield was attained at 2.1 %. Bioactive components found at high content included limonene (64.90 %), γ-terpinene (13.70 %), β-pinene (11.89 %), α-pinene (2.11 %), β-cymene (1.80 %) and sabinen (1.52 %). The lemon essential oil in this study was found to inhibit five bacteria strains including Staphylococcus aureus, Bacillus cereus, Escherichia coli, Salmonella enterica and Pseudomonas aeruginosa.

scholarly journals Gas chromatography of γ-BHC in milk by steam distillation method

1971 ◽  
Vol 20 (3) ◽  
pp. 364-365 ◽  
Author(s):  
Kazuyuki HIRANO ◽  
Shunsuke KAGEHIRA ◽  
Tomoko MIZUNO ◽  
Satoshi KAWAI ◽  
Takeo OHNO
Keyword(s):  
Gas Chromatography ◽  
Steam Distillation ◽  
Distillation Method

Determination of Formaldehyde in Water-Borne Coatings by HPLC

2017 ◽  
Vol 726 ◽  
pp. 355-359 ◽  
Author(s):  
Ming Yu Wang ◽  
Zhong Bao Guo ◽  
Hong Yan Guan ◽  
Man Li
Keyword(s):  
Extraction Method ◽  
High Performance ◽  
Steam Distillation ◽  
High Performance Liquid Chromatographic ◽  
Distillation Method ◽  
Efficient Extraction ◽  
Liquid Chromatographic ◽  
Good Linear Correlation ◽  
Water Borne

A method for determination of formaldehyde in water-borne coatings by high-performance liquid chromatographic was proposed. Ultrasonic water extraction method was used instead of the traditional steam distillation method can be more rapid and efficient extraction of target, filtered and derivatived with DNPH. The extract was separated by C18 column with an elution composed of acetonitrile and water, and detected at 352nm. The detection limit was 0.1mg/L. The method showed good linear correlation, R2 was 0.9997 at the range of 0.1mg/L ~ 20 mg/L. Recovery was 95% ～105%. This method is simple, effective and sensitive.

Chemical Components and Nitrite Cleaning Activity of Essential Oil from Tagetes erecta L. Leaf

2011 ◽  
Vol 183-185 ◽  
pp. 1168-1172 ◽  
Author(s):  
Jian Li ◽  
Shuai Di Song ◽  
Ruo Nan Zhang ◽  
Ning Liu ◽  
Chen Chen Li
Keyword(s):  
Essential Oil ◽  
Sodium Nitrite ◽  
Steam Distillation ◽  
Chemical Components ◽  
Tagetes Erecta ◽  
Heilongjiang Province ◽  
Distillation Method ◽  
Ms Analysis ◽  
Tagetes Erecta L

Steam distillation oil (SDO) and simultaneous distillation oil (SDEO) were obtained from Tagetes Erecta L. leaf of Heilongjiang province by steam distillation method and simultaneous distillation method, respectively. The yields were 0.0943% and 1.005%. Compared the differentiation of essential oil through the GC-MS analysis, the result indicated that there were twenty-nine kinds of compounds can be confirmed from SDO and fifty-one kinds can be confirmed from SDEO. The two kinds of essential oil were assayed for affinity to scavenge sodium nitrite for the purpose of characterizing mechanisms of nitrite cleaning activity. Both show strong nitrite cleaning activity up to a concentration of 0.1mL.The maximum scavenging rate was 95.18% (SDO) and 54.28% (SDEO).

scholarly journals Composition of essential oil of plants some species of the genus Agastache l. Introduced in Belarus

2019 ◽  
Vol 64 (2) ◽  
pp. 147-155
Author(s):  
N. A. Kovalenko ◽  
G. N. Supichenko ◽  
V. N. Leontiev ◽  
A. G. Shutova
Keyword(s):  
Essential Oil ◽  
Essential Oils ◽  
Steam Distillation ◽  
Quantitative Composition ◽  
Gas Liquid Chromatography ◽  
Distillation Method ◽  
Methyl Chavicol ◽  
Oil Distribution ◽  
Main Component ◽  
Optically Pure

The steam distillation method was used to obtain samples of essential oil of some species of genus Agastache L. introduced in Belarus. More than 20 components have been identified and determined in the essential oils of Agastache pallidiflora ssp.neomexicana L., Agastache aurantiaca L., Agastache mexicana L., Agastache foeniculum L. by gas liquid chromatography.The quantitative composition of the samples of essential oils depends on the type of plant material. The main its components are limonene, 1.8-cineol, mentone, isomentone, methyl chavicol, methyeugenol. The main component of essential oils Agastache pallidiflora ssp. neomexicana L. и Agastache aurantiaca L is mentone (40–65 %). Essential oil Agastache foeniculum L. is enriched with pulegone and isomentone. Methyl chavicol and methyleugenol dominate in Agastache mexicana essential oil. Distribution of the enantiomers of limonene, menthone and pulegone are shown. Regardless of the plant species, the samples are optically pure in the (+)-pulegone. The nature of the distribution of the enantiomers of limonene and menthone is an individual characteristic of the studied Agastache L. essential oils.

Analysis of Sulfites in Shrimp Using Rapid Distillation Followed by Redox Titration1

1988 ◽  
Vol 51 (2) ◽  
pp. 137-138 ◽  
Author(s):  
MARIAN V. SIMPSON ◽  
W. STEVEN OTWELL ◽  
MAURICE R. MARSHALL ◽  
JOHN A. CORNELL
Keyword(s):  
Statistical Analysis ◽  
Steam Distillation ◽  
Accurate Determination ◽  
T Test ◽  
Distillation Method ◽  
Student’S T ◽  
Student’S T Test

The use of rapid steam distillation followed by redox iodine titration provides a rapid and accurate determination of total sufite residual in shrimp. Values obtained for sulfite-treated shrimp using the rapid distillation method gave comparable results to those of the officially recognized Monier-Williams method. Values for the rapid distillation method ranged from 6 to 212 ppm while those of the Monier-Williams procedure ranged from 6 to 241 ppm for untreated and treated shrimps, respectively. Statistical analysis using two-sample Student's t-test indicated that there were no significant differences (p>0.05) for residual levels below 100 ppm but the values obtained by the rapid distillation method and the Monier-Williams procedure were significantly different (p<0.05) at concentrations near and above 100 ppm.

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