Characterization of lattice defects in strontium titanate single crystals by X-ray topography and transmission electron microscopy

2000 ◽  
Vol 49 (1) ◽  
pp. 89-92 ◽  
Author(s):  
J. Yamanaka ◽  
J.-i. Yoshimura ◽  
S. Kimura
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Single Crystals ◽  
Strontium Titanate ◽  
Lattice Defects ◽  
X Ray ◽  
Transmission Electron

Detonation Synthesis of Nano-Size Materials

1995 ◽  
Vol 418 ◽  
Author(s):  
J. Forbes ◽  
J. Davis ◽  
C. Wong
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Nucleation And Growth ◽  
Detonation Synthesis ◽  
X Ray Diffraction ◽  
Crystalline Materials ◽  
X Ray ◽  
Transmission Electron ◽  
Nano Size

AbstractThe detonation of explosives typically creates 100's of kbar pressures and 1000's K temperatures. These pressures and temperatures last for only a fraction of a microsecond as the products expand. Nucleation and growth of crystalline materials can occur under these conditions. Recovery of these materials is difficult but can occur in some circumstances. This paper describes the detonation synthesis facility, recovery of nano-size diamond, and plans to synthesize other nano-size materials by modifying the chemical composition of explosive compounds. The characterization of nano-size diamonds by transmission electron microscopy and electron diffraction, X-ray diffraction and Raman spectroscopy will also be reported.

Hydrothermal Synthesis and Characterization of BiFeO3 Polyhedral Crystallites

2012 ◽  
Vol 174-177 ◽  
pp. 508-511
Author(s):  
Lin Lin Yang ◽  
Yong Gang Wang ◽  
Yu Jiang Wang ◽  
Xiao Feng Wang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
Xrd Pattern ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

BiFeO3 polyhedrons had been successfully synthesized via a hydrothermal method. The as-prepared products were characterized by power X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The possible mechanisms for the formation of BiFeO3 polyhedrons were discussed. Though comparison experiments, it was found that the kind of precursor played a key role on the morphology control of BiFeO3 crystals.

The Starting Members of the Series Pr4n+2(C2)nBr5n+5 (n = 1, 2, 3)

2009 ◽  
Vol 64 (8) ◽  
pp. 922-928 ◽  
Author(s):  
Manuel Christian Schaloske ◽  
Hansjürgen Mattausch ◽  
Viola Duppel ◽  
Lorenz Kienle ◽  
Arndt Simon
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Single Crystals ◽  
Lattice Parameters ◽  
Space Group ◽  
X Ray ◽  
Transmission Electron ◽  
General Series ◽  
Microscopy Techniques

The compounds Pr6(C2)Br10, Pr10(C2)2Br15 and Pr14(C2)3Br20 were prepared from PrBr3 and the appropriate amounts of Pr and C and characterized by X-ray structure analyses of single crystals. All three compounds crystallize in space group P1 with lattice parameters a = 7.571(2), b = 9.004(2), c = 9.062(2) Å ,α = 108.57(3), β = 97.77(3), γ = 106.28(3)◦ for Pr6(C2)Br10; a = 9.098(2), b = 10.127(2), c = 10.965(2) A° , α = 70.38(3), β = 66.31(3), γ = 70.84(3)◦ for Pr10(C2)2Br15; a = 9.054(2), b = 10.935(2), c = 13.352(3) Å , α = 86.27(3), β = 72.57(3), γ = 66.88(3)◦ for Pr14(C2)3Br20. They are members of a general series Ln4n+2(C2)nBr5n+5 and isostructural with the corresponding iodides known for Ln = La, Ce, Pr. Pr6(C2)Br10 was further characterized via transmission electron microscopy techniques

Preparation and Characterization of Monodisperse Ceria Microspheres

2010 ◽  
Vol 434-435 ◽  
pp. 850-852
Author(s):  
Qi Wang ◽  
Bo Yin ◽  
Zhen Wang ◽  
Gen Li Shen ◽  
Yun Fa Chen
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Particle Size ◽  
Electron Microscope ◽  
Crystalline Form ◽  
X Ray ◽  
Transmission Electron ◽  
Particle Size Analyzer ◽  
Scanning Electron

In present work, ceria microspheres were synthesized by template hydrothermal method. Crystalline form of the as-synthesized ceria microspheres was defined by X-ray powder diffraction (XRD) and high resolution transmission electron microscopy (HRTEM). Dispersibility of ceria microspheres was comprehensively characterized using scanning electron microscope (SEM) observation and laser particle size analyzer. Furthermore, the ultraviolet light absorption performances of ceria microspheres with several different sizes were compared by ultraviolet visible spectrophotometer. The results showed that ceria microspheres presented excellent UV absorbent property and the size influence was remarkable.

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