Two-photon electron emission from smooth and rough metal films in the threshold region

AbstractOur recent progress in the direct-write femtosecond laser material processing technologies, nanostructuring, and fabrication of photonic devices is reviewed. Special attention is given to the sub-wavelength microstructuring of metals and two-photon polymerization (2PP) technique. Formation of microbumps and nanojets on thin metal films under single pulse laser irradiation is discussed. Microstructuring of different photosensitive materials by 2PP technique is demonstrated. Numerous applications of this technology for the fabrication of 3d structures, waveguides, photonic crystals, etc. are studied.

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Electrical conductivity and electron emission from discontinuous metal films of homogeneous structure

Thin Solid Films ◽

10.1016/0040-6090(81)90535-6 ◽

1981 ◽

Vol 76 (4) ◽

pp. 359-378 ◽

Cited By ~ 33

Author(s):

P.G. Borziak ◽

Yu.A. Kulyupin ◽

S.A. Nepijko ◽

V.G. Shamonya

Keyword(s):

Electrical Conductivity ◽

Electron Emission ◽

Metal Films ◽

Homogeneous Structure

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Historical Introduction

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100077670 ◽

1977 ◽

Vol 35 ◽

pp. 2-5

Author(s):

R. D. Heidenreich

Keyword(s):

Electron Emission ◽

Secondary Electron ◽

Secondary Electron Emission ◽

50Th Anniversary ◽

Secondary Emission ◽

Wave Nature ◽

Nobel Prize In Physics ◽

Primary Electrons ◽

The U.S ◽

Mutual Agreement

This program has been organized by the EMSA to commensurate the 50th anniversary of the experimental verification of the wave nature of the electron. Davisson and Germer in the U.S. and Thomson and Reid in Britian accomplished this at about the same time. Their findings were published in Nature in 1927 by mutual agreement since their independent efforts had led to the same conclusion at about the same time. In 1937 Davisson and Thomson shared the Nobel Prize in physics for demonstrating the wave nature of the electron deduced in 1924 by Louis de Broglie.The Davisson experiments (1921-1927) were concerned with the angular distribution of secondary electron emission from nickel surfaces produced by 150 volt primary electrons. The motivation was the effect of secondary emission on the characteristics of vacuum tubes but significant deviations from the results expected for a corpuscular electron led to a diffraction interpretation suggested by Elasser in 1925.

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Macromolecular structures of biological specimens are not obscured by controlled osmium impregnation

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100076639 ◽

1983 ◽

Vol 41 ◽

pp. 606-607

Author(s):

Klaus-Ruediger Peters ◽

Samuel A. Green

Keyword(s):

Thin Films ◽

Electrical Conductivity ◽

Critical Point ◽

Metal Films ◽

High Magnification ◽

Osmium Impregnation ◽

Instrumental Resolution ◽

20 Nm ◽

Continuous Metal

High magnification imaging of macromolecules on metal coated biological specimens is limited only by wet preparation procedures since recently obtained instrumental resolution allows visualization of topographic structures as smal l as 1-2 nm. Details of such dimensions may be visualized if continuous metal films with a thickness of 2 nm or less are applied. Such thin films give sufficient contrast in TEM as well as in SEM (SE-I image mode). The requisite increase in electrical conductivity for SEM of biological specimens is achieved through the use of ligand mediated wet osmiuum impregnation of the specimen before critical point (CP) drying. A commonly used ligand is thiocarbohvdrazide (TCH), first introduced to TEM for en block staining of lipids and glvcomacromolecules with osmium black. Now TCH is also used for SEM. However, after ligand mediated osinification nonspecific osmium black precipitates were often found obscuring surface details with large diffuse aggregates or with dense particular deposits, 2-20 nm in size. Thus, only low magnification work was considered possible after TCH appl ication.

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