A new calibration concept of the Pulsed Electro Acoustic method allowing to improve charge density measurement

Author(s):  
M. Arnaout ◽  
F. Baudoin ◽  
L. Berquez ◽  
D. Payan
2003 ◽  
Vol 9 (5) ◽  
pp. 419-427 ◽  
Author(s):  
Victor A. Streltsov ◽  
Philip N.H. Nakashima ◽  
Andrew W.S. Johnson

Current X-ray diffraction techniques intended for “ideally imperfect” specimens provide structure factors only on a relative scale and ever-present multiple scattering in strong low-angle Bragg reflections is difficult to correct. Multiple scattering is implicit in the quantitative convergent beam electron diffraction (QCBED) method, which provides absolutely scaled structure factors. Conventional single crystal X-ray diffraction has proved adequate in softer materials where crystal perfection is limited. In hard materials, the highly perfect nature of the crystals is often a difficulty, due to the inadequacy of the conventional corrections for multiple scattering (extinction corrections). The present study on α-Al2O3 exploits the complementarity of synchrotron X-ray measurements for weak and medium intensities and QCBED measurement of the strong low-angle reflections. Two-dimensional near zone axis QCBED data from different crystals at various accelerating voltages, thicknesses, and orientations have been matched using Bloch-wave and multislice methods. The reproducibility of QCBED data is better than 0.5%. The low-angle strong QCBED structure factors were combined with middle and high-angle extinction-free data from synchrotron X-ray diffraction measurements. Static deformation charge density maps for α-Al2O3 have been calculated from a multipole expansion model refined using the combined QCBED and X-ray data.


2003 ◽  
Vol 356-357 ◽  
pp. 84-86 ◽  
Author(s):  
T. Noritake ◽  
S. Towata ◽  
M. Aoki ◽  
Y. Seno ◽  
Y. Hirose ◽  
...  

2021 ◽  
Author(s):  
Amit Kumar ◽  
V. Subramanian ◽  
Shailesh Joshi ◽  
B. Venkatraman

In the present ongoing pandemic, the N95 respirator is an essential protective barrier to suppress the spread of the SARS-Cov-2 virus and protect the frontline worker from exposure. The N95 respirators are meant for single usage; however, they can be used after decontamination in-light of the economy and shortfall in availability. At this juncture, the respirators performance after various types of sterilization and usage condition is required to be analyzed in detail. With this motto, this work has proceeded. The filtration efficiency, pressure drop, and quality factor of the respirator are evaluated for two face velocities (5.8 and 26.4 cm/s) following different sterilization methods. Sterilization techniques used here are dry air oven heating, gamma irradiation, and immersing in a 10% concentration of liquid hydrogen peroxide. The particle filtration performance and electrostatic surface charge density measurement are used to determine the facemasks efficacy after sterilization. The methods recommended to sterilize N95 masks without affecting their performance are (i) using dry air heat at 80oC and (ii) H2O2 soaking. The highest reduction in filtration efficiency is observed to be 30-35% after gamma irradiation due to a change in the electrostatic properties of the respirator layers. However, the filtration efficiency does not change significantly for other sterilization methods despite a change in charge density, but there is no direct correlation with filtration efficiency. Electrostatic charge measurement of the filtration layer is a crucial indicator of filtration efficiency degradation. Policymakers can use these data during potential future N95 shortage to assess the viability of sterilization methods.


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