Selective ultrasound‐assisted aqueous extraction of polyphenols from pomegranate peels and seeds

2020 ◽  
Vol 44 (7) ◽  
Author(s):  
Hiba N. Rajha ◽  
Mohamed Koubaa ◽  
Nadia Boussetta ◽  
Richard G. Maroun ◽  
Nicolas Louka ◽  
...  
2015 ◽  
Vol 11 (4) ◽  
pp. 479-492 ◽  
Author(s):  
Tuyen C. Kha ◽  
Minh H. Nguyen ◽  
Paul D. Roach ◽  
Costas E. Stathopoulos

Abstract The study aimed to optimise the ultrasound-assisted aqueous extraction of oil, β-carotene and lycopene from powdered microwave-dried gac arils. Ultrasound power, extraction time, powder particle size and the ratio of water to gac powder during the extraction, the centrifugal force used to recover the extracted components were investigated. Microwave-drying followed by aqueous extraction without ultrasound-assistance and air-drying followed by aqueous extraction with or without ultrasound-assistance was also carried out for comparisons. The gac material left behind after the extractions was also investigated using scanning electron microscopy (SEM). The results showed that ultrasound power of 32 W/g of aril powder, extraction time of 20 min, powder particle sizes of 0.3–0.5 mm, a ratio of water to powder of 9 g/g and a centrifugal force of 6,750×g gave optimal extraction efficiencies for oil (90%), β-carotene (84%) and lycopene (83%), and the oil had a low peroxide value (PV) of 2.2 meq/kg. The SEM analysis confirmed that the combination of microwave-drying followed by ultrasound-assisted aqueous extraction caused strong disruption of the gac aril cellular structures, which was consistent with the high extraction of oil, β-carotene and lycopene obtained with the combination. It was concluded that gac oil containing high amounts of β-carotene and lycopene and having a low PV could be extracted using microwave-drying and ultrasound-assisted aqueous extraction.


2016 ◽  
Vol 81 (12) ◽  
pp. 1441-1453
Author(s):  
Aleksandra Tasic ◽  
Ivana Sredovic-Ignjatovic ◽  
Ljubisa Ignjatovic ◽  
Danijel Djuranovic ◽  
Malisa Antic

Three different techniques were applied for the aqueous extraction of anions from coal and fly ash: rotary mixer- and ultrasonic-assisted extraction with different duration time, and microwave-assisted extraction at different temperatures. Validation showed that the ion-chromatographic method was suitable for the analysis of anions in coal and fly ash extracts. The variations in the amounts of anions using different extraction times during rotary-assisted extraction were minimal for all investigated anions. The efficiency of ultrasound-assisted extraction of anions from coal depended on the sonication time and was highest at 30 min. The ultrasound-assisted extraction was less efficient for the extraction of anions from fly ash than rotary-assisted extraction. Increase of temperature in the microwave-assisted extraction had a positive effect on the amounts of all anions extracted from coal and sulphate from fly ash, while the amounts of fluoride and chloride in fly ash extracts decreased. The microwave-assisted extraction of coal at 150?C was compared with standard ASTM methods, and results were in good agreement only for chloride. Changes in the pH value and conductivity during ultrasound-assisted extraction were measured in order to explain changes on the surface of coal particles in contact with water and different processes that occur under environmental conditions.


2016 ◽  
Vol 194 ◽  
pp. 503-507 ◽  
Author(s):  
Maryam Khoei ◽  
Fereshteh Chekin

2015 ◽  
Vol 1113 ◽  
pp. 477-480 ◽  
Author(s):  
F.Z. Asma ◽  
M.H. Rodiah ◽  
M.Y. Aziah ◽  
M.N. Norakma ◽  
I. Nurhafizah

There is an abundance of waste contributed by most agricultural industries. Coconut industry wastes such as the (exocarp) outer layer and (mesocarp) husk can be exploited and turned into useful products such as natural dyes. In the present work, solvent extraction of natural dye from exocarp and mesocarp of Cocos nucifera using ultrasound has been studied. Methanol, ethanol and acetone with varying concentration (20%-70%) were used in the extraction process which was carried out at 30°C for 1 hour. Aqueous extraction was also performed with the same condition and acts as a control sample. The extraction of pigment from exocarp using 50% acetone produced the highest percentage of the yield of colorant (11.6%), while for mesocarp extraction, both 50% and 60% acetone yielded the highest percentage of colorant which was 9.2%. In addition, control sample (aqueous extraction of mesocarp and exocarp) showed lower percentages of the yield of colorant which was 6.4% and 6.8%, respectively. The results indicate that there was a significant improvement in the percentage of yield of natural colorant obtained due to the use of ultrasound.


Chemosphere ◽  
2021 ◽  
Vol 263 ◽  
pp. 128071
Author(s):  
P. Selvakumar ◽  
V. Karthik ◽  
P. Senthil Kumar ◽  
P. Asaithambi ◽  
S. Kavitha ◽  
...  

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