Ultrasound-assisted intensified aqueous extraction of phenolics from waste Syzygium cumini leaves: Kinetic studies and evaluation of antioxidant, antidiabetic and anticancer potential

2022 ◽  
pp. 101547
Author(s):  
Komal V. Mahindrakar ◽  
Virendra K. Rathod
2015 ◽  
Vol 11 (4) ◽  
pp. 479-492 ◽  
Author(s):  
Tuyen C. Kha ◽  
Minh H. Nguyen ◽  
Paul D. Roach ◽  
Costas E. Stathopoulos

Abstract The study aimed to optimise the ultrasound-assisted aqueous extraction of oil, β-carotene and lycopene from powdered microwave-dried gac arils. Ultrasound power, extraction time, powder particle size and the ratio of water to gac powder during the extraction, the centrifugal force used to recover the extracted components were investigated. Microwave-drying followed by aqueous extraction without ultrasound-assistance and air-drying followed by aqueous extraction with or without ultrasound-assistance was also carried out for comparisons. The gac material left behind after the extractions was also investigated using scanning electron microscopy (SEM). The results showed that ultrasound power of 32 W/g of aril powder, extraction time of 20 min, powder particle sizes of 0.3–0.5 mm, a ratio of water to powder of 9 g/g and a centrifugal force of 6,750×g gave optimal extraction efficiencies for oil (90%), β-carotene (84%) and lycopene (83%), and the oil had a low peroxide value (PV) of 2.2 meq/kg. The SEM analysis confirmed that the combination of microwave-drying followed by ultrasound-assisted aqueous extraction caused strong disruption of the gac aril cellular structures, which was consistent with the high extraction of oil, β-carotene and lycopene obtained with the combination. It was concluded that gac oil containing high amounts of β-carotene and lycopene and having a low PV could be extracted using microwave-drying and ultrasound-assisted aqueous extraction.


2020 ◽  
Vol 44 (7) ◽  
Author(s):  
Hiba N. Rajha ◽  
Mohamed Koubaa ◽  
Nadia Boussetta ◽  
Richard G. Maroun ◽  
Nicolas Louka ◽  
...  

2016 ◽  
Vol 81 (12) ◽  
pp. 1441-1453
Author(s):  
Aleksandra Tasic ◽  
Ivana Sredovic-Ignjatovic ◽  
Ljubisa Ignjatovic ◽  
Danijel Djuranovic ◽  
Malisa Antic

Three different techniques were applied for the aqueous extraction of anions from coal and fly ash: rotary mixer- and ultrasonic-assisted extraction with different duration time, and microwave-assisted extraction at different temperatures. Validation showed that the ion-chromatographic method was suitable for the analysis of anions in coal and fly ash extracts. The variations in the amounts of anions using different extraction times during rotary-assisted extraction were minimal for all investigated anions. The efficiency of ultrasound-assisted extraction of anions from coal depended on the sonication time and was highest at 30 min. The ultrasound-assisted extraction was less efficient for the extraction of anions from fly ash than rotary-assisted extraction. Increase of temperature in the microwave-assisted extraction had a positive effect on the amounts of all anions extracted from coal and sulphate from fly ash, while the amounts of fluoride and chloride in fly ash extracts decreased. The microwave-assisted extraction of coal at 150?C was compared with standard ASTM methods, and results were in good agreement only for chloride. Changes in the pH value and conductivity during ultrasound-assisted extraction were measured in order to explain changes on the surface of coal particles in contact with water and different processes that occur under environmental conditions.


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