A Phase-Sensitive Technique for Measurements of Liquid Thermal Conductivity

2010 ◽  
Vol 132 (5) ◽  
Author(s):  
Zhefu Wang ◽  
Richard B. Peterson

An experimental technique based on the thermal wave approach for measuring the thermal conductivity of liquids is developed in this paper. A stainless steel strip functions as both a heating element and a sealing cover for a chamber containing a test liquid. A periodic current passing through this metal strip generates a periodic Joule heating source. An infrared detector measures the temperature response at the front surface of the stainless steel strip. The phase and magnitude of the temperature response with respect to the heating signal were measured by a lock-in amplifier at various frequencies from 22 Hz to 502 Hz. A one-dimensional, two-layered transient heat conduction model was developed to predict the temperature response on the front surface of the stainless steel strip. The phase information from this temperature response shows high sensitivity to the change in thermal properties of the liquid layer and is employed to match experimental data to find the thermal properties of the test liquid. The measured thermal conductivities of water and ethylene glycol agree quite well with the data from literature and support the validity of this measurement technique. An aqueous fluid consisting of gold nanoparticles is tested and anomalous thermal conductivity enhancement is observed. A discrepancy in the thermal transport behavior between pure liquids and nanofluids is suggested from our experimental results.

2008 ◽  
Author(s):  
Zhefu Wang ◽  
Richard B. Peterson

This work develops an experimental technique capable of determining thermal conductivity of liquids with application to nanofluids. A periodic current passing through a thin stainless steel strip generates a periodic Joule heating source and an infrared detector measures the temperature response at the front surface of the stainless steel strip. An open chamber is machined out of a delrin plate with the stainless steel strip acting as the sealing cover. This resulting closed chamber contains the test liquid. The phase and magnitude of the temperature response were measured using a lock-in amplifier at various frequencies from 22 to 502 Hz. A one-dimensional, two-layered transient heat conduction model was developed to predict the temperature response on the front surface of the stainless steel strip. This temperature response, including phase and magnitude, is a function of the thermal properties of the liquid. The phase information shows high sensitivity to thermal properties of the liquid layer and is employed to match experimental data to find thermal conductivities. The measured thermal conductivities of water and ethylene glycol agree well with data from the literature and support the validity of this measurement technique. An aqueous fluid consisting of gold nanoparticles was tested. Anomalous thermal conductivity enhancement was observed. Our measurement results also show a divergence of thermal transport behavior between nanofluids and pure liquids. This suggests the need to carefully examine the role of measurement techniques in the study of nanofluid heat transfer phenomena.


1999 ◽  
Vol 121 (3) ◽  
pp. 528-536 ◽  
Author(s):  
S. W. Indermuehle ◽  
R. B. Peterson

A phase-sensitive measurement technique for determining two independent thermal properties of a thin dielectric film is presented. The technique involves measuring a specimen’s front surface temperature response to a periodic heating signal over a range of frequencies. The phase shift of the temperature response is fit to an analytical model using thermal diffusivity and effusivity as fitting parameters, from which the thermal conductivity and specific heat can be calculated. The method has been applied to 1.72-μm thick films of SiO2 thermally grown on a silicon substrate. Thermal properties were obtained through a temperature range from 25°C to 300°C. One interesting outcome stemming from analysis of the experimental data is the ability to extract both thermal conductivity and specific heat of a thin film from phase information alone. The properties obtained with this method are slightly below the bulk values for fused silica with a measured room temperature (25°C) thermal conductivity of 1.28 ± 0.12 W/m-K.


Author(s):  
Heng Ban ◽  
Zilong Hua

The laser flash method is a standard method for thermal diffusivity measurement. This paper reports the development of a method and theory that extends the standard laser flash method to measure thermal conductivity and thermal diffusivity simultaneously. By attaching a transparent reference layer with known thermal properties on the back of a sample, the thermal conductivity and thermal diffusivity of the sample can be extracted from the temperature response of the interface between the sample and the reference layer to a heating pulse on the front surface. The theory can be applied for sample and reference layer with different thermal properties and thickness, and the original analysis of the laser flash method becomes a limiting case of the current theory with an infinitely small thickness of the reference layer. The uncertainty analysis was performed and results indicated that the laser flash method can be used to extract the thermal conductivity and diffusivity of the sample. The results can be applied to, for instance, opaque liquid in a quartz dish with silicon infrared detector measuring the temperature of liquid-quartz interface through the quartz.


2013 ◽  
Vol 465-466 ◽  
pp. 1060-1064 ◽  
Author(s):  
Zazuli Mohid ◽  
M.A. Liman ◽  
M.R.A. Rahman ◽  
N.H. Rafai ◽  
Erween Abdul Rahim

Welding parameters are directly influenced by the work material properties. Thermal properties such as thermal conductivity and melting point are very important to estimate the range of power required and the allowable scanning speed. However, when two or more different materials are involved, modifying lasing parameters are not enough to counter the problems such as imbalance melting region and weak adhesion of contact surface. To counter this problem, the characteristics of welding beads formation for both materials need to be clarified. In this study, comparison of welding beads constructed using the same scanning parameters were done to understand the different and similarity of melted region for the both materials. Actual welding of the both materials were done under different offset distance to obtain a balanced melting area and well mixed melting region.


2014 ◽  
Vol 660 ◽  
pp. 730-734 ◽  
Author(s):  
Khamisah Abdul Hamid ◽  
Wan Hamzah Azmi ◽  
Rizalman Mamat ◽  
Nur Ashikin Usri

Nanofluids are the new coolant fluid that has been widely investigates due to its ability to improved heat transfer better than conventional heat transfer fluid. The need to study the nanofluid properties has been increased to provide better understanding on nanofluid thermal properties and behavior. This study presents the measurement analysis on thermal conductivity enhancement of Al2O3 nanoparticles dispersed in ethylene glycol. The nanofluids are prepared using two step method for volume concentration range from 1.0 % to 4.0 %. The thermal conductivity measurement of the nanofluid is performed by KD2 Pro Thermal Properties Analyzer at working temperature range from 30 °C to 80 °C. The maximum enhancement in thermal conductivity is 21.1 % at volume concentration of 2.0 % and temperature of 70 °C. The results show that the thermal conductivity increases with the increase of nanofluid concentration and temperature. Also, the nanofluid shows enhancement in thermal conductivity compare to the base fluid.


Energies ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3763 ◽  
Author(s):  
Boldoo ◽  
Ham ◽  
Cho

Multiwalled carbon nanotubes (MWCNTs) have attracted attention from researchers because of their superior thermal properties and high optical absorption. In this investigation, the thermal and optical properties of functionalized and nonfunctionalized MWCNT nanofluid based on ethylene glycol/water were experimentally studied and compared. The results indicated that the use of the functionalized MWCNT nanofluid improved the thermal properties and optical absorption performance compared with the nonfunctionalized MWCNT nanofluid. The thermal conductivity enhancement of the functionalized MWCNT nanofluid was higher than that of the nonfunctionalized MWCNT nanofluid. The maximum thermal conductivity enhancement (10.15%) was observed in a functionalized MWCNT concentration of 0.01 wt% at 50 °C compared with the base fluid. In addition, the photo-thermal energy conversion efficiency of the functionalized MWCNT nanofluid was higher than that of the nonfunctionalized one owing to its higher light absorption and thermal conductivity.


2017 ◽  
Vol 30 (3) ◽  
pp. 365-374 ◽  
Author(s):  
Govind Sahu ◽  
VK Gaba ◽  
S Panda ◽  
B Acharya ◽  
SP Mahapatra

Silicone elastomer (SiR) nanocomposites were prepared using multiwalled carbon nanotubes (MWCNT) and nano-graphite (NG). The morphology of the SiR nanocomposites has been studied using scanning electron microscopy and high-resolution transmission electron microscopy techniques. Detailed analysis of the morphology reveals a uniform distribution of the MWCNT and NG filler particles in the silicone matrix. On increasing the filler loading, a continuous network structure is formed and aggregation takes place. The effect of the MWCNT and NG loadings on the thermal properties of the silicone elastomer has been investigated. The thermal properties of the SiR nanocomposites were measured by a thermal properties analyzer based on the transient hot-wire method. Studies also suggest that incorporation of nanoparticles improves the thermal conductivity of SiR nanocomposites. The thermal conductivity of SiR nanocomposites increased from 0.200 W/(m K) to 0.440 W/(m K) and to 0.310 W/(m K) for 6 wt% MWCNT and NG loadings, respectively. Because of the positive temperature coefficient and the conductive nature of the nanoparticles, the thermal conductivity of the material increased on increasing the temperature. The thermal diffusivity and the volumetric heat capacity of the SiR nanocomposites were measured. The thermal diffusivity of the SiR nanocomposites increased from 0.1194 mm2/s to 0.3209 mm2/s and to 0.2050 mm2/s for 6 wt% MWCNT and NG loadings, respectively. This indicates that the temperature response becomes faster with MWCNT and NG loadings. The volumetric heat capacity of the silicone elastomer nanocomposites decreased from 1.80 MJ/(m3K) to 1.34 MJ/(m3K) and to 1.40 MJ/(m3K) for 6 wt% MWCNT and NG loadings, respectively. Thus, MWCNT particles are more effective in increasing the thermal conductivity and diffusivity of the SiR nanocomposites, when compared to NG fillers at any loading.


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