Study for Control of Dimensional Distortion in Tempered Industrial Parts

Author(s):  
João Alfredo Scheidemantel ◽  
Christian Doré ◽  
Lucile Cecília Peruzzo

Abstract The presence of residual stress generated in the manufacturing process defines one of the biggest problems found in the mechanical metal industry. In the search of mechanical properties to a specific application, it is mandatory to impose the parts at very critical mechanical, chemical or thermal requests. The study analyzes all the steps that apply considerable stresses to the component during the manufacturing process and, therefore, discover which ones add more stresses to the yield limit of the material. It was also intended to contribute with relevant information regarding the surface integrity of the material, with bigger coverage in the residual stresses generated where, due to their nature and expressiveness, they can be beneficial or harmful to the component’s useful life. Accordingly, the objective was to analyze the raw material of SAE 4140 steel through its microstructure and verification of its chemical and mechanical characterization. In order to reduce the occurrence of dimensional distortions in excess of tolerance, we sought to identify the most critical step and, therefore, act with viable possibilities and without relevant costs for the prevention of the problem encountered. In order to measure its stress and define the process in which the highest inclusion of residual tractive stresses is characterized, these being the deleterious ones for the process and for the product, we used the method of measuring residual stresses by ray diffraction in X. In your measurement, the stresses included on the surface of the specimens were measured at specific stages of the process. X-ray diffraction analysis analyzes the diffraction planes and their respective interplanar distances from a specific material, as well as the densities of atoms along the crystalline planes. Using mathematical models, it is possible to measure the residual stress existing in the investigated parts. In view of the analysis by X-ray diffraction, it was verified the existence of disordered variations and modifications of the crystalline phases on the material surface, at the end of the finish machining process. These crystalline phases which, together with a less aggressive fabrication, favor plastic deformation due to the presence of residual stresses which surpass those of the yield limit of the analyzed material. In this sense, it was possible to determine which the most critical operation related to the component request is the machining in which it is applied. Since the subsequent processes only aggravates this condition, resulting in an unusable component for the proposed application without adding a higher cost to the product, either through the use of some rework or scrap procedure.

MRS Advances ◽  
2020 ◽  
Vol 5 (23-24) ◽  
pp. 1215-1223
Author(s):  
R.R. Phiri ◽  
O.P. Oladijo ◽  
E.T. Akinlabi

AbstractControl and manipulation of residual stresses in thin films is a key for attaining coatings with high mechanical and tribological performance. It is therefore imperative to have reliable residual stress measurements methods to further understand the dynamics involved. The sin2ψ method of X-ray diffraction was used to investigate the residual stresses on the tungsten carbide cobalt thin films deposited on a mild steel surface to understand the how the deposition parameters influence the generation of residual stresses within the substrate surface. X-ray spectra of the surface revealed an amorphous phase of the thin film therefore the stress measured was of the substrate surface and the effects of sputtering parameters on residual stress were analysed. Compressive stresses were identified within all samples studied. The results reveal that as the sputtering parameters are varied, the residual stresses also change. Optimum deposition parameters in terms of residual stresses were suggested.


2016 ◽  
Vol 368 ◽  
pp. 99-102
Author(s):  
Lukáš Zuzánek ◽  
Ondřej Řidký ◽  
Nikolaj Ganev ◽  
Kamil Kolařík

The basic principle of the X-ray diffraction analysis is based on the determination of components of residual stresses. They are determined on the basis of the change in the distance between atomic planes. The method is limited by a relatively small depth in which the X-ray beam penetrates into the analysed materials. For determination of residual stresses in the surface layer the X-ray diffraction and electrolytic polishing has to be combined. The article is deals with the determination of residual stress and real material structure of a laser-welded steel sample with an oxide surface layer. This surface layer is created during the rolling and it prevents the material from its corrosion. Before the X-ray diffraction analysis can be performed, this surface layer has to be removed. This surface layer cannot be removed with the help of electrolytic polishing and, therefore, it has to be removed mechanically. This mechanical procedure creates “technological” residual stress in the surface layer. This additional residual stress is removed by the electrolytic polishing in the depth between 20 and 80 μm. Finally, the real structure and residual stresses can be determined by using the X-ray diffraction techniques.


2008 ◽  
Vol 571-572 ◽  
pp. 277-282 ◽  
Author(s):  
Xu Song ◽  
Solène Chardonnet ◽  
Giancarlo Savini ◽  
Shu Yan Zhang ◽  
Willem J.J. Vorster ◽  
...  

The aim of the study presented here was to evaluate the residual stresses present in a bar of aluminium alloy 2124-T1 matrix composite (MMC) reinforced with 25vol% particulate silicon carbide (SiCp) using X-ray diffraction and 3D profilometry (curvature measurement using Mitutoyo/Renishaw coordinate measurement machine) and comparing these results with numerical models of residual strain and stress profiles obtained by a simple inelastic bending model and Finite Element Analysis (FEA). The residual strain distribution was introduced into the test piece by plastic deformation in the 4-point bending configuration. At the first stage of this study the elasticplastic behaviour of the MMC was characterized under static and cyclic loading to obtain the material parameters, hardening proprieties and cyclic hysteresis loops. Subsequently, synchrotron Xray diffraction and CMM curvature measurements were performed to deduce the residual stress profile in the central section of the bar. The experimental data obtained from these measurements were used in the inelastic bending and FEA simulations. The specimens were then subjected to incremental slitting using EDM (electric discharge machining) with continuous back and front face strain gauge monitoring. The X-ray diffraction and incremental slitting results were then analysed using direct and inverse eigenstrain methods. Residual stresses plots obtained by different methods show good agreement with each other.


2009 ◽  
Vol 24 (S1) ◽  
pp. S41-S44 ◽  
Author(s):  
A. T. Fry ◽  
J. D. Lord

Residual stresses impact on a wide variety of industrial sectors including the automotive, power generation, industrial plant, construction, aerospace, railway and transport industries, and a range of materials manufacturers and processing companies. The X-ray diffraction (XRD) technique is one of the most popular methods for measuring residual stress (Kandil et al., 2001) used routinely in quality control and materials characterization for validating models and design. The VAMAS TWA20 Project 3 activity on the “Measurement of Residual Stresses by X-ray Diffraction” was initiated by NPL in 2005 to examine various aspects of the XRD test procedure in support of work aimed at developing an international standard in this area. The purpose of this project was to examine and reduce some of the sources of scatter and uncertainty in the measurement of residual stress by X-ray diffraction on metallic materials, through an international intercomparison and validation exercise. One of the major issues the intercomparison highlighted was the problem associated with measuring residual stresses in austenitic stainless steel. The following paper describes this intercomparison, reviews the results of the exercise and details additional work looking at developing best practice for measuring residual stresses in austenitic stainless steel, for which X-ray measurements are somewhat unreliable and problematic.


Author(s):  
Cameron Lonsdale ◽  
John Oliver

Railroad wheels are manufactured with beneficial residual compressive hoop stresses, which are imparted by rim quenching and tempering. Hoop and radial residual stresses for wheels have been studied in detail by various organizations over the years and are relatively well characterized. However axial residual stresses, in the orientation across the rim width from back rim face to front rim face, have not been extensively investigated. This paper describes a failure mode known as a vertical split rim (VSR) and describes efforts to measure the axial residual stresses in, 1) new wheels, 2) service worn wheels and 3) wheels that have failed from VSRs. Initial axial residual stress measurement efforts, using core drilling and x-ray diffraction from the tread surface, are briefly reviewed. Further more extensive work using x-ray diffraction to measure axial residual stress on radial wheel slices is described and data are presented, focusing on differences between the three wheel types. The concept of Axial Stress Amplification (ASA) is outlined, and the relationship of axial residual stress to VSRs is discussed. A proposed mechanism for VSR formation is described. Future work, with a goal of reducing or eliminating VSRs in service, is considered.


2013 ◽  
Vol 768-769 ◽  
pp. 420-427 ◽  
Author(s):  
Jeremy Epp ◽  
Thilo Pirling ◽  
Thomas Hirsch

In this paper the microstructural and residual-stress analysis of an induction hardened plate of medium carbon steel is described. The stress gradient was determined using laboratory X-ray diffraction (IWT, Bremen, Germany) and neutron strain scanning (ILL, Grenoble, France). Due to slight variations of chemical composition in the depth, matchstick like (cross section 2×2mm²) d0-reference samples were prepared from a similarly treated sample. The d0shift induced by variation of chemical composition was measured by neutron and by X-ray diffraction along the strain free direction (sin²ψ*) and used for the evaluation of the neutron stress calculation. The d0distribution obtained from the neutron measurement did not appear reliable while the method using X-ray diffraction seems to be an efficient and reliable method to determine d0profiles in small samples. The evaluation of neutron measurements was then done using the X-ray diffraction d0distribution. High compressive residual stresses were measured in the hardened layer followed by high tensile residual stresses in the core. A comparison of the neutron measurements with X-ray diffraction (XRD) depth profiles obtained after successive layer removal showed that both methods give similar results. However, these investigations opened the question about the direct comparison of the residual stresses obtained by neutron and XRD. Indeed, a correction of the neutron data regarding the residual stresses in thickness direction might be necessary as these are released in the case of X-ray diffraction measurements after layer removal.


1996 ◽  
Vol 118 (4) ◽  
pp. 483-489 ◽  
Author(s):  
Y. Ahn ◽  
S. Chandrasekar ◽  
T. N. Farris

Machining produces surface residual stresses which significantly influence the strength and wear resistance of ceramic components. As new methods are developed for machining ceramics, a quick and reliable technique for measurement of residual stresses would be valuable in assessing the viability of these methods from a residual stress perspective. The residual stresses on ground and polished (i.e. machined) surfaces of soda-lime glass, Ni-Zn ferrite, and silicon nitride have been measured using an indentation technique with a Vickers indenter. In this technique, the surface extent of the median/radial cracks produced by the Vickers indenter in machined and in annealed ceramics are measured. These are then combined with a fracture mechanics analysis to estimate the surface residual stresses produced by machining. In order to determine the validity of the indentation technique for estimating machining residual stresses, these stresses were also measured using an X-ray diffraction and a deflection method. The residual stress values determined using the indentation technique in the machined ceramics were found to be reasonably close to those obtained from the X-ray diffraction and deflection methods. Since the indentation technique is relatively simple and easily applied, it offers a promising method for evaluating surface residual stresses in machined ceramics.


2012 ◽  
Vol 729 ◽  
pp. 199-204 ◽  
Author(s):  
Dávid Cseh ◽  
Valéria Mertinger

Residual stresses have a fundamental effect on the operational behaviour and lifetime of industrial products. The fatigue resistance of machine parts can be increased by introducing residual compressive stresses into the surface region. For certain machine parts especially in the vehicle industry the residual stress is strongly demanded by the quality control. For this reason, measuring the stress accurately is becoming increasingly important. The Almen test, which only gives a qualitative result, is widely used in the industry. Shot peening and rolling are methods which are suitable for creating elastic residual stresses. This paper examines the technologies used by Rába Futómű Nyrt. to increase the lifetime by means of residual stress. We performed analysis of the residual stress of samples shot peened the same way but under different heat treatment states. We compared the residual stress values of burnished and hardened shaft joints, and the residual stress states of gear made of hardened alloy, comparing the carbonized ones to ones which were shot peened under small intensity.


2014 ◽  
Vol 996 ◽  
pp. 469-474 ◽  
Author(s):  
Arne Kromm

Novel Low Transformation Temperature (LTT-) filler materials are specially designed for controlling residual stresses by means of adjusted martensite formation already during welding. Different alloying concepts compete for maximum stress reduction. Two newly developed LTT-alloys were evaluated concerning their potential for residual stress control. For this purpose residual stresses were determined in the surface and also in sub-surface areas of welded joints using X-ray diffraction and Neutron diffraction taking into account local variations of the unstrained lattice parameter.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3104 ◽  
Author(s):  
Marta Valášková ◽  
Zdeněk Klika ◽  
Boris Novosad ◽  
Bedřich Smetana

Kaolin is most often used as traditional raw material in ceramic industry. The purpose of the study was to obtain understanding of the structural and chemical variability of cordierite ceramics influenced by chemical and mineralogical properties of six raw kaolins taken from different localities when they are applied in ceramics mixtures with vermiculite and sintered up to 1300 °C. The X-ray diffraction and simultaneous thermogravimetric and differential thermal analysis were used to identify and characterize crystalline mineral phases and the course of reactions during the heating. The percentages of the crystalline and non-crystalline phases were newly determined by recalculation of the bulk chemical analyses of kaolins and cordierite ceramics using Chemical Quantitative Mineral Analysis (CQMA) method. Varying amounts of minerals in kaolins: kaolinite from 73.3 to 85.0, muscovite from 4.2 to 9.9, and quartz from 6.0 to 19.5 (mass %) affected amount of cordierite/indialite from 75.2 to 85.1, enstatite from 5.8 to 8.9 (when are calculated as their maximal possible percentages), and non-crystalline phases from 8.8 to 15.1 (mass %) in cordierite ceramics. Regression analysis predicted high relationship between quantity of: (a) kaolinite in kaolins and crystalline cordierite and (b) quartz in kaolins and non-crystalline phases in the ceramics. The migration of potassium from muscovite into the cordierite structure, melting point and crystallization of cordierite/indialite phases and pore size variability in relation to impurity of kaolins are documented and discussed.


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