Chemical and optical properties of thermally evaporated manganese oxide thin films

2006 ◽  
Vol 24 (5) ◽  
pp. 1746-1750 ◽  
Author(s):  
M. F. Al-Kuhaili
Author(s):  
Amin moghtaderi ◽  
Haleh kangarlou ◽  
Vahedeh razzazi

Manganese oxide thin films were produced on glass substrates by resistive evaporation at room temperature. The layers with different thickness (30 and 90 nm) at different deposition angle (0 and 40°) were prepared by electron gun evaporation method under ultra-high vacuum condition. After deposition pure manganese oxide thin films a post-annealing proses was used in a uniform oxygen flow of 300 (sccm) and at 500o kelvin annealing temperature. Optical transmittance and reflectance of the layers were measured in the wavelength of 350–850 nm by a spectrophotometer. Kramers–Kronig relations were used to calculate the optical constant. The influence of oxygen flow and annealing temperature on optical properties is investigated. It was found that film thickness and deposition angle plays a significant role on the nanostructures as well as optical properties of layers and cause major variations in behavior of thin titanium oxide films. The physical properties of materials were characterized by X-ray diffraction (XRD), FE-SEM, AFM, EDAX, and UV-Vis techniques.


2021 ◽  
Author(s):  
Amin moghtaderi ◽  
haleh kangarlou ◽  
Vahedeh razzazi

Abstract Manganese oxide thin films were deposited on glass substrates by resistive evaporation at room temperature. The layers were produced with electron gun evaporation method under ultra-high vacuum condition. Thickness of the layers was measured 60 and 120 nm, by a quartz crystal method. Deposition conditions such as deposition rate, vacuum pressure, incidence of angle and substrate temperature were the same for all layers. After producing pure manganese oxide layers a post-annealing method was used in the presence of a uniform oxygen flow of 300 (sccm) and at 320 oC annealing temperature. Optical reflectance and transmittance of the layers were measured in the wavelength of 350–850 nm by a spectrophotometer. Kramers–Kronig relations were used to calculate the optical constant. The influence of annealing temperature and oxygen flow on optical properties is investigated. It was found that film thickness and deposition angle plays an important role on the nanostructures as well as optical properties of layers and cause significant variations in behavior of thin titanium oxide films. The physical properties of materials were characterized by X-ray diffraction (XRD), FE-SEM, AFM, EDX, and UV-Vis techniques.


2021 ◽  
Vol 127 ◽  
pp. 105690
Author(s):  
A. Sáenz-Trevizo ◽  
D. Kuchle-Mena ◽  
P. Pizá-Ruiz ◽  
P. Amézaga-Madrid ◽  
O. Solís-Canto ◽  
...  

2010 ◽  
Vol 177 ◽  
pp. 201-203
Author(s):  
Jing Chu ◽  
Yu Lin Li ◽  
Bing Xu ◽  
Na Zhang ◽  
Qiang Li

Niobium oxide thin films were successfully synthesized starting from niobate nanosheets. The microstructure of as-prepared nanosheets was observed by TEM. The morphology of niobate thin films was investigated by SEM. The phase structure was determined by XRD. The transmittance spectra of as-obtained niobium oxide thin films were measured, and the optical properties were studied. The influences of different thickness on optical properties were also analyzed. As-prepared niobium thin films were treated by being heated at different temperature. The effects of soaking temperature on the structure and optical properties of niobium oxide thin films were discussed in detail.


2008 ◽  
Vol 1111 ◽  
Author(s):  
Celine Lecerf ◽  
Philippe Marie ◽  
Cedric Frilay ◽  
Julien Cardin ◽  
Xavier Portier

AbstractPhotoluminescence activity was observed for neodymium-doped gallium oxide thin films prepared by radiofrequency magnetron co-sputtering. Structural and optical properties of as-grown and annealed films were studied and photoluminescence activity was especially investigated. The most intense lines were associated to the 4F3/2  4I9/2 and 4F3/2  4I11/2 electronic transitions of Nd3+. The effects of deposition and treatment parameters such as the substrate temperature, the post anneal treatment or the neodymium content in the films were particularly examined with the aim to reach the best luminescence efficiency.


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