In situ search for life traces in extraterrestrial samples by synchrotron x-ray fluorescence 2D and 3D imaging

2007 ◽  
Author(s):  
Laurence Lemelle ◽  
Alexandre Simionovici ◽  
Murielle Salomé ◽  
Pierre Bleuet ◽  
Jean Susini ◽  
...  
Keyword(s):  
X Ray ◽  
Metals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 189 ◽  
Author(s):  
Francisco García-Moreno ◽  
Laurenz Alexander Radtke ◽  
Tillmann Robert Neu ◽  
Paul Hans Kamm ◽  
Manuela Klaus ◽  
...  

The foaming behaviour of aluminium alloys processed by the powder compaction technique depends crucially on the exact alloy composition. The AlSi8Mg4 alloy has been in use for a decade now, and it has been claimed that this composition lies in an “island of good foaming”. We investigated the reasons for this by systematically studying alloys around this composition by varying the Mg and Si content by a few percent. We applied in situ X-ray 2D and 3D imaging experiments combined with a quantitative nucleation number and expansion analysis, X-ray tomography of solid foams to assess the pore structure and pore size distribution, and in situ diffraction experiments to quantify the melt fraction at any moment. We found a correlation between melt fraction and expansion height and verified that the “island of good foaming” actually exists, and foams outside a preferred range for the liquid fraction—just above TS and between 40–60%—show a poorer expansion performance than the reference alloy AlSi8Mg4. A very slight increase of Si and decrease of Mg content might further improve this foam.


2019 ◽  
Vol 35 (24) ◽  
pp. 21-29 ◽  
Author(s):  
Yuxin Wang ◽  
Yu-chen Karen Chen ◽  
Wilson K. Chiu

2019 ◽  
Vol 5 (8) ◽  
pp. eaaw5019 ◽  
Author(s):  
Rafaella Georgiou ◽  
Pierre Gueriau ◽  
Christoph J. Sahle ◽  
Sylvain Bernard ◽  
Alessandro Mirone ◽  
...  

The in situ two-dimensional (2D) and 3D imaging of the chemical speciation of organic fossils is an unsolved problem in paleontology and cultural heritage. Here, we use x-ray Raman scattering (XRS)–based imaging at the carbon K-edge to form 2D and 3D images of the carbon chemistry in two exceptionally preserved specimens, a fossil plant dating back from the Carboniferous and an ancient insect entrapped in 53-million-year-old amber. The 2D XRS imaging of the plant fossil reveals a homogeneous chemical composition with micrometric “pockets” of preservation, likely inherited from its geological history. The 3D XRS imaging of the insect cuticle displays an exceptionally well preserved remaining chemical signature typical of polysaccharides such as chitin around a largely hollowed-out inclusion. Our results open up new perspectives for in situ chemical speciation imaging of fossilized organic materials, with the potential to enhance our understanding of organic specimens and their paleobiology.


2020 ◽  
Vol 91 (9) ◽  
pp. 093703
Author(s):  
Kenji Ohta ◽  
Tatsuya Wakamatsu ◽  
Manabu Kodama ◽  
Katsuyuki Kawamura ◽  
Shuichiro Hirai

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