Two-Stage Synthesis of Structured Microsystems Based on Zinc-Oxide Nanorods by Ultrasonic Spray Pyrolysis and the Low-Temperature Hydrothermal Method

2020 ◽  
Vol 54 (11) ◽  
pp. 1496-1502
Author(s):  
A. A. Ryabko ◽  
A. I. Maximov ◽  
V. N. Verbitskii ◽  
V. S. Levitskii ◽  
V. A. Moshnikov ◽  
...  
Author(s):  
А.А. Рябко ◽  
А.И. Максимов ◽  
В.Н. Вербицкий ◽  
В.С. Левицкий ◽  
В.А. Мошников ◽  
...  

The features of a two-stage synthesis of structured microsystems based on zinc oxide nanorods using ultrasonic spray pyrolysis and a low-temperature hydrothermal method with suppression of nucleation in the bulk of the solution are presented. It is shown that the use of two-stage synthesis provides control over the size and aspect ratio of nanorods. It is proposed to control the concentration of intrinsic surface defects by measuring the photocurrent with irradiation through narrow-band interference light filters.


2011 ◽  
Vol 20 (3) ◽  
pp. 037306 ◽  
Author(s):  
Bao-Chen Jiao ◽  
Xiao-Dan Zhang ◽  
Chang-Chun Wei ◽  
Jian Sun ◽  
Jian Ni ◽  
...  

2009 ◽  
Vol 206 (1) ◽  
pp. 106-115 ◽  
Author(s):  
Khedidja Bouzid ◽  
Abdelkader Djelloul ◽  
Noureddine Bouzid ◽  
Jamal Bougdira

Coatings ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1001
Author(s):  
Shih-Chen Shi ◽  
Po-Wei Huang ◽  
Jason Hsiao-Chun Yang

Zinc oxide (ZnO) coatings have various unique properties and are often used in applications such as transparent conductive films in photovoltaic systems. This study developed an atmospheric-pressure microplasma-enhanced ultrasonic spray pyrolysis system, which can prepare large-area ZnO coatings at low temperatures under atmospheric-pressure conditions. The addition of an atmospheric-pressure microplasma-assisted process helped improve the preparation of ZnO coatings under atmospheric conditions, compared to using a conventional ultrasonic spray pyrolysis process, effectively reducing the preparation temperature to 350 °C. A program-controlled three-axis platform demonstrated its potential for the large-scale synthesis of ZnO coatings. The X-ray diffraction results showed that the ZnO coatings prepared by ultrasonic spray pyrolysis exhibited (002) preferred growth orientation and had a visible-light penetration rate of more than 80%. After vacuum treatment, the ZnO reached a 1.0 × 10−3 Ωcm resistivity and a transmittance of 82%. The tribology behavior of ZnO showed that the vacuum-annealed coating had a low degree of wear and a low coefficient of friction as the uniformly distributed and dense coating increased its load capacity.


Sign in / Sign up

Export Citation Format

Share Document