RECOVERY IRON FROM A COPPER FLOTATION TAILING BY NAOH MELTING AND ACID LEACHING PROCESSING

2016 ◽  
Author(s):  
Liangmou Yu
Keyword(s):  
Acid Leaching ◽  
Flotation Tailing ◽  
Copper Flotation

scholarly journals Designing Paste Thickeners for Copper Flotation Tailings, Using Bed depth Scale-up Factor

2018 ◽  
Vol 2 (1) ◽  
Author(s):  
Majid Unesi ◽  
Mohammad Noaparast ◽  
Sied Ziaedin Shafaei ◽  
Esmaeil Jorjani ◽  
Mahdi Yaghobi Moghaddam ◽  
...  
Keyword(s):  
Unit Area ◽  
Scale Up ◽  
Water Recovery ◽  
Copper Tailings ◽  
Flotation Tailings ◽  
Flotation Tailing ◽  
Depth Scale ◽  
Copper Mines ◽  
Influential Parameters ◽  
Copper Flotation

 The paste thickener could increase the water recovery and reduce the environmental impacts in tailings dam. The present work aimed to find the appropriate scale-up factor for bed depth to design paste thickener for copper tailings, using a lab glass cylinder and an operating pilot column. The thickening tests were carried out on the flotation tailing samples obtained from the Sarcheshmeh and Miduk copper mines located in Iran. Based on the industrial conditions, the values of influential parameters for paste thickener used in these experiments were pH=11 and feed solid=10 %. Flocculant type was NF43U and used as 25g/t with dosage of 0.25 gt. The unit area of Sarcheshmeh and Miduk paste thickeners were designed as 0.057 and 0.047m2/t/day, respectively. Based on the dry feed rates to each paste thickener as 7920 and 4320 t/day, the thickener's diameters were determined as 23.9 and 16.1 meters which are similar to the actual thickener’s diameters (24 and 16 meters), respectively. In addition to unit area, the bed depth is also important in the paste thickeners design. Hence, the ratio of industrial to lab unit bed volume for Sarcheshmeh paste thickener was obtained 75 which was equal to the ratio of industrial to lab bed depth (bed depth scale-up factor exclusively for copper flotation tailings). This procedure was validated by using the Miduk sample. The bed depth in the paste thickeners was determined as 7.5 meters, by using the bed depth scale-up factor which was comparable to the actual bed depth (8 meters). This research confirmed that the bed depth scale-up factor is able to correctly determine the bed depth of industrial paste thickeners for copper tailings. 

scholarly journals Recovery of ZnO from lead-zinc flotation tailings by hydrometallurgical processes: XRD, SEM, and AFM studies

2020 ◽  
Vol 56 (1) ◽  
pp. 23-35
Author(s):  
K.T. Perek ◽  
B. Benli ◽  
C. Arslan ◽  
F. Arslan
Keyword(s):  
Cross Sections ◽  
Acid Leaching ◽  
Zinc Hydroxide ◽  
High Iron Content ◽  
Zinc Recovery ◽  
Flotation Tailings ◽  
H2so4 Concentration ◽  
Flotation Tailing ◽  
Iron And Zinc ◽  
Lead Zinc

The hydrometallurgical route of zinc hydroxide and synthesis of nanocrystalline ZnO is a particularly attractive method to recover oxidized lead and zinc from lead-zinc flotation tailings. In Turkey, lead-zinc complex/mixed ores along with high iron content are not suitable for conventional mineral processing methods and need hydrometallurgical treatments. Therefore, the control of iron during zinc processes is really important. In this study, hydrometallurgical process route for zinc recovery from Pb-Zn flotation tailings was investigated by considering the effects of H2SO4 concentration, leaching and roasting temperatures on the zinc dissolution considering the Eh-pH variations. The iron and zinc products were also individually examined by X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM) images in order to compare before and after leaching, precipitation and roasting steps. 83.1% Zn and 91.6% Cd leaching efficiencies were obtained from Pb-Zn flotation tailing particles with the size range of 50-110 nm from AFM image cross-sections, while lead and iron were not dissolved. Elemental sulfur started to form and produce a layer around the particles or a partially agglomerated particle in the size of 170 nm during the sulphuric acid leaching. However, majority of the particles was determined to be less than 20 microns, and AFM images showed that the size reduction between the leached and unleached particles was over 50%. Selective precipitations of iron and zinc in the form of hydroxide were performed in high recovery efficiencies of 90.1% and 99%, respectively. After the heat treatment, nanocrystalline zincite clusters of 96.6% purity were produced in the ZnO mineral form and nearly 13 nm in size. Zinc can be successfully recovered and a flotation tailings ore can be a good candidate for the production of high technology needs of nanocrystalline ZnO nanoparticles.

scholarly journals Designing Paste Thickeners for Copper Flotation Tailings, Using Bed depth Scale-up Factor

2018 ◽  
Vol 1 (1) ◽  
Author(s):  
Majid Unesi ◽  
Mohammad Noaparast ◽  
Sied Ziaedin Shafaei ◽  
Esmaeil Jorjani ◽  
Mahdi Yaghobi Moghaddam ◽  
...  
Keyword(s):  
Unit Area ◽  
Scale Up ◽  
Water Recovery ◽  
Copper Tailings ◽  
Flotation Tailings ◽  
Flotation Tailing ◽  
Depth Scale ◽  
Copper Mines ◽  
Influential Parameters ◽  
Copper Flotation

 The paste thickener could increase the water recovery and reduce the environmental impacts in tailings dam. The present work aimed to find the appropriate scale-up factor for bed depth to design paste thickener for copper tailings, using a lab glass cylinder and an operating pilot column. The thickening tests were carried out on the flotation tailing samples obtained from the Sarcheshmeh and Miduk copper mines located in Iran. Based on the industrial conditions, the values of influential parameters for paste thickener used in these experiments were pH=11 and feed solid=10 %. Flocculant type was NF43U and used as 25g/t with dosage of 0.25 gt. The unit area of Sarcheshmeh and Miduk paste thickeners were designed as 0.057 and 0.047m2/t/day, respectively. Based on the dry feed rates to each paste thickener as 7920 and 4320 t/day, the thickener's diameters were determined as 23.9 and 16.1 meters which are similar to the actual thickener’s diameters (24 and 16 meters), respectively. In addition to unit area, the bed depth is also important in the paste thickeners design. Hence, the ratio of industrial to lab unit bed volume for Sarcheshmeh paste thickener was obtained 75 which was equal to the ratio of industrial to lab bed depth (bed depth scale-up factor exclusively for copper flotation tailings). This procedure was validated by using the Miduk sample. The bed depth in the paste thickeners was determined as 7.5 meters, by using the bed depth scale-up factor which was comparable to the actual bed depth (8 meters). This research confirmed that the bed depth scale-up factor is able to correctly determine the bed depth of industrial paste thickeners for copper tailings. 

ACID LEACHING TO INCREASE DETECTION LIMITS IN GAMMA COUNTING UNSUPPORTED PB-210

2016 ◽  
Author(s):  
Adrian Singleton ◽  
◽  
Chloe Isaacs ◽  
Marcus Hill ◽  
Monica Dix ◽  
...  
Keyword(s):  
Acid Leaching ◽  
Detection Limits ◽  
Gamma Counting

scholarly journals Study on Ultrasonically-Enhanced Sulfuric Acid Leaching of Nickel from Nickel-Containing Residue

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 810
Author(s):  
Zhanyong Guo ◽  
Ping Guo ◽  
Guang Su ◽  
Fachuang Li
Keyword(s):  
Sulfuric Acid ◽  
Acid Leaching ◽  
Ultrasonic Waves ◽  
Sulfuric Acid Leaching ◽  
Solid Product ◽  
Leaching Process ◽  
Diffusion Controlled ◽  
Extraction Degree ◽  
Ultrasonic Conditions ◽  
Complex Nickel

In this paper, nickel-containing residue, a typical solid waste produced in the battery production process, was used to study the cavitation characteristics of ultrasonic waves in a liquid–solid reaction. The ultrasonically-enhanced leaching technology for multicomponent and complex nickel-containing residue was studied through systematic ultrasonic-conventional comparative experiments. An ultrasonic leaching kinetics model was established which provided reliable technological guidance and basic theory for the comprehensive utilization of nickel-containing residue. In the study, it was found that ultrasonically-enhanced leaching for 40 min obtained the same result as conventional leaching for 80 min, and the Ni extraction degree reached more than 95%. According to the kinetic fitting of the leaching process, it was found that the sulfuric acid leaching process belonged to the diffusion-controlled model of solid product layers under conventional and ultrasonic conditions, and the activation energy of the reaction was Ea1 = 17.74 kJ/mol and Ea2 = 5.04 kJ/mol, respectively.

scholarly journals Electrocatalysis for Oxygen Reduction Reaction on EDTAFeNa and Melamine co-Derived Self-Supported Fe-N-C Materials

Catalysts ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 623
Author(s):  
Mengfan Shen ◽  
Ziwei Meng ◽  
Tong Xue ◽  
Hongfang Shen ◽  
Xiang-Hui Yan
Keyword(s):  
Oxygen Reduction Reaction ◽  
Oxygen Reduction ◽  
Large Scale ◽  
Acid Leaching ◽  
Reduction Reaction ◽  
Scale Production ◽  
Final Annealing ◽  
High Performing ◽  
Half Wave ◽  
Mesoscopic Structure

To explore high-performing alternatives to platinum-based catalysts is highly desirable for lowering costs and thus promoting fuel cell commercialization. Herein, self-supported Fe-N-C materials were prepared by the pyrolysis of dual precursors including EDTA ferric sodium (EDTAFeNa) and melamine (MA), followed by acid-leaching and final annealing. Towards an oxygen reduction reaction (ORR) in 0.1 M KOH, the as-prepared MA/EDTAFeNa-HT2 delivered onset (Eonset) and half-wave (E1/2) potentials of 0.97 and 0.84 V vs. RHE, respectively, identical with that of a state-of-the-art Pt/C catalyst, accompanied with predominantly a four-electron pathway. The introduction of MA and extension of acid-leaching promoted a positive shift of 50 mV for E1/2 relative to that of only the EDTAFeNa-derived counterpart. It was revealed that the enhancement of ORR activity is attributed to a decrease in magnetic Fe species and increase in pyridinic/quanternary nitrogen content whilst nearly excluding effects of the graphitization degree, variety of crystalline iron species, and mesoscopic structure. The usage of dual precursors exhibited great potential for the large-scale production of inexpensive and efficient Fe-N-C materials.

scholarly journals Recovery of Zinc and Silver from Zinc Acid-Leaching Residues with Reduction of Their Environmental Impact Using a Novel Water Leaching-Flotation Process

Minerals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 586
Author(s):  
Yunpeng Du ◽  
Xiong Tong ◽  
Xian Xie ◽  
Wenjie Zhang ◽  
Hanxu Yang ◽  
...  
Keyword(s):  
Hazardous Waste ◽  
Acid Leaching ◽  
Copper Recovery ◽  
Water Leaching ◽  
Flotation Process ◽  
Metal Levels ◽  
Valuable Metals ◽  
Leaching Experiments ◽  
Zinc Hydrometallurgy ◽  
Poor Stability

Zinc-leaching residue (ZLR) is a strongly acidic hazardous waste; it has poor stability, high heavy metal levels, and releases toxic elements into the environment. ZLR has potential as a valuable resource, because it contains elevated levels of zinc and silver. In this paper, the recovery of zinc (Zn) and silver (Ag) from ZLR wastes from zinc hydrometallurgy workshops using water leaching followed by flotation was studied. During water leaching experiments, the zinc and copper recovery rates were 38% and 61%, respectively. Thereafter, various flotation testing parameters were optimized and included grinding time, reagent dosages, pulp density, flotation time, and type of adjuster. Experimental results demonstrated this flotation method successfully recycled Ag and Zn. A froth product containing more than 9256.41 g/t Ag and 12.26% Zn was produced from the ZLR with approximately 80.32% Ag and 42.88% Zn recoveries. The toxicity characteristic leaching procedure (TCLP) results indicated the water-leaching flotation process not only recycled valuable metals such as zinc and silver in zinc-containing hazardous wastes but lowered the hazardous waste levels to those of general wastes and recycled wastes in an efficient, economical, and environmentally friendly way.

scholarly journals Regeneration of LiFePO4 from spent lithium-ion battery by a facile closed-loop process featuring acid leaching and hydrothermal synthesis

2021 ◽  
Author(s):  
Yifan Song ◽  
Boyi Xie ◽  
Shuya Lei ◽  
Shaole Song ◽  
Wei Sun ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Lithium Ion Battery ◽  
Closed Loop ◽  
Acid Leaching ◽  
Lithium Ion ◽  
Power Battery

As a widely used power battery, the scrapping boom of LiFePO4 (LFP) battery is coming. Both pyrometallurgical repair and hydrometallurgical processes have been applied in the recycling of spent LFP...

Sign in / Sign up

Export Citation Format

Share Document