HIGH PRESSURE ELECTRICAL RESISTIVITY STUDY ON NONLINEAR SINGLE CRYSTAL ZINC THIOUREA CHLORIDE

2007 ◽  
Vol 21 (11) ◽  
pp. 675-678 ◽  
Author(s):  
S. ARIPONNAMMAL ◽  
R. SELVA VENNILA ◽  
S. RADHIKA ◽  
P. M. USHASREE

Zinc thiourea chloride (ZTC) crystals were crystallized by slow evaporation technique. The lattice parameters of the grown crystals were determined by angle dispersive X-ray powder diffraction technique (XRD) and the structure was confirmed. High pressure electrical resistivity study was carried out on this crystal and the results are reported here.

1996 ◽  
Vol 10 (10) ◽  
pp. 459-465
Author(s):  
S. ARIPONNAMMAL ◽  
S. NATARAJAN

Electrical resistivity measurements under pressure and lattice parameter study on SnTe 1–xSx(0.5≤x≤1) are reported here. The structure of these samples is confirmed by the theoretical calculation of X ray intensities using Lazy-Pulverix programme. The electrical resistivity decreases with the increase of pressure and also with the decrease of sulphur concentration. High pressure electrical resistivity study has produced more evidence that the compounds are layered material.


2019 ◽  
Vol 1 (1) ◽  
pp. 42-45
Author(s):  
Tamiloli Devendhiran ◽  
Keerthika Kumarasamy ◽  
Mei–Ching Lin

Single crystals of 2-Aminothiazole 3,5-Dinitrobenzoic acid has been synthesized and good quality optical crystals were grown by slow evaporation technique at room temperature. The crystallinity nature of the grown crystal was confirmed from X-ray diffraction technique. An optical transmittance study was also carried out by UV – Vis spectra. FTIR spectra confirm the presence of functional groups in the grown crystal. The dielectric measurements were carried out in the range of 50Hz to 2MHz. The dielectric constant was seen to increase exponentially at lower frequencies. The microhardness studies were carried out using Vickers hardness indenter. Photoluminescence study shows that maximum emission occurs at 435nm.


RSC Advances ◽  
2016 ◽  
Vol 6 (39) ◽  
pp. 33159-33169 ◽  
Author(s):  
S. Karthigha ◽  
S. Kalainathan ◽  
Fumio Hamada ◽  
Manabu Yamada ◽  
Yoshihiko Kondo

N-Ethyl quinolinium chromophore crystal 2-[2-(4-chloro-phenyl)-vinyl]-1-ethyl-quinolinium iodide (PCLQI) has been successfully grown by the slow evaporation technique.


1993 ◽  
Vol 07 (23) ◽  
pp. 1527-1531 ◽  
Author(s):  
K. JEYABALAN ◽  
C. VENKATESWARAN ◽  
R. ASOKAMANI ◽  
S. NATARAJAN

Synthesis of air-quenched high-T c superconductors Y 0.8 Sr 0.2 Ba 2 Cu 3 O 6+x and Y 0.8 Ba 2.2 Cu 3 O 6+x exhibiting transition temperatures of 90 K and 88 K respectively and the variation of their electrical resistivity at high pressure are reported here. X-ray powder diffraction of the above systems reveal tetragonal structure.


1996 ◽  
Vol 197 (1) ◽  
pp. K1-K4 ◽  
Author(s):  
S. Ariponnammal ◽  
C. Venkateswaran ◽  
S. Natarajan

2004 ◽  
Vol 11 (01) ◽  
pp. 83-86 ◽  
Author(s):  
S. ABOUELHASSAN ◽  
F. SALMAN ◽  
M. ELMANSY ◽  
E. SHEHA

Single crystals of KHCO 3 were grown by the slow evaporation technique of an aqueous solution. Characterization of the sample was done using different techniques such as X-ray diffraction, infrared spectra (IR) and the differential scanning calorimeter (DSC) technique. The analysis of the X-ray diffraction pattern indicated that the sample was a single crystal. The results obtained by IR and DSC indicated the presence of phase transition. From the analysis of DSC, the activation energy of transition was carried out by two methods (Kissinger and Ozawa).


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