MICROSTRUCTURE AND WEAR RESISTANCE OF CHROMIUM CARBIDE COATING IN SITU SYNTHESIZED BY VEB

2014 ◽  
Vol 21 (05) ◽  
pp. 1450065 ◽  
Author(s):  
BINFENG LU ◽  
LIPING LI ◽  
FENGGUI LU ◽  
XINHUA TANG

In this paper, ( Cr , Fe )7 C 3( M 7 C 3)/γ- Fe composite layer has been in situ fabricated on a low carbon steel surface by vacuum electron beam irradiation (VEB). Three kinds of powder mixtures were placed on a low carbon steel substrate, which was then irradiated with electron beam in vacuum condition. The microstructure and wear resistance of the composite layers has been studied by means of optical microscope (OM), X-ray diffraction (XRD), scanning electron microscope (SEM), microhardness tester and tribological tester. The chemical composition of all specimens were carefully analyzed using energy-dispersive X-ray spectroscopy (EDAX) technique. Depending on three different powder mixtures, hypereutectic and hypoeutectic microstructures were obtained on surface composite layers. No pores and cracks were found on the coatings. The amount of carbides formed in the surface composite layer was mainly determined by carbon concentration. The microstructure close to the fusion line was largely primary austenite dendrite. The hardness and wear resistance of the surface composite layer has been greatly improved due to the extensive distribution of carbides.

2021 ◽  
pp. 2150026
Author(s):  
MIN HUANG ◽  
YONG-CHUAN DUAN ◽  
YU WANG ◽  
YI-CHEN CAI ◽  
LIU-YI HU

An aluminized coating for low-carbon steel with good corrosion and wear resistance was first prepared through low-temperature pack aluminization. Then, the low-temperature-aluminized steel substrate was subjected to thermal oxidation in air. The phase composition, surface morphology, roughness, and elemental distribution of the aluminized carbon steel both before and after thermal oxidation were analyzed through X-ray diffraction spectroscopy, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. The corrosion resistance and wear resistance of the original carbon steel substrate, aluminized carbon steel, and oxidized carbon steel were tested. Results showed that nanowires composed of iron oxide and alumina formed in situ on the top layer of the aluminized carbon steel. The corrosion resistance and wear resistance of the low-carbon steel with the nanowire oxide coating were better than those of the original carbon steel and aluminized carbon steel because the in-situ nanowire oxide film improved the density of the aluminized coating.


2021 ◽  
Vol 800 ◽  
pp. 140249
Author(s):  
Juan Macchi ◽  
Steve Gaudez ◽  
Guillaume Geandier ◽  
Julien Teixeira ◽  
Sabine Denis ◽  
...  

2016 ◽  
Vol 849 ◽  
pp. 677-682
Author(s):  
Hao Chen ◽  
Yang Rong Zhang ◽  
Zhu Huang

By plasma jet surface metallurgy, the thick composite coatings reinforced by in-situ TiC were produced on low carbon steel. Composition, microstructures and performance were characterized by scanning electron microscope (SEM), energy dispersive X-ray (EDX), X-ray diffraction (XRD), micro-hardness tester and wear tester. The results showed that the excellent bonding between the coating and the carbon steel substrate was achieved by strong metallurgical interface. The microstructure of the coating is mainly composed of γ-(Fe, Ni) dendrite, M23C6, CrB and in-situ synthesized TiC ceramic particle. Because of the particulate reinforcement, the dispersion strengthening, refinement strengthening, micro-hardness and wear resistant of Fe-based coating can be enhanced.


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3459 ◽  
Author(s):  
Baoming Shi ◽  
Shiming Huang ◽  
Ping Zhu ◽  
Changen Xu ◽  
Tengfei Zhang

In the present study, plasma spray welding was used to prepare an in-situ niobium carbide (NbC) reinforced Ni-based composite coating on the low carbon steel, and the phase composition and the microstructure of the composite coatings were studied. The wear resistance and the wear mechanism of the composite coatings were also researched by the wear tests. The results showed that the main phases of the composite coating were NbC, γ-Ni, Cr23C6, Ni3Si, CrB, Cr5B3, Cr7C3 and FeNi3. A number of fine in-situ NbC particles and numerous chromium carbide particles were distributed in the γ-Ni matrix. The increase in the mass fraction of Nb and NiCr-Cr3C2 could lead to the increase in NbC particles in the composite coatings. Due to the high hardness of NbC and chromium carbides, the micro-hardness and the wear resistance of the composite coatings were advanced. The composite coating with the powder mixtures of 20% (Nb + NiCr-Cr3C2) and 80% NiCrBSi had the highest micro-hardness and the best wear resistance in this study. The average micro-hardness reached the maximum value 1025HV0.5. The volume loss was 39.2 mm3, which was merely 37% of that of the NiCrBSi coating and 6% of that of the substrate under the identical conditions.


2012 ◽  
Vol 538-541 ◽  
pp. 302-305
Author(s):  
Ran Yang Zhang ◽  
Gang Yao Zhao ◽  
Yue Chen

Surface composite layer was fabricated on the cast steel matrix using the evaporative pattern casting (EPC) technology. The pre-coating with WC and Cr-Fe particles as raw reinforcements was reacted with matrix and formed the composite layer. Then, the microstructure and hardness of surface composite layer were investigated by Scanning Electron Microscope (SEM), Olympus Microscope (OM), Energy Dispersive X-ray Spectroscopy (EDAX) and Rockwell Apparatus. The results show that the composite layer can be divided into transitive layer and penetrated layer, and the component analysis shows that the microstructure distribution of the penetrated layer is homogeneous.


2014 ◽  
Vol 1055 ◽  
pp. 73-77
Author(s):  
Xian Ming Sun ◽  
Gui Rong Yang ◽  
Lei Wei ◽  
Yu Lan Liu

The surface composite layer Ni/ZrO2 on the ZG45 cast steel surface was fabricated through vacuum infiltration casting method. This paper researched on the Ni/ZrO2 composite infiltrated layer morphology, hardness and the friction property under fry friction. The results show that the main phase structure of the layer is ZrO2, Cr2B, NiB and FeNi. The macrohardness of the layer is HRC60~64. The micohardness presents gradient change. The maximum hardness appears at subsuface. The 10% ZrO2 composite infiltrated layer wear resistance increases 10 times and 15% ZrO2 composite infiltrated layer increases 22.6 times than ZG45 under the 100N load. The 10% ZrO2 composite infiltrated layer wear resistance increases 8.5 times and 15% ZrO2 composite infiltrated layer increases 21.9 times under 250N load. The wear resistance has greatly improved.


2012 ◽  
Vol 729 ◽  
pp. 320-325
Author(s):  
Viktória Janó ◽  
Gábor Buza

Composites of ceramic particle reinforcement (such as alumina) have potential for high temperature structural applications. In contrast to conventional processing methods (e.g. mechanical alloying), in situ processing techniques can be inexpensive and can also lead to unique microstructures, such as very fine dispersions of the reinforcements or interconnecting phases. The feasibility of processing Fe/Al2O3 composites layer by an in situ displacement reaction between Fe2O3 and Al by using laser beam pre-experiments were carried out and the results are presented in this paper.


Sign in / Sign up

Export Citation Format

Share Document