Synthesis of reduced graphene oxide paper for EMI shielding by a multi-step process

2020 ◽  
Vol 13 (05) ◽  
pp. 2051024
Author(s):  
Yangyang Lin ◽  
Genliang Hou ◽  
Song Bi ◽  
Xunjia Su ◽  
Hao Li

A multi-step reduction process was developed to produce reduced graphene oxide (rGO) paper for electromagnetic interference (EMI) shielding. First step reduction was achieved by hydroiodic acid to remove most of the oxygen-containing functional groups, and sodium borohydride was used in the second step reduction to reduce carbonyl group which is the most difficult functional group to remove. In the last step reduction, hydroiodic acid was used as reducing agent again to remove the remaining oxygen-containing functional groups. The results show that this method can greatly improve the conductivity and EMI shielding performance of rGO paper. The resulting rGO paper with a C/O ratio of 19.38 and a thickness of 9.1[Formula: see text][Formula: see text]m exhibited high conductivity of 1084[Formula: see text]S/cm and excellent average EMI shielding efficiency of 45.84[Formula: see text]dB in the X-band, better than that reduction by other chemical methods.

2021 ◽  
pp. 108645
Author(s):  
Jiaying Li ◽  
Wei Li ◽  
Xingyu Tong ◽  
Shaowei Lu ◽  
Baichen Wang ◽  
...  

2015 ◽  
Vol 17 (3) ◽  
pp. 1610-1618 ◽  
Author(s):  
Meenakshi Verma ◽  
Avanish Pratap Singh ◽  
Pradeep Sambyal ◽  
Bhanu Pratap Singh ◽  
S. K. Dhawan ◽  
...  

Barium ferrite decorated reduced graphene oxide nanocomposite has been synthesized for absorption dominated enhanced EMI shielding.


Nanomaterials ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 621 ◽  
Author(s):  
Yadav ◽  
Kuřitka ◽  
Vilčáková ◽  
Machovský ◽  
Škoda ◽  
...  

Herein, we presented electromagnetic interference shielding characteristics of NiFe2O4 nanoparticles—in-situ thermally-reduced graphene oxide (RGO)—polypropylene nanocomposites with the variation of reduced graphene oxide content. The structural, morphological, magnetic, and electromagnetic parameters and mechanical characteristics of fabricated nanocomposites were investigated and studied in detail. The controllable composition of NiFe2O4-RGO-Polypropylene nanocomposites exhibited electromagnetic interference (EMI) shielding effectiveness (SE) with a value of 29.4 dB at a thickness of 2 mm. The enhanced EMI shielding properties of nanocomposites with the increase of RGO content could be assigned to enhanced attenuation ability, high conductivity, dipole and interfacial polarization, eddy current loss, and natural resonance. The fabricated lightweight NiFe2O4-RGO-Polypropylene nanocomposites have potential as a high performance electromagnetic interference shielding nanocomposite.


RSC Advances ◽  
2015 ◽  
Vol 5 (66) ◽  
pp. 53604-53610 ◽  
Author(s):  
Labrini Sygellou ◽  
George Viskadouros ◽  
Costas Petridis ◽  
Emmanuel Kymakis ◽  
Costas Galiotis ◽  
...  

The effect of the reduction process and oxygen-contained functional groups on the field emission performance of reduced graphene oxide cathodes.


Polymers ◽  
2021 ◽  
Vol 13 (19) ◽  
pp. 3316
Author(s):  
Asim Mansha ◽  
Khadija Zubair ◽  
Zulfiqar Ahmad Rehan ◽  
H. M. Fayzan Shakir ◽  
Talha Javed ◽  
...  

The co-precipitation and in situ modified Hummers’ method was used to synthesize Nickel Spinal Ferrites (NiFe) nanoparticles and NiFe coated with Thermally Reduced Graphene Oxide (TRGO) (NiFe-TRGO) nanoparticles, respectively. By using polyvinyl chloride (PVC), tetrahydrofuran (THF), and NiFe-TRGO, the nanocomposite film was synthesized using the solution casting technique with a thickness of 0.12–0.13 mm. Improved electromagnetic interference shielding efficiency was obtained in the 0.1–20 GHz frequency range. The initial assessment was done through XRD for the confirmation of the successful fabrication of nanoparticles and DC conductivity. The microstructure was analyzed with scanning electron microscopy. The EMI shielding was observed by incorporating a filler amount varying from 5 wt.% to 40 wt.% in three different frequency regions: microwave region (0.1 to 20 GHz), near-infrared (NIR) (700–2500 nm), and ultraviolet (UV) (200–400 nm). A maximum attenuation of 65 dB was observed with a 40% concentration of NiFe-TRGO in nanocomposite film.


2015 ◽  
Vol 3 (38) ◽  
pp. 9802-9810 ◽  
Author(s):  
Faisal Shahzad ◽  
Pradip Kumar ◽  
Seunggun Yu ◽  
Seunghwan Lee ◽  
Yoon-Hyun Kim ◽  
...  

Herein, for the first time, we demonstrate that a laminated structure of sulfur-doped reduced graphene oxide (SrGO) provides significant potential for electromagnetic interference shielding applications.


Nanomaterials ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1196 ◽  
Author(s):  
Francisco Mederos-Henry ◽  
Julien Mahin ◽  
Benoit P. Pichon ◽  
Marinela M. Dîrtu ◽  
Yann Garcia ◽  
...  

Electronic systems and telecommunication devices based on low-power microwaves, ranging from 2 to 40 GHz, have massively developed in the last decades. Their extensive use has contributed to the emergence of diverse electromagnetic interference (EMI) phenomena. Consequently, EMI shielding has become a ubiquitous necessity and, in certain countries, a legal requirement. Broadband absorption is considered the only convincing EMI shielding solution when the complete disappearance of the unwanted microwave is required. In this study, a new type of microwave absorber materials (MAMs) based on reduced graphene oxide (rGO) decorated with zero-valent Fe@γ-Fe2O3 and Fe/Co/Ni carbon-protected alloy nanoparticles (NPs) were synthesized using the Pechini sol-gel method. Synthetic parameters were varied to determine their influence on the deposited NPs size and spatial distribution. The deposited superparamagnetic nanoparticles were found to induce a ferromagnetic resonance (FMR) absorption process in all cases. Furthermore, a direct relationship between the nanocomposites’ natural FMR frequency and their composition-dependent saturation magnetization (Ms) was established. Finally, the microwave absorption efficiency (0.4 MHz to 20 GHz) of these new materials was found to range from 60% to 100%, depending on the nature of the metallic particles grafted onto rGO.


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