scholarly journals Electrical Characterization of Sol-Gel Derived TiO2Film on c-Si Substrate by Admittance Measurement

2014 ◽  
Vol 2014 ◽  
pp. 1-5
Author(s):  
Ayşe Evrim Saatci ◽  
Orhan Özdemir

Transport and storage properties of sol-gel synthesized, namely, dip coating technique, titanium dioxide (TiO2) thin film over crystalline silicon (c-Si), has been investigated by means of current-voltage (I-V) and admittance analysis within different ambient. Considering the work function of anatase TiO2film, determined by both FTIR and TG/DTA analysis, silver (Ag) as front metal electrode was chosen to hinder a barrier for charge carriers. Electrical analysis implied that Ag/TiO2/c-Si structure was actually constituted by Ag/TiO2/native silicon dioxide (SiO2)/c-Si [SIS] structure, in which SiO2layer was identified by FTIR analysis. Consequently, the electrical features of the film were interpreted in terms of SIS diode that is capable of explaining C-V features.

2015 ◽  
Vol 1109 ◽  
pp. 148-152
Author(s):  
A.K.M. Muaz ◽  
U. Hashim ◽  
Sharipah Nadzirah ◽  
M. Wesam Al-Mufti ◽  
Fatimah Ibrahim ◽  
...  

In the present research, nanocrystalline TiO2thin films have been prepared via a sol-gel method using Ti {OCH(CH3)2}4act as a precursor. The morphological effect of sets of as-deposited and annealed samples (100, 300, 500 and 700°C for 1 hour) and thickness variation on the structural properties were investigated by Atomic Force Microscopy (AFM) measurements. The observation showed that the size of grain increases with film thickness, indicating that the size of the particles in the films can be effectively controlled by changing the temperature of thermal treatment. AFM topology images of the as-deposited and annealed TiO2films at 100 and 300°C indicates the films are rather smooth, compact, bulky, not uniform and column-like structure. TiO2thin films annealed at 500 and 700°C showed homogenous morphology surface with regular size of spherical particles.


2008 ◽  
Vol 517 (3) ◽  
pp. 1077-1080 ◽  
Author(s):  
R.E. Marotti ◽  
C.D. Bojorge ◽  
E. Broitman ◽  
H.R. Cánepa ◽  
J.A. Badán ◽  
...  

Author(s):  
Yuk L. Tsang ◽  
Alex VanVianen ◽  
Xiang D. Wang ◽  
N. David Theodore

Abstract In this paper, we report a device model that has successfully described the characteristics of an anomalous CMOS NFET and led to the identification of a non-visual defect. The model was based on detailed electrical characterization of a transistor exhibiting a threshold voltage (Vt) of about 120mv lower than normal and also exhibiting source to drain leakage. Using a simple graphical simulation, we predicted that the anomalous device was a transistor in parallel with a resistor. It was proposed that the resistor was due to a counter doping defect. This was confirmed using Scanning Capacitance Microscopy (SCM). The dopant defect was shown by TEM imaging to be caused by a crystalline silicon dislocation.


Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1554
Author(s):  
Justinas Januskevicius ◽  
Zivile Stankeviciute ◽  
Dalis Baltrunas ◽  
Kęstutis Mažeika ◽  
Aldona Beganskiene ◽  
...  

In this study, an aqueous sol-gel synthesis method and subsequent dip-coating technique were applied for the preparation of yttrium iron garnet (YIG), yttrium iron perovskite (YIP), and terbium iron perovskite (TIP) bulk and thin films. The monophasic highly crystalline different iron ferrite powders have been synthesized using this simple aqueous sol-gel process displaying the suitability of the method. In the next step, the same sol-gel solution was used for the fabrication of coatings on monocrystalline silicon (100) using a dip-coating procedure. This resulted, likely due to substrate surface influence, in all coatings having mixed phases of both garnet and perovskite. Thermogravimetric (TG) analysis of the precursor gels was carried out. All the samples were investigated by X-ray powder diffraction (XRD) analysis. The coatings were also investigated by scanning electron microscopy (SEM), atomic force microscopy (AFM) and Mössbauer spectroscopy. Magnetic measurements were also carried out.


Coatings ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 243
Author(s):  
Diana Horkavcová ◽  
Quentin Doubet ◽  
Gisèle Laure Lecomte-Nana ◽  
Eva Jablonská ◽  
Aleš Helebrant

The sol-gel method provides a wide variety of applications in the medical field. One of these applications is the formation of coatings on the metal implants. The coatings containing specific additive can enhance or improve the existing surface properties of the substrate. In this work, titania sol-gel coatings were doped with two forms of silver (AgNO3, Ag3PO4) and synthetic hydroxyapatite and applied on the titanium samples by dip-coating technique. After drying and slow firing, all coatings were characterized with scanning electron microscopy. Thin coatings were successfully prepared with excellent adhesion to the substrate (measured by ASTM D 3359-2), despite cracks. Coatings containing silver and hydroxyapatite demonstrated a 100% antibacterial effect against Escherichia coli after 24 h. The bioactivity of the coatings containing hydroxyapatite tested in modified simulated body fluid under static-dynamic conditions was confirmed by bone-like hydroxyapatite precipitation. To better understand the interaction of the coatings with simulated body fluid (SBF), changes of Ca2+ and (PO4)3− ions concentrations and pH values were studied.


2019 ◽  
Vol 49 (3) ◽  
pp. 1993-2002
Author(s):  
Manuel A. Hernández-Ochoa ◽  
Humberto Arizpe-Chávez ◽  
Rafael Ramírez-Bon ◽  
Alain Pérez-Rodríguez ◽  
Manuel Cortez-Valadez ◽  
...  

2005 ◽  
Vol 38 (1) ◽  
pp. 211-216 ◽  
Author(s):  
Pang-Hung Liu ◽  
Kuei-Jung Chao ◽  
Xing-Jian Guo ◽  
Kuo-Ying Huang ◽  
Yen-Ru Lee ◽  
...  

A continuous silica film with well aligned mesochannels parallel to the Si(001) surface was found to be formed through sol–gel dip-coating of a silica precursor with nonionic ethylene oxide surfactant. Two two-dimensional mesoporous structures in centered and non-centered rectangular symmetries and with the short axes of elongated ellipsoidal pores normal to the surface were observed by X-ray and electron diffraction. Detailed transmission electron microscopy investigations were employed to view the direction dependence of the channel or pore packing in the continuous film.


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