scholarly journals Physicochemical Properties of Calcium Phosphate Based Coating on Gutta-Percha Root Canal Filling

2015 ◽  
Vol 2015 ◽  
pp. 1-5 ◽  
Author(s):  
Afaf Al-Haddad ◽  
Muralithran G. Kutty ◽  
Noor Hayaty Abu Kasim ◽  
Zeti Adura Che Ab Aziz
Keyword(s):  
Calcium Phosphate ◽  
Root Canal ◽  
Calcium Phosphate Coating ◽  
Filling Material ◽  
Cohesive Failure ◽  
Root Canal Filling ◽  
Gutta Percha ◽  
Sealing Ability ◽  
Coating Method ◽  
Root Dentin

Dental Gutta-percha (GP) is a polymer based standard root canal filling material that has been widely used in dentistry. However, it has an inadequate sealing ability and adhesion to root dentin. The aim of this study is to coat GP with a bioactive material to enhance its sealing ability and adhesion to the root sealer and subsequently to the root dentin. The choice of coating method is limited by the nature of GP as it requires a technique that is not governed by high temperatures or uses organic solvents. In this study, biomimetic coating technique using 1.5 Tas-simulated body fluids (SBF) was employed to coat the treated GP cones. The coated samples were characterized using Fourier transform infrared spectroscopy (FTIR), X-ray Diffraction (XRD), and field emission scanning electron microscope (FESEM). The presence of hydroxyl, carbonate, and phosphate groups was detected by FTIR while the formation of hydroxyapatite (HA)/calcium phosphate was confirmed with XRD. FESEM revealed uniform, thin, and crystalline HA calcium phosphate coating. The adhesion of the coating to the GP substrate was assessed with microscratch technique. It was viable with cohesive failure mode. In conclusion, Tas-SBF is able to coat pretreated GP cones with a crystalline apatitic calcium phosphate layer.

scholarly journals Sealing Ability of AH Plus and GuttaFlow Bioseal

2020 ◽  
Vol 2020 ◽  
pp. 1-8
Author(s):  
Soo-Hyuk Lee ◽  
Soram Oh ◽  
Adel Saeed Al-Ghamdi ◽  
Ayman Omar Mandorah ◽  
Kee-Yeon Kum ◽  
...  
Keyword(s):  
Fluid Flow ◽  
Root Canal ◽  
Glass Ceramics ◽  
Filling Material ◽  
Root Canal Filling ◽  
Measuring Device ◽  
Gutta Percha ◽  
Sealing Ability ◽  
Ah Plus ◽  
The Mean

The objective of root canal obturation is to achieve a fluid-tight seal. Recently, GuttaFlow bioseal (GB), a root canal sealer composed of polydimethylsiloxane, gutta-percha particles, and bioactive glass ceramics, has been developed, to enhance the sealing ability of root canal filling material. The objective of this study was to assess the sealing ability of GB using a subnanoliter-scaled fluid-flow measuring device and to compare with that of AH Plus (AH). The fluid flow in root canal-filled teeth using either gutta-percha cone (GP) with AH (GAR; n = 10) or GP with GB (GBR; n = 10) and in GP inserted in AH blocks (GA; n = 10) or GP inserted in GB blocks (GB; n = 10) was measured. In addition, fluid flow in sealer blocks of AH (A; n = 10) and GB (B; n = 10), which served as negative controls, was measured. Root canal-filled teeth using GP without any sealer (GR) acted as positive controls (n = 10). The leakage was obtained by calculating the volume of moved water by time (s), after stabilization of the fluid flow was achieved. Statistical analysis was performed using the Kruskal–Wallis test and Mann–Whitney U-test with Bonferroni correction. A p value less than 0.00238 (0.05/21) was considered significantly different. The mean leakages (nL/s) in the groups are as follows: GAR, 0.0958 ± 0.0543; GBR, 0.0223 ± 0.0246; GA, 0.0644 ± 0.0803; GB, 0.0267 ± 0.0182; A, 0.0055 ± 0.0057; B, 0.0052 ± 0.005; and GR, 0.2892 ± 0.3018. The mean leakage in the GBR group was lower than that in the GAR group (p = 0.001), while the mean leakages in the GA and GB groups were not significantly different. GuttaFlow bioseal can be useful in single-cone obturation technique.

scholarly journals Comparison of apical sealing ability of resected mineral trioxide aggregate, gutta-percha and a resin-based root canal filling material (resilon)

2011 ◽  
Vol 10 (51) ◽  
pp. 10516-10519
Author(s):  
Froughreyhani Mohammad ◽  
Salem Milani Amin ◽  
Rahimi Saeed ◽  
Shakouie Sahar ◽  
Fateh Somaieh
Keyword(s):  
Root Canal ◽  
Mineral Trioxide Aggregate ◽  
Filling Material ◽  
Root Canal Filling ◽  
Gutta Percha ◽  
Sealing Ability

scholarly journals Analysis of sealing ability of root canal sealers using scanning electronic microscopy technique

2010 ◽  
Vol 138 (11-12) ◽  
pp. 694-698 ◽  
Author(s):  
Mirjana Vujaskovic ◽  
Nevenka Teodorovic
Keyword(s):  
Root Canal ◽  
Filling Material ◽  
Scanning Electronic Microscopy ◽  
Electronic Microscopy ◽  
Good Adhesion ◽  
Root Canal Filling ◽  
Adhesion Properties ◽  
Microscopy Technique ◽  
Gutta Percha ◽  
Sealing Ability

Introduction. An ideal endodontic sealer should adhere firmly both to dentin and to gutta-percha. Objective. The aim of this study was to evaluate the adhesion of the root canal filling to dentin and gutta-percha using scanning electronic microscopy (SEM). Methods. The sealing ability of endodontic sealers to dentinal walls of the root canal was assessed in recently extracted human single canal premolars. Twenty teeth were prepared using the crown-down technique and irrigated with 3% NaOCl. A total of 20 samples were divided into two groups. The root canals were obturated using Ketac-Endo Aplicap and GutaFlow. The sealing ability and adhesion properties at the sealer-dentin interface were studied using SEM and the results were rated from 1 to 3; extremely good adhesion (rated 1), good adhesion (rated 2) and a relatively good adhesion (rated 3). Results. The results showed extremely good adhesion on Ketac-Endo and GuttaFlow dentin interface. GuttaFlow has strong adhesion (rated 1) to gutta-percha in comparison with Ketac-Endo to gutta-percha interface (rated 2). Conclusion. New GuttaFlow filling material has a strong sealing ability and excellent adhesion to dentinal walls and gutta-percha cones. Ketac-Endo showed excellent bond to dentin with a slightly weaker adhesion capacity to the gutta-percha cones in comparison to GuttaFlow.

scholarly journals Push-Out Bond Strength of Experimental Apatite Calcium Phosphate Based Coated Gutta-Percha

2018 ◽  
Vol 2018 ◽  
pp. 1-5 ◽  
Author(s):  
Afaf Y. Al-Haddad ◽  
Muralithran G. Kutty ◽  
Zeti Adura Che Ab Aziz
Keyword(s):  
Calcium Phosphate ◽  
Bond Strength ◽  
Failure Mode ◽  
Failure Modes ◽  
Test Machine ◽  
Filling Material ◽  
Cohesive Failure ◽  
Root Canal Filling ◽  
Gutta Percha ◽  
Push Out

Objectives. To evaluate the push-out bond strength of experimental apatite calcium phosphate coated gutta-percha (HAGP) compared to different commercially available coated gutta-percha root obturation points. Methods. Extracted teeth were selected and instrumented using ProTaper rotary files. The canals were assigned into five equal groups and obturated using matching single cone technique as follows: EndoREZ cones and EndoREZ sealer, Bioceramic Endosequence gutta-percha (BCGP) with Endosequence BC sealer, Active GP with Endosequence BC sealer (ActiV GP), conventional GP with Endosequence BC sealer, and HAGP with Endosequence BC sealer. Each root was sectioned transversally at the thickness of 1±0.1 mm to obtain 5 sections (n=25 per group). The specimens were subjected to push-out test using a Universal Test Machine at a loading speed of 0.5 mm/ min. Failure modes after push-out test was examined under stereomicroscope and the push-out data were analyzed using ANOVA and the post hoc Dunnett T3 test (p = 0.05). Results. The highest mean bond strength was yielded by HAGP followed by BCGP, ActiV GP, conventional GP, and EndoREZ. There were significant differences between EndoREZ and all other groups (p<0.001). The prominent failure mode of HAGP was mixed mode, whereas EndoREZ exhibited adhesive failure mode. Conventional GP, ActiV GP, and BCGP showed cohesive failure mode. Conclusion. HAGP showed promising results to be used as root canal filling material in combination with bioceramic sealer.

Injectable calcium phosphate and styrene–butadiene polymer-based root canal filling material

2021 ◽  
Vol 15 (1) ◽  
pp. 19-26
Author(s):  
Hala B. Kaka ◽  
Raid F. Salman
Keyword(s):  
Calcium Phosphate ◽  
Root Canal ◽  
Setting Time ◽  
Molar Ratio ◽  
Styrene Butadiene Rubber ◽  
Filling Material ◽  
Butadiene Rubber ◽  
Root Canal Filling ◽  
Phosphate Powder ◽  
Styrene Butadiene

Abstract Background Three-dimensional obturation of the root canal system is mandatory for a successful root canal treatment. Using a filling material with optimal properties may enable the root canal to be sealed well and therefore obtain the desired obturation. Objective To develop a new injectable paste endodontic filling material using calcium phosphate powder and a styrene–butadiene emulsion polymer. Methods The powder phase comprised an equivalent molar ratio of tetracalcium phosphate, anhydrous dicalcium phosphate, bismuth oxide, and calcium chloride. The liquid phase comprised a styrene–butadiene rubber emulsion in distilled water. The powder and the liquid were mixed to achieve a paste consistency. The paste was subjected to various tests including flow, setting time, dimensional change, solubility, and radiopacity to indicate its suitability as a root canal filling material. All these tests were conducted according to the American National Standards Institute–American Dental Association for endodontic sealing materials. After passing these tests, the paste was submitted to an injectability test. Results The material showed acceptable flowability with 19.1 ± 1.3 min setting time and 0.61 ± 0.16% shrinkage after 30 days of storage. We found the highest solubility at 24 h (6.62 ± 0.58%), then the solubility decreased to 1.09 ± 0.08% within 3 days. The material was more radiopaque than a 3 mm step on an aluminum wedge. Furthermore, the material showed good injectability of 93.67 ± 1.80%. Conclusions The calcium phosphate powder in styrene–butadiene emulsion met basic requirements for a root canal filling material with promising properties.

scholarly journals Healing of a tooth with an overinstrumented apex, extensive transportation and periapical lesion using a 5 mm calcium hydroxide apical plug: an 8-year follow-up report

2012 ◽  
Vol 23 (5) ◽  
pp. 608-611
Author(s):  
Ronaldo Araújo Souza ◽  
Yara T. Corrêa Silva-Sousa ◽  
Suely Colombo ◽  
Maurício Lago ◽  
Marco Antonio Hungaro Duarte ◽  
...  
Keyword(s):  
Calcium Hydroxide ◽  
Root Canal ◽  
Apical Periodontitis ◽  
Filling Material ◽  
Root Canal Filling ◽  
Apical Constriction ◽  
Gutta Percha ◽  
Open Apices ◽  
Canal Transportation

Besides the risk of filling material extrusion throughout the apex, a satisfactory apical seal can be difficult to achieve in canals with open apices or iatrogenic enlargements of the apical constriction. These situations pose a challenge to root canal filling. This paper describes the root canal filling of a maxillary right canine with an overinstrumented apex, complete loss of the apical stop, extensive canal transportation and apical periodontitis. A 5 mm calcium hydroxide apical plug was placed before root canal filling. The plug was made by soaking paper points with saline, dipping the points in calcium hydroxide powder and then applying it to the apex several times, until a consistent apical plug was obtained. The canal was then irrigated with saline in order to remove any residual calcium hydroxide from the root canal walls, dried with paper points and obturated with an inverted #80 gutta-percha cone and zinc oxide-eugenol based sealer by the lateral condensation technique. An 8-year radiographic follow-up showed formation of mineralized tissue sealing the apical foramen, apical remodeling and no signs of apical periodontitis.

Coronal Leakage of Teeth Root-Filled With Gutta-Percha or Resilon Root Canal Filling Material

2006 ◽  
Vol 32 (9) ◽  
pp. 879-881 ◽  
Author(s):  
Etienne Pitout ◽  
Theunis Gerhardus Oberholzer ◽  
Elaine Blignaut ◽  
Julitha Molepo
Keyword(s):  
Root Canal ◽  
Filling Material ◽  
Root Canal Filling ◽  
Gutta Percha

scholarly journals Effect of a sonic device on bonding of fiberglass posts to root canals

2018 ◽  
Vol 17 ◽  
pp. e18924
Author(s):  
Marina de Almeida Salim ◽  
Thais Mageste Duque ◽  
Heloisa Carla Dell Santo Gusman ◽  
Carolina Oliveira de Lima ◽  
Brenda Paula Figueiredo de Almeida Gomes ◽  
...  
Keyword(s):  
Root Canal ◽  
Adhesive System ◽  
Resin Cement ◽  
Root Canal Filling ◽  
Root Canals ◽  
Gutta Percha ◽  
Ah Plus ◽  
Root Dentin ◽  
Post Hoc ◽  
Adhesive Cement

Aim: This study evaluated the effect of a sonic device on the bonding of fiberglass posts cemented with a self-etching adhesive combined with conventional cement or a self-adhesive cement to root dentin. Methods: Forty single-rooted bovine incisors were endodontically prepared using a step-back technique. Gutta-percha and AH Plus sealer were used for root canal filling, combined with a thermoplasticization technique. After 1 week, the post space was prepared and the roots were divided into four groups according to the following factors: adhesive system/resin cement (Ambar/ AllCem Core [FGM] and RelyX U200 [3M]) and application mode (manual or sonic). The posts were cemented and the roots were cut into discs and submitted to push-out bond strength (POBS) test. The failure mode was evaluated using a stereoscope at 25x magnification. The data were analyzed statistically using ANOVA and Tukey’s post-hoc test (α = 0.05). Results: The sonically activated RelyX U200 group was superior to the other groups. RelyX U200 manually applicated showed similar results to those of sonically activated Âmbar/AllCem. These three groups outperformed the Âmbar/AllCem manually applicated group. Adhesive failure between dentin and resin cement was the most predominant pattern. Conclusion: Sonic application of self-etching adhesive and self-adhesive cement improved the POBS of fiber posts to the root canal.

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