Cavitation erosion resistance of ZrC nanoceramic coating

Author(s):  
Hongqin Ding ◽  
Shuyun Jiang ◽  
Jiang Xu

A ZrC nanoceramic coating was prepared on the bare 316 stainless steel for improving the cavitation erosion resistance by the double glow discharge sputter technique. The phase constitution and surface microstructure of the ZrC nanoceramic coating were characterized by X-ray diffraction, scanning electron microscope, and transmission electron microscopy. A 10-µm-thick ZrC nanoceramic coating exhibited equiaxed grains with an average grain size of 9 nm. The adhesion strength and mechanical properties for the ZrC nanoceramic coating were evaluated by scratch test and nanoindentation. The hardness value of the ZrC nanoceramic coating was about four times that of the uncoated 316 stainless steel. The cavitation erosion behavior of the ZrC nanoceramic coating in tap water was characterized by the combination of an ultrasonic vibration system with an electrochemical workstation. The volume loss, erosion depth, scanning electron microscope morphology, and electrochemical test were adopted to assess the surface damage of the ZrC nanoceramic coating. The results show that the volume loss of the ZrC nanoceramic coating is 0.53 mm3, which is only 46% of the 316 stainless steel (1.14 mm3) after cavitation test, and erosion damage of the ZrC nanoceramic coating is significantly decreased as compared to the uncoated 316 stainless steel. The electrochemical test results also indicate that the ZrC nanoceramic coating shows higher corrosion resistance than the 316 stainless steel under cavitation erosion condition. Thus, the ZrC nanoceramic coating can be adopted to enhance the cavitation erosion resistance of the 316 stainless steel.

2014 ◽  
Vol 225 ◽  
pp. 109-114
Author(s):  
Beata Śniegocka ◽  
Marek Szkodo ◽  
Jarosław Chmiel

Cavitation erosion performance of modified macroscopic internal structure 316L stainless steel was investigated. The samples processed by means of SLM method were subjected to cavitation erosion test. The scanning electron microscope Philips 30/ESEM was used to examine morphology of eroded surface.


Author(s):  
Hongqin Ding ◽  
Shuyun Jiang ◽  
Jiang Xu

The purpose of this paper is to study the effect of chemical heat treatments on cavitation erosion resistance of the 304 stainless steel. Three types of diffusion layers are prepared on the 304 stainless steel using gas nitriding, gas carburizing, and carbonitriding treatments. Phase composition and surface microstructure of the diffusion layers are characterized by X-ray diffraction and scanning electron microscopy. And then, the cavitation erosion behavior of the diffusion layers are tested and compared with the one of the 304 stainless steel. The cavitation test is performed in an ultrasonic vibration system integrated with an electrochemical workstation. The mass loss, scanning electron microscopic morphology, and electrochemical test are adopted to assess the surface damage of the diffusion layers. A measurement for the mechanical properties of the diffusion layers shows that the hardness and the elastic modulus of the gas nitrided diffusion layer, carbonitrided diffusion layer, carburized diffusion layer, and 304 stainless steel are 5.3 GPa and 260 GPa, 4.2 GPa and 236 GPa, 4.0 GPa and 210 GPa, 2.5 GPa and 193 GPa, respectively. A cavitation erosion test of 14 h shows that mass loss of the gas nitrided diffusion layer, carbonitrided diffusion layer, carburized diffusion layer, and 304 stainless steel is 5.19 mg, 8.97 mg, 14.37 mg, and 6.62 mg, respectively. The electrochemical test results also indicate that the gas nitrided diffusion layer has a higher corrosion resistance than the carburized diffusion layer, carbonitrided diffusion layer, and stainless steel under cavitation erosion condition. As a conclusion, the gas nitrided diffusion layer is capable of enhancing the cavitation erosion resistance of the stainless steel, while the carburized diffusion layer and carbonitrided diffusion layer increases the mass loss of the stainless steel under cavitation erosion condition.


Coatings ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 307 ◽  
Author(s):  
Xiang Ding ◽  
Du Ke ◽  
Chengqing Yuan ◽  
Zhangxiong Ding ◽  
Xudong Cheng

Conventional, multimodal and nanostructured WC-12Co coatings with different WC sizes and distributions were prepared by high velocity oxy-fuel spray (HVOF). The micrographs and structures of the coatings were analyzed by scanning electron microscope (SEM), X-ray diffractometer (XRD) et al. The porosity, microhardness and fracture toughness of the WC-Co coatings were measured. The coating resistance to cavitation erosion (CE) was investigated by ultrasonic vibration cavitation equipment and the cavitation mechanisms were explored. Results show that there is serious WC decarburization in nanostructured and multimodal WC-Co coatings with the formation of W2C and W phases. The nanostructured WC-Co coating has the densest microstructure with lowest porosity compared to the other two WC-Co coatings, as well as the highest fracture toughness among the three coatings. It was also discovered that the nanostructured WC-Co coating exhibits the best CE resistance and that the CE rate is approximately one-third in comparison with conventional coating.


2011 ◽  
Vol 239-242 ◽  
pp. 2229-2232 ◽  
Author(s):  
Chang Jun Chen ◽  
Yan Zhan Su ◽  
Qin Cao ◽  
Min Zhang

In this paper, Electro-Spark Deposition (ESD) technology was used to enhance the cavitation erosion resistance of the stainless steel. The microstructure and composition of the deposition layers were studied by optical microscope (OM), scanning electron microscope (SEM) and energy dispersive Spectrometry (EDS) on cavitation erosion resistance was investigated. The microhardness was measured too. The cavitation erosion resistance was measured in ultrasonic equipment. The preliminary study confirmed that the cavitation erosion resistance of the deposition layer was enhanced compared to the untreated substrate. Now, vane wheel made of cast-iron, stainless steel and oil bump damaged by cavitation erosion have been repaired by ESD. And the properties of the repaired vane wheels were the same as the new ones.


1980 ◽  
Vol 59 (2) ◽  
pp. 124-128 ◽  
Author(s):  
Y. Galindo ◽  
K. McLachlan ◽  
Z. Kasloff

A silver-plating technique was developed in an effort to produce good mechanical bonding characteristics between stainless steelpins and amalgam. Metallographic microscope and scanning electron microscope (SEM) studies were made to assess the presence, or otherwise, of such a bond between (a) the silver layer plating and the surface of the stainless steel pins, and (b) and silver plating and the amalgam. Unplated stainless steel and sterling silver pins were used as a control and as a comparison, respectively. A "rubbing" technique of condensation was devised to closely adapt amalgam to the pins. It is concluded that there is strong evidence for the existence of a good bond between the plated pins and amalgam. The mechanical performance of the bond is discussed elsewhere. 1.


2016 ◽  
Vol 1133 ◽  
pp. 324-328 ◽  
Author(s):  
Muhammad Aslam ◽  
Faiz Ahmad ◽  
P.S.M. Bm-Yousoff ◽  
Khurram Altaf ◽  
Afian Omar ◽  
...  

Optimization of solvent debinding process parameters for powder injection molded 316L stainless steel (SS) has been reported in this research work. Powder gas atomized (PGA) 316L SS was blended with a multicomponent binder in Z-blade mixer at 170°C ± 5°C for 90 minutes. Feedstock was successfully injected at temperature 170 ± 5°C. Injection molded samples were immersed in n-heptane for 2h, 4h, 6h and 8h at temperatures 50°C ,55°C and 60°C to extract the soluble binder components. Scanning electron microscope (SEM) results attested that soluble binder components were completely extracted from injection molded samples at temperature 55°C after 6h.


Author(s):  
Rajeev Kumar ◽  
Sanjeev Bhandari ◽  
Atul Goyal

Various aspects such as development, experimentation, and analysis have been covered in the present work to examine the behavior of test coatings under slurry erosion. The primary objective of the present study was to establish the specific mass loss from the test coatings under various slurry environmental conditions and highlights the importance of the addition of alumina in improving the slurry erosion resistance of Ni-TiO2 coating. To attain this objective, two powder compositions, viz. Ni-20TiO2 and Ni-15TiO2-5Al2O3 were deposited onto the CA6NM grade hydro-turbine steel using high velocity frame spray process. The microstructural characterization of the coatings was done by employing surface roughness tester, scanning electron microscope/energy-dispersive X-ray spectroscopy, and X-ray diffraction techniques, whereas mechanical analysis was carried out using micro-hardness and bond strength tester. The slurry erosion tests were performed using an indigenously fabricated high speed slurry erosion test rig at different levels of rotational speed, average particle size of erodent, and slurry concentration in order to explore their effects on slurry erosion performance of test coatings. The slurry erosion results, as well as scanning electron microscope observations of eroded specimens, revealed higher slurry erosion resistance of Ni-15TiO2-5Al2O3 coating in comparison with Ni-20TiO2 coating. Furthermore, each operational parameter was found to have a proportional effect on specific mass loss in case of both the coatings.


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