scholarly journals Effect of grain size of dental zirconia on shear bond strength of composite resin cement

2020 ◽  
Vol 18 ◽  
pp. 228080002097813
Author(s):  
JiHwan Jeon ◽  
Shin Hye Chung ◽  
Seung-Hoon Um ◽  
Sang-Hoon Rhee
Keyword(s):  
Grain Size ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Interfacial Free Energy ◽  
Small Sample ◽  
Resin Cement ◽  
Alumina Powder ◽  
Average Grain Size ◽  
Interfacial Free Energies

The effect of grain size of dental zirconia on the shear bond strength of composite resin cement was newly studied. Disc-shaped dental zirconia with small (sample S) and large (sample L) grains were made by sintering of pre-sintered dental zirconia at 1450°C for 0.5 h and 40 h, respectively. After the sintering, the average grain size of sample S was 1.37 ± 0.15 µm, while that of sample L was 3.74 ± 0.50 µm. The sintered discs were successively polished with different grades of diamond and alumina slurries. The interfacial free energies were 63.5 ± 4.2 dyne/cm for sample S and 52.1 ± 5.5 dyne/cm for sample L. Stainless steel cylinders, previously sandblasted with 50 µm alumina powder, were bonded to the zirconia discs using composite resin cement. Next, samples were kept in an oven for 7 d at 36.5°C. The shear bond strength of sample S was 23.0 ± 4.5 MPa while that of sample L was 17.5 ± 4.6 MPa. After the fracture, the areal % values of composite resin cement remaining on the zirconia surfaces were 89.7 ± 5.9% for sample S and 61.6 ± 5.5% for sample L. The results suggest that grain size reduction has a potential to enhance the degree of bonding between a composite resin cement and a dental zirconia due to the increase of interfacial free energy.

scholarly journals Long Term Water Storage Deteriorates Bonding of Composite Resin to Alumina and Zirconia Short Communication

2013 ◽  
Vol 7 (1) ◽  
pp. 123-125 ◽  
Author(s):  
T.T. Heikkinen ◽  
J.P Matinlinna ◽  
P.K. Vallittu ◽  
L.V.J. Lassila
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Resin Composite ◽  
Water Storage ◽  
Particulate Composite ◽  
Resin Cement ◽  
Control Group ◽  
Set Up

Objective of this study was to evaluate the effects of long term water storage and ageing on the bond strength of resin composite cement to yttria-stabilized zirconium dioxide (zirconia) and dialuminium trioxide (alumina). Substrate specimens of alumina and zirconia were air particle abraded with dialuminium trioxide before priming and application of composite resin. Priming was made with gamma metharyloxy-trimethoxysilane or acryloxypropyl-trimethoxysilane monomer after which the intermediate dimethacrylate resin was applied and photopolymerized. This was followed by curing particulate composite resin cement (Relyx ARC) to the substrate as a resin stub. The ageing methods of the specimens (n=6) were: (1) they stored four years in 37±1ºC distilled water, (2) thermocycled 8000 times between 55±1ºC and 5±1ºC, (3) stored first in water for four years and then thermocycled. Specimens which were stored dry, were used as controls. Bonding of composite resin was measured by shear-bond strength test set-up. Both thermocycling and long-term water storage decreased significantly shear bond strength values compared to the control group (from the level of 20 MPa to 5 MPa) regardless of the used primer or the type of the substrate. Combination of four years water storage and thermocyling reduced the bond strength even more, to the level of two to three megapascals. In can be concluded that water storage and thermocycling itselves, and especially combination of water storage and thermocycling can cause considerable reduction in the bond strength of composite resin cement to alumina and zirconia.

Early Hardness and Shear Bond Strength of Dual-cure Resin Cement Light Cured Through Resin Overlays With Different Dentin-layer Thicknesses

2014 ◽  
Vol 39 (4) ◽  
pp. 398-406 ◽  
Author(s):  
H-S Chang ◽  
J-W Kim
Keyword(s):  
Bond Strength ◽  
Layer Thickness ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Surface Hardness ◽  
Resin Cement ◽  
Indirect Composite ◽  
Light Curing ◽  
Power Densities ◽  
Enamel Layer

SUMMARY The purpose of this study was to investigate whether dentin-layer thickness of resin overlays could affect the early hardness and shear bond strength of dual-cure resin cement (DCRC, RelyX ARC) after light curing with light curing units (LCUs) of various power densities: Optilux 360 (360), Elipar Freelight 2 (FL2), and Elipar S10 (S10). Resin overlays were fabricated using an indirect composite resin (Sinfony) with a dentin layer, an enamel layer, and a translucent layer of 0.5 mm thickness each (0.5-0.5-0.5) or of 0.2 mm, 0.5 mm, and 0.8 mm thickness (0.2-0.5-0.8), respectively. The DCRC was light cured for 40 seconds through the overlays, and surface hardness and shear bond strength to bovine dentin were tested 10 minutes after the start of light curing. Surface hardness was higher when the DCRC was light cured through the 0.2-0.5-0.8 combination than when the DCRC was light cured through the 0.5-0.5-0.5 combination with all LCUs. The ratio of upper surface hardness of DCRC light cured through resin overlays relative to the upper surface hardness of DCRC light cured directly was more than 90% only when the DCRC was light cured with S10 through the 0.2-0.5-0.8 combination. The shear bond strength value was higher when the DCRC was light cured with S10 through the 0.2-0.5-0.8 combination than when light cured with S10 through the 0.5-0.5-0.5 combination. This study indicates that reducing the dentin-layer thickness while increasing the translucent-layer thickness of resin inlays can increase the photopolymerization of DCRC, thereby increasing the early bond strength of resin inlays to dentin.

Shear bond strength between acrylic resin teeth and composite resin

2014 ◽  
Vol 30 ◽  
pp. e38-e39
Author(s):  
M.A. Basílio ◽  
K.V. Cardoso ◽  
G.M.R.M. De Souza ◽  
E.M. Mariscal ◽  
J.N. Arioli-Filho
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Acrylic Resin

scholarly journals Effect of surface treatments of laboratory-fabricated composites on the microtensile bond strength to a luting resin cement

2004 ◽  
Vol 12 (1) ◽  
pp. 45-50 ◽  
Author(s):  
Carlos José Soares ◽  
Marcelo Giannini ◽  
Marcelo Tavares de Oliveira ◽  
Luis Alexandre Maffei Sartini Paulillo ◽  
Luis Roberto Marcondes Martins
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Composite Resin ◽  
Surface Treatments ◽  
Resin Cement ◽  
Single Bond ◽  
Microtensile Bond Strength ◽  
Bonded Interface ◽  
Luting Composite ◽  
Effect Of Surface

The purpose of this study was to evaluate the influence of different surface treatments on composite resin on the microtensile bond strength to a luting resin cement. Two laboratory composites for indirect restorations, Solidex and Targis, and a conventional composite, Filtek Z250, were tested. Forty-eight composite resin blocks (5.0 x 5.0 x 5.0mm) were incrementally manufactured, which were randomly divided into six groups, according to the surface treatments: 1- control, 600-grit SiC paper (C); 2- silane priming (SI); 3- sandblasting with 50 mm Al2O3 for 10s (SA); 4- etching with 10% hydrofluoric acid for 60 s (HF); 5- HF + SI; 6 - SA + SI. Composite blocks submitted to similar surface treatments were bonded together with the resin adhesive Single Bond and Rely X luting composite. A 500-g load was applied for 5 minutes and the samples were light-cured for 40s. The bonded blocks were serially sectioned into 3 slabs with 0.9mm of thickness perpendicularly to the bonded interface (n = 12). Slabs were trimmed to a dumbbell shape and tested in tension at 0.5mm/min. For all composites tested, the application of a silane primer after sandblasting provided the highest bond strength means.

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