Formation Process of Antimony-Doped Stannic Oxide Film from Organometallic Compounds by Thermal Decomposition

1972 ◽  
pp. 880-885 ◽  
Author(s):  
Toru MATSUSHITA ◽  
Tadashi SEKIYA ◽  
Iwao YAMAI
2011 ◽  
Vol 412 ◽  
pp. 44-48
Author(s):  
Zhi Rong Suo ◽  
Hui Liu ◽  
Na Wei

The walnut-like α-Ni (OH)2 architectures have been successfully synthesized through a microwave-assisted hydrothermal method using urea as a hydrolysis-controlling agent and polyethylene glycol (PEG) as a surfactant. The NiO architectures with similar morphology were obtained by a simple thermal decomposition process of the precursor α-Ni (OH)2. The as-obtained products were well characterized by XRD, SEM, TEM, and FTIR. The experimental results shown that walnut-like α-Ni (OH)2 architectures with a diameter of 2-6 μm. The formation process of Ni (OH)2 architectures was observed by SEM via different hydrothermal reaction times.


Polyhedron ◽  
1985 ◽  
Vol 4 (7) ◽  
pp. 1293-1295 ◽  
Author(s):  
John D. Donaldson ◽  
Susan M. Grimes ◽  
Arthur F. Lec. Holding ◽  
Michelle Hornby

2013 ◽  
Vol 737 ◽  
pp. 153-158 ◽  
Author(s):  
Agus Haryono ◽  
Sri Budi Harmami ◽  
Dewi Sondari

The thermal decomposition of organometallic compounds was used to synthesize magnetite nanoparticles in high boiling point organic solvent containing stabilizing surfactants. Iron (III) acetylacetonate was used as the organometallic precursor in this work. Thermal decomposition of cationic metal center leads directly to the metal oxide, in the presence of 1,2-hexadecanediol, oleylamine, and oleic acid in diphenyl ether. Characterization with the Particle Size Analyzer (PSA) showed the size of the obtained magnetite nanoparticles was 2.1 ± 0.9 nm with polydispersity index of 0.327. The morphology and chemical structure of the obtained magnetite nanoparticle was characterized by using of Transmition Electron Microscopy (TEM) and Fourier-Transformed Infrared (FTIR) spectroscopy. The application of magnetite nanoparticles in the industrial wastewater treatment was also discussed.


1985 ◽  
Vol 24 (S3) ◽  
pp. 7 ◽  
Author(s):  
Akira Ariizumi ◽  
Kiyoshi Kawamura ◽  
Ichiro Kikuchi ◽  
Iwao Kato

2007 ◽  
Vol 26 (1) ◽  
pp. 191-198 ◽  
Author(s):  
Raouf S. H. Mikhail ◽  
Suzy A. Selim ◽  
Farouk I. Zeidan

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