scholarly journals Influence of nickel on butanol production by Clostridium beijerinckii using hydrolyzate from green coconut shell

2021 ◽  
Vol 29 ◽  
pp. 381-388
Author(s):  
Petrúcia Karine Santos de Brito Bezerra ◽  
Beatriz Meneghetti Costa de Araújo ◽  
Otávio Lima da Silva ◽  
Beatriz de Azevedo ◽  
Stephanie Caroline Bivar Matias ◽  
...  
Keyword(s):  
Industrial Waste ◽  
High Performance ◽  
Ammonium Acetate ◽  
Clostridium Beijerinckii ◽  
Added Value ◽  
Coconut Shell ◽  
Fermentable Sugars ◽  
Process Conditions ◽  
Butanol Production ◽  
Biotechnological Processes

The improvement of biotechnological processes capable of transforming agro-industrial waste into products with high added value has stood out in the area of renewable energies, promoting positive impacts to the environment. Thus, the present work evaluated the influence of nickel on the conversion of fermentable sugars, present in the green coconut shell hydrolyzate (GCSH), into butanol and other products. Fermentation assays were performed at 37 °C, starting with 19.4 g.L-1 of sugars and 1.0 g.L-1 of inoculum (C. beijerinckii). The GCSH was supplemented with tryptone, yeast extract, ammonium acetate, minerals and phosphate buffer. Two conditions were tested: with and without addition of nickel. Concentrations of sugars (glucose and xylose), intermediate products (organic acids), acetone, butanol, and ethanol were determined by high performance liquid chromatography (HPLC). The results show that the butanol production was higher from GCSH without addition of nickel, reaching a concentration of 2.14 g.L-1 of butanol. Therefore, the presence of nickel in the hydrolyzate was not favorable in the production of butanol under the studied process conditions.

Discussion of Feasibility of Producing Soil Stabilizer with Industrial Waste

2011 ◽  
Vol 243-249 ◽  
pp. 2194-2197
Author(s):  
Xiao Xuan Deng ◽  
Lei Dai ◽  
Zhan Guo Li ◽  
Xin Huang
Keyword(s):  
Industrial Waste ◽  
Economic Benefit ◽  
High Performance ◽  
Soil Structure ◽  
Added Value ◽  
Management Mode ◽  
Cost Ratio ◽  
Soil Stabilizer ◽  
Technical Effect ◽  
Stabilized Soil

The feasibility of utilizing industrial waste to produce soil stabilizer with high added value is discussed from technical effect, economic benefit and production and management mode. Principle of design of the stabilizer with industrial waste is offered based on the properties of stabilized soil structure formation and its special demand on stabilizer components; the examples of the stabilizer composition are presented, and the performance/cost ratio of the stabilizers are compared with that of cement. Reasonable production and management mode for industrially producing the stabilizer with industrial waste is discussed also. It is suggested that as long as appropriate industrial waste is selected intentionally to meet the special demand on the stabilizer composition needed to form stabilized soil structure, the soil stabilizer with high performance/cost ratio can be obtained. It is advised that the stabilizer should be designed individually according to the properties of the soil to be stabilized, the stabilizer should be produced with the production mode of mixing multi-components and adopt the management pattern of incorporating designing, production and sale.

scholarly journals Simple HPLC-PDA Analysis to Determine Illegal Synthetic Dyes in Herbal Medicines

2021 ◽  
Vol 11 (14) ◽  
pp. 6641
Author(s):  
Kyung-Yuk Ko ◽  
Eun-Young Choi ◽  
Se-Hee Jeong ◽  
Sohwa Kim ◽  
Choon-Kil Lee ◽  
...  
Keyword(s):  
High Performance ◽  
Hplc Analysis ◽  
Ammonium Acetate ◽  
Herbal Medicines ◽  
Positive Sample ◽  
Array Detector ◽  
Synthetic Dyes ◽  
Sunset Yellow ◽  
Herbal Medication ◽  
Relative Standard

Various synthetic dyes are artificially added to herbal medicines for the purpose of visual attraction. In order to monitor the illegal usage of synthetic dyes in herbal medication, a rapid and straightforward analysis method to determine synthetic dyes is required. The study aimed to develop and validate a high-performance liquid chromatography (HPLC) analysis to determine ten synthetic dyes in Hawthorn fruit, Cornus fruit, and Schisandra fruit. Ten synthetic dyes such as Tartrazine, Sunset yellow, Metanil yellow, Auramine O, Amaranth, Orange II, Acid red 73, Amaranth, New Coccine, Azorubine, and Erythrosine B, were extracted using 50 mM ammonium acetate in 70% MeOH; then separated by gradient elution with a mobile phase consisting of acetonitrile and 50 mM ammonium acetate in distilled water using a photodiode array detector (PDA) at 428 nm or 500 nm. In addition, this study established the LC-MS/MS method to confirm the existence of synthetic dyes in the positive sample solution. The HPLC analysis had good linearity (r2 > 0.999). The recoveries of this method ranged from 74.6~132.1%, and the relative standard deviation (RSD) values were less than 6.9%. Most of the samples fulfilled the acceptance criteria of the AOAC guideline. This study demonstrates that the HPLC analysis can be applied to determine ten synthetic dyes in herbal medication.

On the Extraction of Milling Tools Out of Shrink Fit Chucks

2012 ◽  
Vol 523-524 ◽  
pp. 445-450 ◽  
Author(s):  
Berend Denkena ◽  
Dennis Heinisch
Keyword(s):  
High Performance ◽  
Experimental Investigations ◽  
Process Conditions ◽  
Geometrical Parameters ◽  
Dynamic Force ◽  
Unique Type ◽  
Milling Operations ◽  
Torque Transmission ◽  
Shrink Fit ◽  
Milling Tools

Thermal shrink fit chucks are widely used in high performance machining where excellent concentricity and high torque transmission are required. It was reported that in those milling operations, severe damage of tools, workpieces, and also machine tools occurs due to an extraction of the milling tool out of the shrink fit chuck during the process. Although, theoretically the interference fit assembly should withstand certain process forces, milling tools are apparently pulled out under special process conditions. The resulting increase of the cutting depth often leads to tool overload and breakage. So far, the phenomenon of tool extraction could not be explained. This paper presents an experimental approach of the investigation of the phenomenon of axial tool extraction. Therefore, a unique type of test rig for main spindles and tool interfaces is used. Experimental investigations on dynamic force and torque combinations leading to tool extraction are described. Results show, that the holding force is not only affected by geometrical parameters of the shrink fit chuck, but also by the applied dynamic load.

scholarly journals DETERMINATION OF SULFONAMIDES IN CHICKEN MEAT BY SOLID PHASE EXTRACTION AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY

1970 ◽  
Vol 63 ◽  
Author(s):  
C. T. Matea ◽  
C. Bele ◽  
F. Dulf
Keyword(s):  
High Performance ◽  
Ammonium Acetate ◽  
Solid Phase ◽  
Simultaneous Detection ◽  
Gradient Elution ◽  
Normal Phase ◽  
Chicken Meat ◽  
Liquid Liquid Extraction ◽  
Halogenated Solvents

This paper describes a method for the simultaneous detection and quantification of six sul-fonamides in chicken meat using normal phase cartridge clean-up and HPLC with UV detection . A liquid – liquid extraction and Sep- Pak silica clean-up procedure which minimizes the presence of halogenated solvents was used for sample preparation . The HPLC determination was performed using a RP C 18 column and sulfonamides were detected at 266 nm. Mobile phase was 0.01 M ammonium acetate pH 4.6 ( A ) and methanol ( B). Chromatographic separation was obtained by gradient elution ( 22 % B to 50 % within 17 min , back to 22 % in 2 min, equilibration for 5 min).Average recoveries of analytes from spiked meat were higher than 74 % .

scholarly journals Bioreactors for lignocellulose conversion into fermentable sugars for production of high added value products

2015 ◽  
Vol 100 (2) ◽  
pp. 597-611 ◽  
Author(s):  
Rossana Liguori ◽  
Valeria Ventorino ◽  
Olimpia Pepe ◽  
Vincenza Faraco
Keyword(s):  
Added Value ◽  
Fermentable Sugars ◽  
Lignocellulose Conversion

scholarly journals High-performance liquid chromatography of uroporphyrinogen and coproporphyrinogen isomers with amperometric detection

1986 ◽  
Vol 234 (3) ◽  
pp. 629-633 ◽  
Author(s):  
C K Lim ◽  
F Li ◽  
T J Peters
Keyword(s):  
Mobile Phase ◽  
High Performance ◽  
Ammonium Acetate ◽  
Amperometric Detection ◽  
Reversed Phase ◽  
Fluorescent Detection ◽  
Organic Modifiers ◽  
Ammonium Acetate Buffer ◽  
Effects Of Ph ◽  
Ph Buffer

A reversed-phase h.p.l.c. system, with an ODS-Hypersil column with acetonitrile or methanol in ammonium acetate buffer as mobile phase, is described for the separation of uro-and copro-porphyrinogen isomers. The porphyrinogens are detected amperometrically with sensitivity comparable with that of the fluorescent detection of porphyrins. The effects of pH, buffer concentration and organic modifiers on retention and resolution were studied. The method is suitable for both analytical and preparative separation of porphyrinogens.

Comparison of different Vetiver grass pretreatment techniques and their impact on immobilized butanol production by Clostridium beijerinckii TISTR 1461

Cellulose ◽  
2021 ◽  
Author(s):  
Fuangfa Srisuk ◽  
Piyawat Chinwatpaiboon ◽  
Thanaphat Atjayutpokin ◽  
Akarin Boonsombuti ◽  
Ancharida Savarajara ◽  
...  
Keyword(s):  
Clostridium Beijerinckii ◽  
Vetiver Grass ◽  
Butanol Production

Process and Evaluation of High Reliability Reworkable Edge Bond Adhesives for Large Area BGA Applications

2016 ◽  
Vol 2016 (DPC) ◽  
pp. 002018-002053
Author(s):  
Swapan Bhattacharya ◽  
Fei Xie ◽  
Daniel F. Baldwin ◽  
Han Wu ◽  
Kelley Hodge ◽  
...  
Keyword(s):  
High Performance ◽  
Printed Circuit Boards ◽  
Process Development ◽  
High Reliability ◽  
Optimum Process ◽  
Process Conditions ◽  
Harsh Environment ◽  
Mechanical Shock ◽  
Large Area ◽  
Reliability Performance

Reworkable underfills and edge bond adhesives are finding increasing utility in high reliability and harsh environment applications. The ASICs and FPGAs often used in these systems typically require designs incorporating large BGAs and ceramic BGAs. For these high reliability and harsh environment applications, these packages typically require underfill or edge bond materials to achieve the needed thermal cycle, mechanical shock and vibration reliability. Moreover, these applications often incorporate high dollar value printed circuit boards (on the order of thousands or tens of thousands of dollars per PCB) hence the need to rework these assemblies and maintain the integrity of the PCB and high dollar value BGAs. This further complicates the underfill requirements with a reworkability component. Reworkable underfills introduce a number of process issues that can result in significant variability in reliability performance. In contrast, edge bond adhesives provide a high reliability solution with substantial benefits over underfills. One interesting question for the large area BGA applications of reworkable underfills and edge bond materials is the comparison of their reliability performance. This paper presents a study of reliability comparison between two robust selected reworkable underfill and edge bond adhesive in a test vehicle including 11mm, 13mm, and 27mm large area BGAs. Process development for those large area BGA applications was also conducted on the underfill process and edge bond process to determine optimum process conditions. For underfill processing, establishing an underfill process that minimizing/eliminates underfill voids is critical. For edge bond processing, establishing an edge bond that maximizes bond area without encapsulating the solder balls is key to achieving high reliability. In addition, this paper also presents a study of new high performance reworkable edge bond materials designed to improve the reliability of large area BGAs and ceramic BGAs assemblies while maintaining good reworkablity. Four edge bond materials (commercially available) were studied and compared for a test vehicles with 12mm BGAs. The reliability testing protocol included board level thermal cycling (−40 to 125°C), mechanical drop testing (2900 G), and random vibration testing (3 G, 10 – 1000 Hz).

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