scholarly journals Development of Solid Phase Micro Extraction Technique for Determination of Triazines in Water Samples Using Experimental Design

2016 ◽  
Vol 28 (3) ◽  
pp. 562-566 ◽  
Author(s):  
Md Pauzi Abdullah ◽  
Kamarruddin Asri ◽  
Mohamad Salleh Ramli ◽  
Maimunah Sulaiman Wahid ◽  
Wan Mohd Afiq Wan Mohd Khalik
RSC Advances ◽  
2015 ◽  
Vol 5 (49) ◽  
pp. 39084-39096 ◽  
Author(s):  
Arash Asfaram ◽  
Mehrorang Ghaedi ◽  
Alireza Goudarzi ◽  
Mustafa Soylak

Novel dispersive solid phase micro-extraction and dispersive liquid–liquid micro-extraction determination of Auramine-O content in various real samples.


2015 ◽  
Vol 39 (12) ◽  
pp. 9813-9823 ◽  
Author(s):  
Arash Asfaram ◽  
Mehrorang Ghaedi ◽  
Alireza Goudarzi ◽  
Mustafa Soylak ◽  
Sanaz Mehdizadeh Langroodi

This paper presents an extraction method based on dispersive-nanoparticle-solid phase microextraction for the preliminary preconcentration and subsequent spectrophotometric determination of trace amounts of malachite green.


2015 ◽  
Vol 103 (5) ◽  
Author(s):  
Mostafa Khajeh ◽  
Mousa Bohlooli ◽  
Elham Jahanbin ◽  
Mansour Ghaffari-Moghaddam ◽  
Zahra Safaei Moghaddam

AbstractIn this study, the solid-phase tea waste procedure was used for separation, preconcentration and determination of uranium from water samples by UV-Vis spectrophotometer. In addition, Box-Behnken experimental design was employed to investigated the influence of six variables including pH, mass of adsorbent, eluent volume, amount of 1-(2-pyridylazo)-2-naphthol (PAN); and sample and eluent flow rates on the extraction of analyte. High determination coefficient (


2009 ◽  
Vol 7 (1) ◽  
pp. 35-41 ◽  
Author(s):  
Aleksandra Dubiella-Jackowska ◽  
Żaneta Polkowska ◽  
Lech Dariusz ◽  
Piotr Pasławski ◽  
Wojciech Staszek ◽  
...  

AbstractA solid phase extraction technique for the determination of platinum(IV) at trace levels by inductively coupled plasma mass spectromA solid phase extraction technique for the determination of platinum(IV) at trace levels by inductively coupled plasma mass spectrometry (ICP-MS) was developed. The method was based on retention of platinum in a sample on silica gel modified with aminepropyl groups. The retention of platinum(IV) from the sample solution and the recovery of platinum with 1.0 mol L−1 thiourea solution were quantitative. The relative standard deviation (RSD) was calculated as 5% (n = 7) at the 10 ng L−1 level. The enrichment factor was found to be (50-fold) for 250 mL of water sample. Under optimum conditions, the method detection limit (MDL) was found to be 1 ng L−1 for platinum in water matrices. Recoveries of Pt from spike addition to atmospheric water samples were quantitative (80–95%). The present method was used for the determination of platinum in precipitation, throughfall and runoff water samples.


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