Bulk cure study of nanoclay filled epoxy glass fiber reinforced composite material

2017 ◽  
Vol 37 (3) ◽  
pp. 247-259
Author(s):  
John Olusanya ◽  
Krishnan Kanny ◽  
Shalini Singh

Abstract The correlation between cure properties and structure of nanoclay filled composite laminate has not been studied extensively. Most of the cure studies were preferably done using small samples through a calorimetric method. In this study, the effect of varying weight ratio of nanoclay (1–5 wt%) on bulk cure properties of epoxy glass fiber reinforced composite (GFRC) laminates was studied. Bulk cure of unfilled and clay filled GFRC laminates was determined using the dynamic mechanical analysis-reheat method (DMA-RM). DMA-RM cure properties gave a better coordinate method, with better cure efficiency achieved in clay filled GFRC laminates when compared to unfilled GFRC laminates. The correlation between nanoclay and DMA-RM degree of cure was coordinated with compressive and in-plane shear strength properties. The degree of cure value of 78% by DMA-RM at 1 wt% clay filled GFRC corresponds with the compressive modulus and in-plane shear strength highest values, which are 20% and 14% increase, respectively, also at 1 wt% clay filled GFRC. The structures of the unfilled and clay filled epoxy were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Clay filled epoxy up to 3 wt% showed no distinct diffraction peak, which suggested that nanoclay is randomly dispersed in the matrix.

2021 ◽  
pp. 096739112110141
Author(s):  
Ferhat Ceritbinmez ◽  
Ahmet Yapici ◽  
Erdoğan Kanca

In this study, the effect of adding nanosize additive to glass fiber reinforced composite plates on mechanical properties and surface milling was investigated. In the light of the investigations, with the addition of MWCNTs additive in the composite production, the strength of the material has been changed and the more durable composite materials have been obtained. Slots were opened with different cutting speed and feed rate parameters to the composite layers. Surface roughness of the composite layers and slot size were examined and also abrasions of cutting tools used in cutting process were determined. It was observed that the addition of nanoparticles to the laminated glass fiber composite materials played an effective role in the strength of the material and caused cutting tool wear.


2017 ◽  
Author(s):  
◽  
John Olumide Olusanya

In this study, the fatigue life of fiber reinforced composite (FRC) materials system was investigated. A nano-filler was used to increase the service life of the composite structures under cyclical loading since such structures require improved structural integrity and longer service life. Behaviour of glass fiber reinforced composite (GFRC) enhanced with various weight percentages (1 to 5 wt. %) of Cloisite 30B montmorillonite (MMT) clay was studied under static and fatigue loading. Epoxy clay nanocomposite (ECN) and hybrid nanoclay/GFRC laminates were characterised using differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA). The mechanical properties of neat GFRC and hybrid nanoclay/GFRC laminates were evaluated. Fatigue study of the composite laminates was conducted and presented using the following parameter; matrix crack initiation and propagation, interfacial debonding, delamination and S–N relationship. Residual strength of the materials was evaluated using DMA to determine the reliability of the hybrid nanoclay/GFRC laminates. The results showed that ECN and hybrid nanoclay/GFRC laminates exhibited substantial improvement in most tests when compared to composite without nanoclay. The toughening mechanism of the nanoclay in the GFRC up to 3 wt. % gave 17%, 24% and 56% improvement in tensile, flexural and impact properties respectively. In the fatigue performance, less crack propagations was found in the hybrid nanoclay/GFRC laminates. Fatigue life of hybrid nanoclay/GFRC laminate was increased by 625% at the nanoclay addition up to 3 wt. % when compared to neat GFRC laminate. The residual strength of the composite materials revealed that hybrid nanoclay/GFRC showed less storage modulus reduction after fatigue. Likewise, a positive shift toward the right was found in the tan delta glass transition temperature (Tg) of 3 wt. % nanoclay/GFRC laminate after fatigue. It was concluded that the application of nanoclay in the GFRC improved the performance of the material. The hybrid nanoclay/GFRC material can therefore be recommended mechanically and thermally for longer usage in structural application.


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