Determination of 210Po in low-level wild bilberries reference material for quality control assurance in environmental analysis using extraction chromatography and α-particle spectroscopy

2020 ◽  
Vol 108 (2) ◽  
pp. 99-103 ◽  
Author(s):  
Santiago Hurtado-Bermúdez ◽  
José Luis Mas
Keyword(s):  
Quality Control ◽  
Reference Material ◽  
Reference Materials ◽  
Environmental Analysis ◽  
Extraction Chromatography ◽  
Activity Concentration ◽  
Natural Radionuclide ◽  
Research Centre ◽  
Low Level ◽  
Wild Berries

AbstractCertified reference materials (CRM) are being widely used for quality control assurance in environmental analysis. For certain CRM, the analytes and/or the range of concentrations are not be available or certified at all. The Joint Research Centre – Institute for Reference Materials and Measurements (JRC-IRMM) of the European Commission has issued a CRM of Wild Berries (IRMM-426) in order to validate radionuclide measurement methods for activity concentrations of the natural radionuclide 40K and the anthropogenic nuclides 90Sr and 137Cs, but not for 210Po. The aim of the work was to determine low-level activity concentration of 210Po in these wild berries. The activity concentration of 210Po was assessed by α-particle spectroscopy after dissolution of the sample by wet digestion and chemical isolation of Po by extraction chromatography. According to the time elapsed since sample collection, the results here shown can be useful not only for ultra low-level analysis of 210Po but also for 210Pb in the reference material.

scholarly journals Production and Use of BCR Reference Materials for Quality Assurance in Environmental Analysis: An Update

2001 ◽  
Vol 84 (6) ◽  
pp. 1786-1792 ◽  
Author(s):  
Philippe Quevauviller
Keyword(s):  
Quality Control ◽  
Quality Assurance ◽  
Reference Materials ◽  
Environmental Analysis ◽  
Control Charts ◽  
Certified Reference Materials ◽  
Background Information ◽  
Analytical Quality Control ◽  
Analytical Quality ◽  
Invaluable Tool

Abstract Reference materials represent an invaluable tool for analytical quality control. Certified Reference Materials (CRMs) are used for the validation of methods, whereas various types of (uncertified) Reference Materials (RMs) are used for routine quality control (establishment of control charts) and interlaboratory testing (e.g., proficiency testing). This paper provides background information on the production and use of environmental RMs and describes recent CRMs produced by the BCR (European Commission) for quality assurance in environmental analysis.

Experience with Certified Reference Material Proficiency Testing for Quality Control of Wheat

1998 ◽  
Vol 6 (A) ◽  
pp. A53-A61
Author(s):  
Judit Budai ◽  
Judit Fükó
Keyword(s):  
Quality Control ◽  
Reference Material ◽  
Proficiency Testing ◽  
Reference Materials ◽  
Certified Reference Material ◽  
Certified Reference Materials ◽  
Long Term Stability ◽  
Determining Factors ◽  
Chemical Section

The Chemical Section of OMH1,2 embarked on the preparation of a series of wheat samples as Certified Reference Materials (CRMs) in 1992. The certification processes were carried out according to the recommendations of ISO. Since then we have developed a series of flour samples as well. The investigations of the long-term stability and the application of wheat and flour CRMs are continuous. Wheat is one of the most widely grown crops in Hungary and it is one of the major determining factors of the economy. Its uniform and objective qualification is of great importance. There are well-equipped laboratories available with sufficient experience but, as the proficiency testing regularly showed, certified samples need to be used to achieve exact and uniform measuring results.

Activity concentration measurements of 137Cs, 90Sr and 40K in a wild food matrix reference material (Wild Berries) CCRI(II)-S8

Metrologia ◽  
2014 ◽  
Vol 51 (1A) ◽  
pp. 06007-06007 ◽  
Author(s):  
U Wätjen ◽  
T Altzitzogloa ◽  
A Ceccatelli ◽  
H Dikmen ◽  
L Ferreux ◽  
...  
Keyword(s):  
Reference Material ◽  
Activity Concentration ◽  
Wild Food ◽  
Food Matrix ◽  
Matrix Reference Material ◽  
Concentration Measurements ◽  
Wild Berries

Cooperative Survey of "SMA" Analyzers in Wisconsin—A Method of Improving Interlaboratory Performance

1973 ◽  
Vol 19 (1) ◽  
pp. 62-66 ◽  
Author(s):  
Ronald H Laessig ◽  
Thomas H Schwartz ◽  
Toni A Paskey
Keyword(s):  
Quality Control ◽  
Reference Material ◽  
Reference Materials ◽  
Interlaboratory Comparison ◽  
Essential Element ◽  
Control Program ◽  
Total Quality ◽  
Quality Control Program ◽  
Large Group ◽  
Cooperative Survey

Abstract A state-wide cooperative quality-control program for automated multichannel analytical systems is described. The survey benefits participating laboratories by providing, through regular comparison, a means of improving interlaboratory precision. A common lot of reference material used for a large group of similar multichannel analyzers is shown to significantly improve their precision. The study delineates components of interlaboratory variation resulting from the inconsistency of the reference materials and from the inherent precision of the analyzers. Errors in the assay values of commercial controls and reference sera, as well as problems of homogeneity in these products, are documented. These errors make some form of regular interlaboratory comparison an essential element of a total quality-control program

scholarly journals Study on the production of Reference Material (RM) for Vitamin B1, B2, B6 in health supplements

2021 ◽  
Vol 4 (4) ◽  
pp. 307-314
Author(s):  
Hang Nguyen Thi ◽  
Phuong Thao Le Thi ◽  
Huu Cuong Dang ◽  
Huyen Trang Luu Thi ◽  
Hong Hao Le Thi ◽  
...  
Keyword(s):  
Quality Control ◽  
Reference Material ◽  
Reference Materials ◽  
Vitamin B1 ◽  
Assessment Method ◽  
Internal Quality ◽  
Standard Samples ◽  
Mandatory Requirement ◽  
The Cost ◽  
Health Supplements

Vitamins are essential nutrients commonly found in food products in general and health supplements in particular. In order to accurately evaluate product quality, laboratories need to use reference material in analysis, proficiency assessment, method validation and ensure the validity of the results. The use of reference materials plays an important role in the quality control of test results and is a mandatory requirement for laboratories wishing to demonstrate appropriate competence as required by ISO/IEC 17025:2017. The need to provide reference materials for laboratories is huge. However, at present, there are very few domestic organizations that can produce reference materials, while the cost of buying reference materials from reputable firms in the world is expensive. In this study, we introduced the procedure and production reference materials for the analysis of B-group vitamins (B1, B2, B6). These reference materials were evaluated for homogeneity and stability in 322 days. The certified values are consistent with the concentrations of substances present in normal samples in practice. The measurement uncertainty ranges from 14.5 - 23.3 %. The reference materials can be used for internal quality control for domestic laboratories and is also a premise for further research on standard samples with different matrix and analytical criteria.

ICP-MS AND ICP-AES ANALYSIS OF PLANT REFERENCE MATERIALS

2019 ◽  
Vol 85 (6) ◽  
pp. 11-24
Author(s):  
I. V. Nikolaeva ◽  
A. A. Kravchenko ◽  
S. V. Palessky ◽  
S. V. Nechepurenko ◽  
D. V. Semenova
Keyword(s):  
Reference Material ◽  
Mass Spectrometer ◽  
Reference Materials ◽  
Atomic Emission ◽  
Icp Ms ◽  
Lithium Metaborate ◽  
Relative Standard ◽  
Microwave System ◽  
Total Analysis ◽  
Siberian Pine

Two methods — ICP-MS and ICP-AES are used for certification of the new reference material — needles of Siberian pine (NSP-1). Techniques of the analysis include decomposition of plant samples in two different ways: acid digestion in a microwave system MARS-5 and lithium metaborate fusion followed by ICP-MS and ICP-AES analysis of the solutions. Simultaneous determinations of all the elements were carried out in low, medium and high resolution using SF-mass-spectrometer ELEMENT and atomic-emission spectrometer IRIS Advantage with external calibrations and internal standards (In — ICP-MS, Sc —ICP-AES). Middle and high resolutions of ICP mass spectrometer were used for interference corrections. Data obtained by ICP-MS and ICP-AES with different decomposition techniques are in good agreement. The ICP-MS and ICP-AES techniques have been validated by the analysis of three plant reference materials: LB-1 (leaf of a birch), Tr-1 (grass mixture) and EK-1 (Canadian pondweed). These techniques were used for the determination of 38 elements in the new reference material NSP-1. Relative standard deviations for most of the determined elements were below 10%. Combination of ICP-MS and ICP-AES techniques for certification of the new reference material makes it possible to expand the set of elements to be determined and to reduce the total analysis time.

Studies and Application of Auger Monitoring System for Quality Control and Assurance of Al Bondpads

2016 ◽  
Author(s):  
Hua Younan
Keyword(s):  
Quality Control ◽  
Sample Preparation ◽  
Monitoring System ◽  
Failure Mechanisms ◽  
Wafer Fabrication ◽  
Contamination Level ◽  
Auger Analysis ◽  
Low Level ◽  
Monitoring Frequency ◽  
Control Procedures

Abstract In wafer fabrication (Fab), Fluorine (F) based gases are used for Al bondpad opening process. Thus, even on a regular Al bondpad, there exists a low level of F contamination. However, the F level has to be controlled at a lower level. If the F level is higher than the control/spec limits, it could cause F-induced corrosion and Al-F defects, resulting in pad discoloration and NSOP problems. In our previous studies [1-5], the theories, characteristics, chemical and physical failure mechanisms and the root causes of the F-induced corrosion and Al-F defects on Al bondpads have been studied. In this paper, we further study F-induced corrosion and propose to establish an Auger monitoring system so as to monitor the F contamination level on Al bondpads in wafer fabrication. Auger monitoring frequency, sample preparation, wafer life, Auger analysis points, control/spec limits and OOC/OOS quality control procedures are also discussed.

Analytical Quality Control (AQC) For Monitoring Trace Metals in the Coastal and Estuarine Environment

1986 ◽  
Vol 18 (4-5) ◽  
pp. 35-41 ◽  
Author(s):  
M. J. Gardner ◽  
D T. E. Hunt ◽  
G. Topping
Keyword(s):  
Quality Control ◽  
Trace Metals ◽  
Marine Pollution ◽  
Pollution Monitoring ◽  
Research Centre ◽  
Analytical Quality Control ◽  
Analytical Quality ◽  
Management Group ◽  
Analytical Results ◽  
Saline Waters

It is widely recognised that, unless special steps are taken, analytical results from a group of laboratories engaged in a monitoring programme are likely to be of poor comparability. This in turn can prejudice the conclusions drawn from the results of monitoring. On the basis of previous studies, the problem is known to be particularly acute for measurements of trace metals in saline waters. Recognising the difficulty, the Marine Pollution Monitoring Management Group (MPMMG) and the Water Research centre (WRc) have organised a programme of Analytical Quality Control (AQC). This has the objective of ensuring that analytical results for filterable cadmium and mercury in saline waters, obtained by water industry and other relevant laboratories, are of adequate accuracy and comparability for their intended uses. WRc is to coordinate a series of tests, some involving distributions of standards and samples, which the participating laboratories undertake; this series of tests, the background to the approach and some of the results obtained to date are described here.

Development and Certification of Formononetin Reference Material for Quality Control of Functional Foods and Botanical Supplements

2019 ◽  
Vol 15 (5) ◽  
pp. 553-559
Author(s):  
Ningbo Gong ◽  
Baoxi Zhang ◽  
Kun Hu ◽  
Zhaolin Gao ◽  
Guanhua Du ◽  
...  
Keyword(s):  
Quality Control ◽  
Reference Material ◽  
Functional Foods ◽  
Certified Reference Materials ◽  
Coulometric Titration ◽  
Pharmaceutical Formulations ◽  
Uncertainty Estimation ◽  
Expanded Uncertainty ◽  
Scanning Calorimetry ◽  
Botanical Supplements

Background: Formononetin is a common soy isoflavonoid that can be found abundantly in many natural plants. Previous studies have shown that formononetin possesses a variety of activities which can be applied for various medicinal purposes. Certified Reference Materials (CRMs) play a fundamental role in the food, traditional medicine and dietary supplement fields, and can be used for method validation, uncertainty estimation, as well as quality control. Methods: The purity of formononetin was determined by Differential Scanning Calorimetry (DSC), Coulometric Titration (CT) and Mass Balance (MB) methods. Results: This paper reports the sample preparation methodology, homogeneity and stability studies, value assignment, and uncertainty estimation of a new certified reference material of formononetin. DSC, CT and MB methods proved to be sufficiently reliable and accurate for the certification purpose. The purity of the formononetin CRM was therefore found to be 99.40% ± 0.24 % (k = 2) based on the combined value assignments and the expanded uncertainty. Conclusion: This CRM will be a reliable standard for the validation of the analytical methods and for quality assurance/quality control of formononetin and formononetin-related traditional herbs, food products, dietary supplements and pharmaceutical formulations.

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