scholarly journals Bond Strength Assessment Between Acrylic Teeth and Acrylic Resin Repairs: Effect of Different Surface Treatments

2016 ◽  
Vol 18 (2) ◽  
pp. 109
Author(s):  
M.T. Muñoz MSc ◽  
E. Reales DDS ◽  
L.H.M. Prates DDS, MSc, PhD ◽  
C.A.M. Volpato DDS, MSc, PhD

The aim of this study was to compare the shear bond strength between acrylic resin teeth and autopolymerizing acrylic resin repairs after different surface treatments. Seventy-two upper anterior acrylic resin denture teeth (MFT, Vita, Germany) were selected. Specimens were randomly assigned into six groups (n=12): G1-C, without surface treatment (control); G2-M, methylmetacrylate monomer (Jet, Clássico, Brazil) application; G3-A treatment with methylmetacrylate and metiletilcetone-based bonding agent (Vitacoll, Vita, Germany). The surface of G4-OA, G5-OAM and G6-OAA was airborne-particle abraded with aluminum oxide (Polidental, Wilson, Brazil); being repeated the treatments respectively of groups G1-C, G2-M e G3-A. All groups were then repaired with autopolymerizing acrylic resin (Jet, Clássico, Brazil). Shear bond strength test was performed using an universal testing machine (Instron 4444). Two-way ANOVA and post hoc Tukey’s analysis (p<0,05) were used for statistical comparison. The shear bond strengths of groups G4-OA, G5-OAM and G6-OAA were significantly higher (p<0,05) than that of groups G1-C, G2-M and G3-A. The shear bond strength of Group G3-A were significantly higher (p<0,05) than that of groups G1-C and G2-M. In conclution, chemical treatments in combination with bondig agents showed significant improvements in bond strength without aluminum oxide treatment. More significantly, surface treatment with aluminum oxide particles resulted in the highest bond strength values for acrylic resin teeth repaired with autopolymerizing acrylic resin. 

2016 ◽  
Vol 18 (2) ◽  
pp. 109
Author(s):  
M.T. Muñoz MSc ◽  
E. Reales DDS ◽  
L.H.M. Prates DDS, MSc, PhD ◽  
C.A.M. Volpato DDS, MSc, PhD

The aim of this study was to compare the shear bond strength between acrylic resin teeth and autopolymerizing acrylic resin repairs after different surface treatments. Seventy-two upper anterior acrylic resin denture teeth (MFT, Vita, Germany) were selected. Specimens were randomly assigned into six groups (n=12): G1-C, without surface treatment (control); G2-M, methylmetacrylate monomer (Jet, Clássico, Brazil) application; G3-A treatment with methylmetacrylate and metiletilcetone-based bonding agent (Vitacoll, Vita, Germany). The surface of G4-OA, G5-OAM and G6-OAA was airborne-particle abraded with aluminum oxide (Polidental, Wilson, Brazil); being repeated the treatments respectively of groups G1-C, G2-M e G3-A. All groups were then repaired with autopolymerizing acrylic resin (Jet, Clássico, Brazil). Shear bond strength test was performed using an universal testing machine (Instron 4444). Two-way ANOVA and post hoc Tukey’s analysis (p<0,05) were used for statistical comparison. The shear bond strengths of groups G4-OA, G5-OAM and G6-OAA were significantly higher (p<0,05) than that of groups G1-C, G2-M and G3-A. The shear bond strength of Group G3-A were significantly higher (p<0,05) than that of groups G1-C and G2-M. In conclution, chemical treatments in combination with bondig agents showed significant improvements in bond strength without aluminum oxide treatment. More significantly, surface treatment with aluminum oxide particles resulted in the highest bond strength values for acrylic resin teeth repaired with autopolymerizing acrylic resin. 


2013 ◽  
Vol 18 (4) ◽  
pp. 29-34 ◽  
Author(s):  
Josiane Xavier de Almeida ◽  
Mauren Bitencourt Deprá ◽  
Mariana Marquezan ◽  
Luciana Borges Retamoso ◽  
Orlando Tanaka

OBJECTIVE: To assess the adhesive resistance of metallic brackets bonded to temporary crowns made of acrylic resin after different surface treatments. METHODS: 180 specimens were made of Duralay and randomly divided into 6 groups (n = 30) according to surface treatment and bonding material: G1 - surface roughening with Soflex and bonding with Duralay; G2 - roughening with aluminum oxide blasting and bonding with Duralay; G3 - application of monomer and bonding with Duralay; G4 - roughening with Soflex and bonding with Transbond XT; G5 - roughening with aluminum oxide blasting and bonding with Transbond XT and G6: application of monomer and bonding with Transbond. The results were statistically assessed by ANOVA/Games-Howell. RESULTS: The means (MPa) were: G1= 18.04, G2= 22.64, G3= 22.4, G4= 9.71, G5= 11.23, G6= 9.67. The Adhesive Remnant Index (ARI) ranged between 2 and 3 on G1, G2 and G3 whereas in G4, G5 and G6 it ranged from 0 to 1, showing that only the material affects the pattern of adhesive flaw. CONCLUSION: The surface treatment and the material influenced adhesive resistance of brackets bonded to temporary crowns. Roughening by aluminum blasting increased bond strength when compared to Soflex, in the group bonded with Duralay. The bond strength of Duralay acrylic resin was superior to that of Transbond XT composite resin.


2017 ◽  
Vol 22 (4) ◽  
pp. 47-52 ◽  
Author(s):  
Marina Cumerlato ◽  
Eduardo Martinelli de Lima ◽  
Leandro Berni Osorio ◽  
Eduardo Gonçalves Mota ◽  
Luciane Macedo de Menezes ◽  
...  

ABSTRACT Objective: The aim of this in vitro study was to evaluate and compare the effects of grinding, drilling, sandblasting, and ageing prefabricated teeth (PfT) on the shear bond strength (SBS) of orthodontic brackets, as well as the effects of surface treatments on the adhesive remnant index (ARI). Methods: One-hundred-ninety-two PfT were divided into four groups (n = 48): Group 1, no surface treatment was done; Group 2, grinding was performed with a cylindrical diamond bur; Group 3, two drillings were done with a spherical diamond bur; Group 4, sandblasting was performed with 50-µm aluminum oxide. Before the experiment, half of the samples stayed immersed in distilled water at 37oC for 90 days. Brackets were bonded with Transbond XT and shear strength tests were carried out using a universal testing machine. SBS were compared by surface treatment and by ageing with two-way ANOVA, followed by Tukey’s test. ARI scores were compared between surface treatments with Kruskal-Wallis test followed by Dunn’s test. Results: Surface treatments on PfT enhanced SBS of brackets (p< 0.01), result not observed with ageing (p= 0.45). Groups II, III, and IV showed higher SBS and greater ARI than the Group 1 (p< 0.05). SBS was greater in the groups 3 and 4 (drilling, sandblasting) than in the Group 2 (grinding) (p< 0.05). SBS and ARI showed a positive correlation (Spearman’s R2= 0.57; p< 0.05). Conclusion: Surface treatment on PfT enhanced SBS of brackets, however ageing did not show any relevance. Sandblasting and drilling showed greater SBS than grinding. There was a positive correlation between SBS and ARI.


2018 ◽  
Vol 21 (4) ◽  
pp. 377
Author(s):  
Vinícius Felipe Wandscher ◽  
Luana Brondani ◽  
Gabriel Kalil Rocha Pereira ◽  
Renata Marques De Melo

<p><strong>Objective:</strong> To evaluate the bond strength of different repair treatments for composite resin to aged Y-TZP ceramics.  <strong>Material and Methods:</strong> Zirconia blocks were cut into smaller specimens, sintered according to manufacturer’s recommendations (final dimensions of 4×4×3 mm), and randomly allocated into nine groups (n=15) according to the surface treatment and presence/absence of aging of the substrate (subjected to low-temperature degradation - LTD), as follows: without LTD (Control: without treatment; TBS: tribochemical silica coating + silane + adhesive); with LTD (Control-LTD: without treatment; TBS-LTD: TBS with hydrothermal degradation; MoS-LTD: Monobond S + adhesive; MoP-LTD: Monobond Plus + adhesive; MZP-LTD: Metal/Zirconia Primer + adhesive; USB-LTD: Single Bond Universal; AP-LTD: Alloy primer + adhesive). LTD was simulated in an autoclave (134 °C, 2 bar, 5 h). The ceramic blocks were embedded in PVC cylinders with a self-curing acrylic resin; each surface treatment protocol was performed; a composite resin cylinder (Æ: 3.25 mm and height: 3 mm) was then build-up using split metallic matrices. All the specimens were aged (thermocycling + storage in water for 90 days) and subjected to the shear bond strength test using a universal testing machine (1 mm/min). The failure mode was classified into four types: adhesive, composite resin cohesive fracture, ceramic cohesive fracture, and mixed. The bond strength values were subjected to Mann–Whitney test. <strong>Results:</strong> Only air-abraded samples (TBS and TBS–LTD) survived thermocycling. More than 80% of the samples of the other groups presented pre-test failures. TBS groups presented higher values of bond strength (3.94) compared to TBS-LTD (0.96). The predominant type of failure for the surviving samples were adhesive. <strong>Conclusion:</strong> Air particle abrasion is mandatory to improve the bond strength of the Y-TZP substrate; an aged substrate presents an even more unfavorable scenario for adhesion.</p><p><strong>Keywords</strong></p><p> Dental prosthesis repair; Hydrothermal degradation; Zirconia; Shear bond strength; Sandblasting.</p><p> </p>


2019 ◽  
Author(s):  
Premkumari S. Sharma

The aim of this study is to assess the shear security quality of two intra oral clay fix frameworks on metal substrate and fired substrate and to contrast among gatherings with evaluate a superior earthenware fix framework after corrosive scratching and laser surface treatment. Therefore, 40 Nickel chromium and 40 feldspathic ceramic specimens were fabricated and divided into two main groups which were further subdivided into four subgroups based on the repair systems used and surface treatments, which had ten specimens each. Hydrofluoric acid and Erbium-doped Yttrium aluminum garnet laser were used as surface treatments and two intra oral repair systems used were Bisco and Angelus. Bonded specimens were stored in distilled water for 24 hours before being thermocycled at 5°C to 55°C for 300 cycles with a 30-second dwell time. The specimens were stored for an additional 7 days before being subjected to shear force in a universal testing machine with a 10KN load cell at a crosshead speed of 0.5 mm/min. The bond strength values obtained were recorded in MPa and analyzed using independent t test. The outcomes indicate that the shear bond strength values obtained were highly significant for Bisco when compared to Angelus for both the metal and ceramic substrates. Similarly, after acid etching and laser surface treatment, Bisco proved to be better. At the end, Bisco repair system had significantly higher shear bond strength values when compared to Angelus. Hence it is the preferred choice for intraoral repair of fractured metal ceramic restorations. Er: YAG laser surface treatment is the recommended surface treatment for intraoral repair. Available online at https://int-scientific-journals.com


2019 ◽  
Vol 13 (3) ◽  
pp. 227-233
Author(s):  
Tahereh Ghaffari ◽  
Elnaz Moslehifard ◽  
Mehrnaz Motiei

Background. Due to the fragile nature of all-ceramic restorations, it is necessary to provide an appropriate (core) infrastructure to support the veneering porcelain. The veneer detachment and chipping are disadvantages of these restorations. Several techniques have been proposed to minimize these problems. This study evaluated the effect of thermal and mechanical cycles on the shear bond strength of zirconia core to porcelain veneer under different surface treatments. Methods. Sixty disk-like zirconium samples were randomly divided into three groups. The first group was polished and veneered with porcelain, without additional surface treatments. The two other groups were subjected to different surface treatments (modified aluminum oxide by silica and activator‒aluminum oxide and primer) and veneering with porcelain. Half of the samples in each group were subjected to 6000 thermal cycles and 20,000 masticatory cycles of 50 N to imitate the intraoral conditions; the other half were placed in distilled water at 37°C until the shear strength test. Each sample was then buried using PMMA in a mounting jig so that the gap between the core and the veneer could be placed upward. Then, they were exposed to shear stress using a universal testing machine at a rate of 1 mm/min until fracture. The maximum force leading to the fracture was recorded. Results. Comparison of the groups showed that the highest shear bond strength was related to the samples treated with aluminum oxide and primer, without applying thermal and masticatory cycles, which indicated no significant difference from the group treated with aluminum oxide and primer, with thermal and masticatory cycles. The lowest shear bond strengths were related to the polished samples without surface treatment by applying thermal and masticatory cycles (P=0.001), which indicated no significant difference from the untreated group without thermal and masticatory cycles. Conclusion. Based on the results, treatment with aluminum oxide and primer increased the shear bond strength of zirconia core to porcelain veneer. Thermocycling and masticatory cycles failed to reduce the shear bond strength in all the three groups significantly.


2021 ◽  
Vol 10 (5) ◽  
pp. e20910511337
Author(s):  
Mirko Dennys Ayala Perez ◽  
Renato Pichini de Oliveira ◽  
Fernando Maeda ◽  
Walter Gomes Miranda-Jr ◽  
Angelica Castro Pimentel ◽  
...  

In order to improve the adhesion between cement and zirconia, aluminum oxide sandblasting (JAT) and Rocatec, sandblasting with silica coated aluminum oxide (ROC), also the primer Signum Zirconia Bond (SZB) were used. The objective of the study was to verify the influence of the surface treatment and the presence of SZB primer in relation to the bond strength between cement and zirconia, using 60 zirconia specimens measuring 7 mm in length, 7 mm in width and 3 mm in length. thickness. Three surface treatments were evaluated: sandblasting with pre-sintering aluminum oxide (OPre), Rocatec Soft before (RPre) and zirconia final sintering (RPos), and also, regarding the presence or not of SZB. All specimens were cemented with Panavia F. The bond strength (RU) was evaluated through a shear test with a standardization device from SDI (Southern Dental Industrie) on a universal testing machine (Kratos), with a speed of 0 , 5 mm / min. The data were evaluated using Kruskal-Wallis / Mann-Whitney (α = 0.05). Average (SD) of UK without the use of SZB: OPre: 5.5 (0.9) Ba; RPre: 4.0 (1.4) Bb; RPos: 5.0 (0.5) Bab. Average (SD) of UK using SZB: OPre: 7.9 (1.5) Aab; RPre: 6.7 (2.3) Ab; RPos: 9.0 (1.2) Aa. The use of primer increased the cement / zirconia bond strength regardless of the surface treatment performed, in addition, the Rocatec group after sintering with primer, obtained higher bond strength values ​​compared to the other study groups.


2019 ◽  
Vol 7 (3) ◽  
pp. 82
Author(s):  
Kosuke Kurahashi ◽  
Takashi Matsuda ◽  
Yuichi Ishida ◽  
Tetsuo Ichikawa

These days, new prosthodontic materials are appearing with the development of digitalization. Among these, the use of polyetheretherketone (PEEK) as the clasp of removable partial dentures has been proposed. The adhesive strength between the PEEK and acrylic resin influences the probability of denture fracture. To investigate the effect of PEEK surface treatments on the shear bond strength to acrylic resin, five surface treatment conditions of PEEK were analyzed: 1. no treatment; 2. ceramic primer application; 3. Al2O3 sandblasting; 4. Rocatec; and 5. Rocatec with ceramic primer application, comparing with a metal primer-treated Co-Cr alloy. Two kinds of autopolymerizing resin (Unifast II and Palapress Vario) were used as bonding materials. The specimens were evaluated to determine the bond strength. Rocatec treatment with ceramic primer application yielded the highest bond strengths (12.71 MPa and 15.32 MPa, respectively, for Unifast II and Palapress Vario). When compared to a metal primer-treated Co-Cr alloy, the bond strength of PEEK to Unifast II was similar, whereas it was about 60% of that to Palapress Vario. Rocatec treatment, combined with ceramic primer, showed the highest bond strength of PEEK to acrylic resin. Treatment of PEEK will enable its use as the clasp of removable dentures and the fixation of PEEK prostheses.


2013 ◽  
Vol 38 (3) ◽  
pp. E58-E66 ◽  
Author(s):  
SD Cho ◽  
P Rajitrangson ◽  
BA Matis ◽  
JA Platt

SUMMARY Aged resin composites have a limited number of carbon-carbon double bonds to adhere to a new layer of resin. Study objectives were to 1) evaluate various surface treatments on repaired shear bond strength between aged and new resin composites and 2) to assess the influence of a silane coupling agent after surface treatments. Methods Eighty disk-shape resin composite specimens were fabricated and thermocycled 5000 times prior to surface treatment. Specimens were randomly assigned to one of the three surface treatment groups (n=20): 1) air abrasion with 50-μm aluminum oxide, 2) tribochemical silica coating (CoJet), or 3) Er,Cr:YSGG (erbium, chromium: yttrium-scandium-gallium-garnet) laser or to a no-treatment control group (n=20). Specimens were etched with 35% phosphoric acid, rinsed, and dried. Each group was divided into two subgroups (n=10): A) no silanization and B) with silanization. The adhesive agent was applied and new resin composite was bonded to each conditioned surface. Shear bond strength was evaluated and data analyzed using two-way analysis of variance (ANOVA). Results Air abrasion with 50-μm aluminum oxide showed significantly higher repair bond strength than the Er,Cr:YSGG laser and control groups. Air abrasion with 50-μm aluminum oxide was not significantly different from tribochemical silica coating. Tribochemical silica coating had significantly higher repair bond strength than Er,Cr:YSGG laser and the control. Er,Cr:YSGG laser and the control did not have significantly different repair bond strengths. Silanization had no influence on repair bond strength for any of the surface treatment methods. Conclusion Air abrasion with 50-μm aluminum oxide and tribochemical silica followed by the application of bonding agent provided the highest repair shear bond strength values, suggesting that they might be adequate methods to improve the quality of repairs of resin composites.


2014 ◽  
Vol 08 (04) ◽  
pp. 498-503 ◽  
Author(s):  
Lucas da Fonseca Roberti Garcia ◽  
Hebert Luis Rossetto ◽  
Fernanda de Carvalho Panzeri Pires-de-Souza

ABSTRACT Objective: To evaluate the shear bond strength of a novel calcium aluminate-based cement, EndoBinder (EB), to dentine in comparison with Grey and White Mineral Trioxide Aggregate (MTA). Materials and Methods: Root canal hemi-sections obtained from 30 extracted molar teeth were embedded in self-polymerized acrylic resin and were grounded wet in order to obtain a flat dentine surface. Next, the roots were randomly assigned into three groups (n = 10), according to the cement used, as follows: EB: EndoBinder; WMTA: White MTA and GMTA: Grey MTA. The shear bond strength test was performed using a Universal Testing Machine (0.5 mm/min) and the data were submitted to statistical analysis (1-way ANOVA and Tukey tests, P < 0.05). Results: EB presented the highest shear bond strength values; however, there was no statistically significant difference in comparison with GMTA (P > 0.05). WMTA presented the lowest mean values, which were significant in comparison with EB (P < 0.05). Conclusions: The novel calcium aluminate-based cement presented higher shear bond strength than WMTA, and should be considered as a promising alternative in endodontic therapy.


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