Compression behavior of TiB2-particulate-reinforced composites of Al22Fe3Ti8

1991 ◽  
Vol 6 (3) ◽  
pp. 530-538 ◽  
Author(s):  
M.S. DiPietro ◽  
K.S. Kumar ◽  
J.D. Whittenberger

The compression behavior of both the monolithic L12 compound Al22Fe3Ti8 and discontinuous composites obtained by incorporating ∼1 μm TiB2 particles was studied for various volume percent reinforcements as a function of temperature and at high temperatures as a function of strain rate. In this study, by varying the Fe and Ti contents, the nature and volume fraction of the minor phases coexisting with the dominant L12 phase were changed and were examined with and without TiB2 reinforcement. At high strain rates (10−4 s−1), the TiB2 reinforcements significantly enhance ambient and warm-temperature strength, although a crossover is observed at ∼1000 K, above which the monolithic material is stronger than the composite. At slow strain rates (10−7 s−1), representative of creep conditions, however, the TiB2-containing composites retain their superiority at least up to 1200 K. Power law fits of compressive flow stress at 1% strain versus strain rate yielded a stress exponent of ∼3.0 with an activation energy of 310 kJ/mol for the monolithic material. For the particulate composites (20 vol. % TiB2), the corresponding values were ∼5.0 and 465 kJ/mol, suggesting a change in the dominant deformation mechanism.

1990 ◽  
Vol 213 ◽  
Author(s):  
K.S. Kumar ◽  
M.S. Dipietro ◽  
J.D. Whittenberger

ABSTRACTCompression studies were conducted on monolithic and TiB2 particulatereinforced composites of AI22 Fe3 Ti8, both with and without minor quaternary alloying additions (2 at.% Nb and 2 at.% Mn) as a function of temperature and as a function of strain rate at high temperature. The volume fraction of reinforcement was varied between 0 and 20 percent. The particulate reinforcements were found to be effective in increasing ambient- and warm-temperature strength; at high temperatures, the monolithic material is stronger than the composites, although the composites are superior at slow strain rates. The microstructures of the monolithic and composite specimens were examined before and after deformation to explain these observations.


2014 ◽  
Vol 626 ◽  
pp. 353-358
Author(s):  
Geun Su Joo ◽  
Min Kuk Choi ◽  
Hoon Huh

The tension/compression hardening behavior is important in sheet metal forming processes because of complicated loading paths. Experimental methods to measure the tension/ compression behavior have not considered the effect of the strain rate although the strain rate is related to the hardening behavior of sheet metal. The tension/compression tests need to be conducted considering the strain rate to acquire accurate hardening behavior.This paper deals with an experimental technique to measure the tension/compression behavior of sheet metal at various strain rates. A new clamping device was developed to prevent a sheet specimen from buckling under compression loading condition. Compared to previous clamping devices, the clamping device was devised to uniformly impose a clamping force and easily measure the strain from side of a specimen. Tension/compression tests have been conducted at various strain rates for SPCC and DP590 with displacement of 10%. Hardening curves under the tension or compression loading condition were obtained and analyzed with respect to the strain rate.


1991 ◽  
Vol 113 (4) ◽  
pp. 475-484 ◽  
Author(s):  
K. P. Jen ◽  
J. N. Majerus

This paper presents the evaluation of the stress-strain behavior, as a function of strain-rate, for three tin-lead solders at room temperature. This behavior is critically needed for reliability analysis of printed circuit boards (PCB) since handbooks list minimal mechanical properties for the eutectic solder used in PCBs. Furthermore, most handbook data are for stable eutectic microstructure whereas PCB solder has a metastable microstructure. All three materials were purchased as “eutectics.” However, chemical analysis, volume fraction determination, and microhardness tests show some major variations between the three materials. Two of the materials have a eutectic composition, and one does not. The true stress-strain equations of one eutectic and the one noneutectic material are determined from compressive tests at engineering strain-rates between 0.0002/s and 0.2/s. The second eutectic material is evaluated using tensile tests with strain-rates between 0.00017/s and 0.042/s. The materials appear to exhibit linear elastic behavior only at extremely small strains, i.e., less than 0.0005. However, this “elastic” behavior showed considerable variation, and depended upon the strain rate. In both tension and compression the eutectic alloy exhibits nonlinear plastic behavior, i.e., strain-softening followed by strain-hardening, which depends upon the strain rate. A quadratic equation σy = σy(ε˚/ε˚0) + A(ε˚/ε˚0)ε + B(ε˚/ε˚0)ε2 fit to the data gives correlation coefficients R2 > 0.91. The coefficients σy(ε˚/ε˚0), A(ε˚/ε˚0), B(ε˚/ε˚0) are fitted functions of the normalized engineering strain rate ε˚/ε˚0. Replicated experiments are used at each strain-rate so that a measure of the statistical variation could be estimated. Measures of error associated with the regression analysis are also obtained so that an estimate of the total error in the stress-strain relations can be made.


2010 ◽  
Vol 638-642 ◽  
pp. 3616-3621 ◽  
Author(s):  
K.P. Rao ◽  
Y.V.R.K. Prasad ◽  
Norbert Hort ◽  
Karl Ulrich Kainer

The hot working behavior of Mg-3Sn-2Ca alloy has been investigated in the temperature range 300–500 oC and strain rate range 0.0003–10 s-1, with a view to evaluate the mechanisms and optimum parameters of hot working. For this purpose, a processing map has been developed on the basis of the flow stress data obtained from compression tests. The stress-strain curves exhibited steady state behavior at strain rates lower than 0.01 s-1 and at temperatures higher than 350 oC and flow softening occurred at higher strain rates. The processing map exhibited two dynamic recrystallization domains in the temperature and strain rate ranges: (1) 300–420 oC and 0.0003–0.003 s-1, and (2) 420–500 oC and 0.003–1.0 s-1, the latter one being useful for commercial hot working. Kinetic analysis yielded apparent activation energy values of 161 and 175 kJ/mole in domains (1) and (2) respectively. These values are higher than that for self-diffusion in magnesium suggesting that the large volume fraction of intermetallic particles CaMgSn present in the matrix generates considerable back stress. The processing map reveals a wide regime of flow instability which gets reduced with increase in temperature or decrease in strain rate.


2015 ◽  
Vol 825-826 ◽  
pp. 182-188 ◽  
Author(s):  
Lutz Krüger ◽  
Steffen Grützner ◽  
Sabine Decker ◽  
Ines Schneider

Composite materials, which consist of a metastable austenitic TRIP-steel matrix (CrMnNi TRIPsteel; TRansformation Induced Plasticity) reinforced by alumina particles (25 vol.% ceramic, designated as AT 25/75) and reinforced by alumina and MgO partially stabilized zirconia particles (Mg-PSZ) (35 vol.% ceramic, designated as AT 25/75 + MgPSZ) were synthesized through spark plasma sintering (SPS). In the AT 25/75 + MgPSZ, the steel particles were mainly surrounded by alumina. Hence, mostly steel/alumina and alumina/MgPSZ interfaces existed. The mechanical behavior of the as-sintered samples was characterized by compression tests at room temperature and 40 °C and in a range of strain rates between 103s-1and 103s1. The influence of the ceramic content, strain rate and temperature on TRIP-effect of the steel matrix was investigated. Due to the increasing ceramic volume fraction, AT 25/75 + MgPSZ exhibits the highest compressive yield strength under all loading conditions and no strain rate sensitivity. This composite showed no measurable TRIP-effect, due to the low fracture strain. The deformation-induced α’martensite within the steel particles in pure steel and AT 25/75 primary depends on the testing temperature and the strain rate. This is attributed to an increase of stacking fault energy with rising temperature. High strain rates cause adiabatic heating, counteracting the martensitic transformation.


2017 ◽  
Vol 898 ◽  
pp. 137-143
Author(s):  
Lin Xiang ◽  
Bin Tang ◽  
Hong Chao Kou ◽  
Jie Shao ◽  
Jin Shan Li

Isothermal compression tests were conducted to investigate the effect of hot deformation parameters on flow behavior and microstructure of Ti-6Al-4V-0.2O alloy. The experimental results show that the strain rate and height reduction have little effect on the volume fraction of primary α at a deformation temperature of 860 ̊C. At a deformation temperature of 940 ̊C, the volume fraction of primary α at a high strain rate (10s-1) is about 10% less than that at low strain rates (0.01s-1~1s-1). It may be one of the reasons for the significantly discontinuous yielding phenomenon. Another reason is that the dislocation density decreased suddenly due to the dynamic recovery. With the increasing strain rate and the decreasing deformation temperature, the volume fraction of irregular secondary α increases and lamellar secondary α decreases. And with height reduction increasing, the irregular secondary α increases firstly and then tends to be steady because of dynamic recovery and recrystallization.


2015 ◽  
Vol 798 ◽  
pp. 357-361 ◽  
Author(s):  
Haris A. Khan ◽  
Mehr Nigar ◽  
Imran Ali Chaudhry

This paper focuses on progressive damage investigation and failure analysis of carbon fiber reinforced laminates under varying strain rates in tensile mode. Samples specimen prepared for experiments were made from unidirectional ply with 70/30 fiber-matrix volume fraction and cross-ply (0°-90°) balanced stacking. These laminates were subjected to uniaxial longitudinal tensile loading in a Universal Testing Machine (UTM) with varying strain rates. Results acquired from the experiments were used to plot stress versus strain curves for different strain rates. These plots were subsequently analyzed to investigate the effect of varying loading rates on the mechanical properties and failure behavior of these composites. Experimental data revealed a considerable increase in the tensile strength with increasing strain rate. The tensile modulus and strain to failure were also found to exhibit slight increase with the increasing strain rate.


Author(s):  
Siu Wing Or ◽  
Geoffrey P. McKnight ◽  
Nersesse Nersessian ◽  
Gregory P. Carman

This paper describes the effect of particulate crystallographic orientation on the dynamic magnetomechanical properties of Terfenol-D/epoxy 1–3 magnetostrictive particulate composites. Two different types of composites with approximately 50% Terfenol-D volume fraction were fabricated for comparison with [112]-textured monolithic Terfenol-D. In the first type, needle-shaped, [112]-oriented particles cut from the monolithic Terfenol-D were used and in the second type, irregular-shaped, randomly oriented particles ball-milled from the monolithic material were employed. Elastic moduli (E33H and E33B), dynamic strain coefficient (d33), and magnetomechanical coupling coefficient (k33) were investigated as a function of bias field. Both composites demonstrate similar property trends with the negative-ΔE, d33, and k33 values maximizing near 30 kA/m. The maximum values achieved in the oriented type are up to 67% larger than the non-oriented type and approaches 65% of the monolithic Terfenol-D. The property improvement in the oriented type is shown to be attributed to [112] preferential particulate orientation.


Author(s):  
J. L. Jordan ◽  
J. E. Spowart ◽  
M. J. Kendall ◽  
B. Woodworth ◽  
C. R. Siviour

Whether used as structural components in design or matrix materials for composites, the mechanical properties of polymers are increasingly important. The compressive response of extruded polymethyl methacrylate (PMMA) rod with aligned polymer chains and Al–Ni–PMMA particulate composites are investigated across a range of strain rates and temperatures. The particulate composites were prepared using an injection-moulding technique resulting in highly anisotropic microstructures. The mechanics of these materials are discussed in the light of theories of deformation for glassy polymers. The experimental data from this study are compared with PMMA results from the literature as well as epoxy-based composites with identical particulates. The PMMA exhibited the expected strain rate and temperature dependence and brittle failure was observed at the highest strain rates and lowest temperatures. The Al–Ni–PMMA composites were found to have similar stress–strain response to the PMMA with reduced strain softening after yield. Increasing volume fraction of particulates in the composite resulted in decreased strength.


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