A two-powder process for Bi-2223 precursors

1996 ◽  
Vol 11 (1) ◽  
pp. 28-38 ◽  
Author(s):  
T. G. Holesinger ◽  
K. V. Salazar ◽  
D. S. Phillips ◽  
B. L. Sargent ◽  
J. K. Bremser ◽  
...  

A two-powder process is described for the production of uniform, fine-grained Bi2Sr2Ca2Cu3Oy (Bi-2223) powders. One powder is the Bi2.1−xPbxSr1.9−yCayOz (2:2 Cu-free) phase. The other is a multi-phase powder of approximate overall composition SrCaCu3Oy. The 2:2 Cu-free is one of the first Bi-containing phases to form from a nominal Bi-2223 mixture of oxides and carbonates. This precursor route was chosen for investigation because (1) the powders have very similar particle morphologies and (2) the mixing volumes are closely matched. Both of these characteristics facilitate the milling and blending process. This precursor mix was found to be stable in that explosive grain growth of undesirable phases was not observed during sintering. Critical current densities up to 26,900 A/cm2 in self field at 75 K were obtained in tapes.

1989 ◽  
Vol 4 (3) ◽  
pp. 526-529 ◽  
Author(s):  
Mireille Treuil Clapp ◽  
Zhang Jian ◽  
Tariq Manzur

Alloys of Nb73Al12Si14.5B0.5 were rapidly solidified into amorphous ribbons using the melt spinning technique. These were isothermally annealed at temperatures ranging from 660 to 780 °C. The A15 phase began to crystallize at 700 °C and small amounts of second phases appeared at the higher temperatures. Crystallization was dependent on quenching rate as well as annealing conditions. Below 750 °C nucleation was nonuniform and was enhanced by surfaces and quenched-in nuclei. Above 750 °C nucleation became more uniform and completely crystalline ribbons with equiaxed grains ∼30 nm in diameter were obtained. These ultra fine grained ribbons had extremely high superconducting critical current densities of 8 × 1010 A/m2 and 5 × 1010 A/m2 at magnetic fields of 0.5 and 15 tesla, respectively, at 4.2 K.


1989 ◽  
Vol 03 (14) ◽  
pp. 1053-1060 ◽  
Author(s):  
A. J. BOURDILLON ◽  
N. X. TAN ◽  
N. SAVVIDES ◽  
J. SHARP

Texture growth in incongruently melting ceramic superconductor materials, such as YBa 2 Cu 3 O 7−x, can be combined with zone refinement in thermal gradients to increase critical current densities. In gravity aided texture growth (GATEG), a vertical thermal gradient is used with downward motion of the partially molten specimen (relative to the furnace) so that the molten phase recrystallizes with grain growth.


1992 ◽  
Vol 7 (11) ◽  
pp. 2956-2961 ◽  
Author(s):  
L.S. Hung

Bi2Sr2CaCu2O8+x films were prepared by mixing 2-ethylhexanoate precursors with heptafluorobutyric acid and annealing at 820 °C in dry ambient. The films underwent substantial mass transport and exhibited abnormal grain growth, indicating that some liquid phases might be involved in the process. It was found that the high atomic mobilities during annealing significantly improved in-plane orientations and consequently increased critical current densities.


1989 ◽  
Vol 169 ◽  
Author(s):  
N. X. Tan ◽  
A. J. Bourdillon ◽  
N. Sawides

AbstractTexture growth in incongruently melting ceramic superconductor materials, such as YBa2Cu3O7‐χ can be combined with zone refinement in thermal gradients to increase critical current densities. In gravity aided texture growth (GATEG), a vertical thermal gradient is used with downward motion of the partially molten specimen (relative to the furnace) so that the molten phase recrystallizes with grain growth. The oxidation features of Y‐Ba‐Cu‐0 and Bi‐Sr‐Ca‐Cu‐0 can be explained by Madelung potentials.


Author(s):  
I-Fei Tsu ◽  
D.L. Kaiser ◽  
S.E. Babcock

A current theme in the study of the critical current density behavior of YBa2Cu3O7-δ (YBCO) grain boundaries is that their electromagnetic properties are heterogeneous on various length scales ranging from 10s of microns to ˜ 1 Å. Recently, combined electromagnetic and TEM studies on four flux-grown bicrystals have demonstrated a direct correlation between the length scale of the boundaries’ saw-tooth facet configurations and the apparent length scale of the electrical heterogeneity. In that work, enhanced critical current densities are observed at applied fields where the facet period is commensurate with the spacing of the Abrikosov flux vortices which must be pinned if higher critical current density values are recorded. To understand the microstructural origin of the flux pinning, the grain boundary topography and grain boundary dislocation (GBD) network structure of [001] tilt YBCO bicrystals were studied by TEM and HRTEM.


2021 ◽  
Vol 7 (1) ◽  
pp. 4
Author(s):  
Katsuya Hirota ◽  
Tomoko Ariga ◽  
Masahiro Hino ◽  
Go Ichikawa ◽  
Shinsuke Kawasaki ◽  
...  

A neutron detector using a fine-grained nuclear emulsion has a sub-micron spatial resolution and thus has potential to be applied as high-resolution neutron imaging. In this paper, we present two approaches to applying the emulsion detectors for neutron imaging. One is using a track analysis to derive the reaction points for high resolution. From an image obtained with a 9 μm pitch Gd grating with cold neutrons, periodic peak with a standard deviation of 1.3 μm was observed. The other is an approach without a track analysis for high-density irradiation. An internal structure of a crystal oscillator chip, with a scale of approximately 30 μm, was able to be observed after an image analysis.


Author(s):  
Hezhen Hu ◽  
Wengang Zhou ◽  
Junfu Pu ◽  
Houqiang Li

Sign language recognition (SLR) is a challenging problem, involving complex manual features (i.e., hand gestures) and fine-grained non-manual features (NMFs) (i.e., facial expression, mouth shapes, etc .). Although manual features are dominant, non-manual features also play an important role in the expression of a sign word. Specifically, many sign words convey different meanings due to non-manual features, even though they share the same hand gestures. This ambiguity introduces great challenges in the recognition of sign words. To tackle the above issue, we propose a simple yet effective architecture called Global-Local Enhancement Network (GLE-Net), including two mutually promoted streams toward different crucial aspects of SLR. Of the two streams, one captures the global contextual relationship, while the other stream captures the discriminative fine-grained cues. Moreover, due to the lack of datasets explicitly focusing on this kind of feature, we introduce the first non-manual-feature-aware isolated Chinese sign language dataset (NMFs-CSL) with a total vocabulary size of 1,067 sign words in daily life. Extensive experiments on NMFs-CSL and SLR500 datasets demonstrate the effectiveness of our method.


2006 ◽  
Vol 89 (13) ◽  
pp. 132510 ◽  
Author(s):  
Xianping Zhang ◽  
Zhaoshun Gao ◽  
Dongliang Wang ◽  
Zhengguang Yu ◽  
Yanwei Ma ◽  
...  

1874 ◽  
Vol 1 (1) ◽  
pp. 1-2
Author(s):  
Edward Hull

This granite forms an isolated mass, rising into two eminences a few miles south of Louisburg, called Corvock Brack (1287 feet) and Knockaskeheen (1288 feet). It is a greyish granite—generally fine—grained—consisting of quartz, two felspars,—one orthoclase, the other triclinic, probably oligoclase—and dark green mica. In some places there are patches in which the felspar assumes the appearance of “graphic granite.” Numerous boulders of this granite are strewn over the district to the north-west, and on the south side of Knockaskeheen; the rock is traversed by regular joints ranging N. 10 W., along which it splits off into nearly vertical walls. The position of the granite is shown on Griffith's Geological Map of Ireland, and it is surrounded by schistose beds, generally metamorphosed, and probably of Lower Silurian age. The granite itself is of older date than the Upper Llandovery beds, which lie to the southward.


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