In Situ Straining Tem Observation of Fracture behavior in Pst Crystals of TiAl

1994 ◽  
Vol 364 ◽  
Author(s):  
Mingwei Chen ◽  
Da Chen ◽  
Dongliang Lin

AbstractCrack propagation process in TiAl alloy PST crystal has been investigated by in situ straining TEM observation. It has been found that the influence of lamellar boundaries on the fracture behaviors is connected with the types of interfaces (twin, pseudo-twin and α2/γ interfaces). Even though secondary microcracks always nucleate at α2/γ interfaces due to stress concentration, the crack growth is cleavage in α2 and γ phases rather than along interlamellae. When a crack meet γ/γ interfaces, its propagation can be inhibited and crack tips blunt by the slide of the interfaces. It also deserves to be mentioned that ductility of PST crystals has connection with the rate of crack propagation..

1998 ◽  
Vol 554 ◽  
Author(s):  
J. A. Horton ◽  
J. L. Wright ◽  
J. H. Schneibel

AbstractThe fracture behavior of a Zr-based bulk amorphous alloy, Zr-10 Al-5 Ti-17.9 Cu-14.6Ni (at.%), was examined by transmission electron microscopy (TEM) and x-ray diffraction forany evidence of crystallization preceding crack propagation. No evidence for crystallizationwas found in shear bands in compression specimens or at the fracture surface in tensile specimens.In- situ TEM deformation experiments were performed to more closely examine actualcrack tip regions. During the in-situ deformation experiment, controlled crack growth occurredto the point where the specimen was approximately 20 μm thick at which point uncontrolledcrack growth occurred. No evidence of any crystallization was found at the crack tips or thecrack flanks. Subsequent scanning microscope examination showed that the uncontrolledcrack growth region exhibited ridges and veins that appeared to have resulted from melting. Performing the deformations, both bulk and in-situ TEM, at liquid nitrogen temperatures (LN2) resulted in an increase in the amount of controlled crack growth. The surface roughness of the bulk regions fractured at LN2 temperatures corresponded with the roughness of the crack propagation observed during the in-situ TEM experiment, suggesting that the smooth-appearing room temperature fracture surfaces may also be a result of localized melting.


1980 ◽  
Vol 102 (4) ◽  
pp. 347-349 ◽  
Author(s):  
R. Pilkington ◽  
E. Smith

The paper presents an outline model for creep crack growth under LEFM conditions. The incremental nature of the crack propagation process is taken into account, and a theoretical analysis shows that the relation between crack tip stress intensification and crack growth rate is not unique.


2014 ◽  
Vol 513-517 ◽  
pp. 20-23
Author(s):  
Hai Chao Wang ◽  
Xue Hua Wang ◽  
Xue Hui An

The different fracture characteristics of self-compacting rock-filled concrete with large-size natural and recycled aggregate are analyzed by three-point bending experiment. According to the analysis of the crack propagation process, the fracture mechanism differences of self-compacting rock-filled concrete with large-size natural and recycled aggregate are discussed. The further analysis of the differences of fracture toughness, fracture energy, and are gain


Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Masato Hoshino ◽  
...  

Recently, due to the increasing heat density of printed circuit boards (PCBs), thermal fatigue damage in the joints has exerted a more significant influence on the reliability of electronic components. Accordingly, the development of a new nondestructive inspection technology is strongly desired by related industries. The authors have applied a synchrotron radiation X-ray micro-tomography system to the nondestructive observation of micro-cracks. However, the reconstruction of CT images is difficult for planar objects such as PCB substrates, due to insufficient X-ray transmission in the direction parallel to the substrates. In order to solve this problem, a synchrotron radiation laminography system was developed to relax size restrictions on the observation samples, and was applied to the three-dimensional nondestructive evaluation of several kinds of solder joints, which were loaded under accelerated thermal cyclic conditions via thermal shock tests. Moreover, the thermal fatigue crack propagation process that occurs under actual PCB energization loading conditions will differ from that under the usual acceleration test conditions. In this work, the possibility of in-situ monitoring of the thermal fatigue crack propagation process using the laminography system was investigated at die-attached joints subjected to cyclic energization loading, which is close to the actual usage conditions of PCBs. The optical system developed for use in the laminography system was constructed to provide a rotation stage with a tilt from the horizontally incident X-ray beam, and to obtain X-ray projection images via a beam monitor. In this manner, the X-ray beam is sufficiently transmitted through the planar specimen in all projections. The observed specimens included several die-attached joints, in which 3 mm square ceramic dies had been mounted on a 40 mm square FR-4 substrate using Sn-3.0wt%Ag-0.5wt%Cu solder. Consequently, the laminography system was successfully applied to the in-situ monitoring of thermal fatigue cracks that appeared in the solder layer under cyclic energization. This was possible because the laminography images obtained in the energization state have a quality that is equivalent to those obtained in a non-energized state, provided that the temperature distribution of the specimen is stable. In addition, the fatigue crack propagation process can be quantitatively evaluated by measuring the crack surface area and calculating the average crack propagation rate. However, in some cases, the appearance of thermal fatigue cracks was not observed in a solder layer that had been loaded by the accelerated thermal cycle test. This result strongly suggests that delamination occurred at the interface, which indicates that the corresponding fracture mode was significantly influenced by the type of thermal loading.


2007 ◽  
Vol 2007.7 (0) ◽  
pp. 221-222
Author(s):  
Hiroyuki Tsuritani ◽  
Toshihiko Sayama ◽  
Yoshiyuki Okamoto ◽  
Takeshi Takayanagi ◽  
Kentaro Uesugi ◽  
...  

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