Microstructural Evolution of Radiation Induced Defects In ZnO During Isochronal Annealing

1998 ◽  
Vol 540 ◽  
Author(s):  
S. Brunner ◽  
W. Puff ◽  
P. Mascher ◽  
A.G. Balogh
Keyword(s):  
Room Temperature ◽  
Proton Irradiation ◽  
Positron Lifetime ◽  
Thermal Evolution ◽  
Isochronal Annealing ◽  
Doppler Broadening ◽  
Thermal Dependence ◽  
Radiation Induced ◽  
Induced Defects ◽  
Mev Protons

AbstractIn this study we discuss the microstructural changes after electron and proton irradiation and the thermal evolution of the radiation induced defects during isochronal annealing. The nominally undoped samples were irradiated either with 3 MeV protons to a fluence of 1.2× 1018 p/cm2 or with 1 MeV electrons to a fluence of 1×1018 e/cm2. The investigation was performed with positron lifetime and Doppler-broadening measurements. The measurements were done at room temperature and in some cases down to 10 K to investigate the thermal dependence of the trapping characteristics of the positrons.

Radiation-Induced Defects in Electron and Proton Irradiated ZnS

1998 ◽  
Vol 540 ◽  
Author(s):  
S. Brunner ◽  
W. Puff ◽  
P. Mascher ◽  
A.G. Balogh
Keyword(s):  
Vapour Deposition ◽  
Proton Irradiation ◽  
Positron Lifetime ◽  
Chemical Vapour ◽  
Isochronal Annealing ◽  
Doppler Broadening ◽  
Defect Complexes ◽  
Radiation Induced ◽  
The Stability ◽  
Induced Defects

AbstractIn this contribution, we present a study aimed at investigating the microstructural changes of ZnS single crystals and CVD (chemical vapour deposition) grown crystals after electron and proton irradiation. Positron lifetime and Doppler-broadening measurements were performed to investigate the stability of the radiation induced defects and possible clustering mechanisms during isochronal annealing. After electron as well as proton irradiation the significant changes in the annihilation characteristics are indications of radiation induced open-volume-type defects. It is found that electron and proton irradiation causes different changes in the positron annihilation characteristics. After electron irradiation a significant defect component is observed which can be attributed to the annihilation in monovacancies. During isochronal annealing agglomerations to divacancy-type defects take place. Proton irradiation reveals a significantly different defect structure. Isochronal annealing causes agglomerations to larger defect complexes. The observed annealing stages are indications of the annealing of variously sized vacancy complexes.

Vacancy-Type Defects in Electron and Proton Irradiated II-VI Compounds

1998 ◽  
Vol 510 ◽  
Author(s):  
S. Brunner ◽  
W. Puff ◽  
P. Mascher ◽  
A.G. Balogh
Keyword(s):  
Band Gap ◽  
Proton Irradiation ◽  
Positron Lifetime ◽  
Wide Band ◽  
Compound Semiconductors ◽  
Doppler Broadening ◽  
Wide Band Gap ◽  
Radiation Induced ◽  
Induced Defects ◽  
Mev Protons

AbstractIn this contribution we present a study aimed at comparing results of positron-lifetime and Doppler-broadening measurements on the wide-band-gap compound semiconductors ZnS, ZnSe, and ZnTe. To investigate the basic properties of intrinsic and radiation induced defects the samples were irradiated either with 3 MeV protons or 1 MeV electrons. The isochronal annealing was performed in an Ar atmosphere. It was found that electron and proton irradiation cause different changes in the positron annihilation characteristics. Several annealing stages were observed, related to the annealing of variously sized vacancy complexes.

Proton Irradiation Induced Defects in 611- and 4H-SiC

1998 ◽  
Vol 540 ◽  
Author(s):  
Werner Puff ◽  
Adam G. Balogh ◽  
Peter Mascher
Keyword(s):  
Proton Irradiation ◽  
Positron Lifetime ◽  
Doppler Broadening ◽  
Defect Complexes ◽  
Radiation Induced ◽  
Positron Lifetime Spectroscopy ◽  
Induced Defects ◽  
Irradiation Induced Defects ◽  
Type Sample

AbstractAnnealing of defects in proton irradiated bulk n-type 6H- and semi-insulating 4H-SiC has been investigated by positron lifetime spectroscopy and Doppler-broadening measurements. For the n-type sample radiation induced defects in dependence of the proton fluence were studied. Three or four annealing stages were found, during which the formation of larger defect complexes could be observed.

An Investigation of Point Defects in NiAl Using Positron Annihilation Techniques

1998 ◽  
Vol 552 ◽  
Author(s):  
Werner Puff ◽  
Bernd Logar ◽  
Adam G. Balogh
Keyword(s):  
Positron Annihilation ◽  
Point Defects ◽  
Proton Irradiation ◽  
Positron Lifetime ◽  
Composition Range ◽  
Isochronal Annealing ◽  
Doppler Broadening ◽  
Positron Lifetime Spectroscopy ◽  
Induced Defects

ABSTRACTVacancy-like defects in NiAl in the composition range 47 at.-% < CNi < 53 at.-% are investigated by means of positron lifetime spectroscopy and Doppler-broadening measurements. The observed lifetimes in the annealed samples confirm that defects are quenched-in during the production of the samples. Isochronal annealing of samples quenched at 1600°C and after proton irradiation show that the induced defects are quite different.

Studies of Defects in ZnO by Positron Annihilation

1995 ◽  
Vol 378 ◽  
Author(s):  
Werner Puff ◽  
Sebastian Brunner ◽  
Peter Mascher ◽  
Adam G. Balogh
Keyword(s):  
Positron Annihilation ◽  
Colour Change ◽  
Doppler Broadening ◽  
Positron Annihilation Lifetime ◽  
Dark Orange ◽  
Radiation Induced ◽  
Induced Defects ◽  
Annealing Experiments ◽  
Mev Protons ◽  
Yellowish White

AbstractIn order to investigate the basic properties of radiation-induced defects in ZnO crystals, positron annihilation lifetime and Doppler-broadening measurements were performed on crystals sinterd for 18 hours at 1200 °C and irradiated with 3 MeV protons at 223 K. The irradiation induced a colour change of the specimens from the original yellowish-white to dark orange or even brown. Isochronal annealing experiments showed three annealing stages, centred at about 150 °C, 500 – 550 °C, and 750 °C, respectively. These stages are related to the annealing of variously sized vacancy complexes.

Vacancy-Type Defects in as-Grown and Proton-Irradiated 6H-SiC

1998 ◽  
Vol 512 ◽  
Author(s):  
Werner Puff ◽  
Peter Mascher ◽  
Adam G. Balogh
Keyword(s):  
Positron Lifetime ◽  
Doppler Broadening ◽  
Defect Complexes ◽  
Radiation Induced ◽  
Positron Lifetime Spectroscopy ◽  
P Type ◽  
Induced Defects

ABSTRACTAnnealing of defects in as-grown and proton irradiated bulk n- and p-type 6H-SiC has been investigated by positron lifetime spectroscopy and Doppler-broadening measurements. The grown-in defects do not anneal out until 1600 °C, whereas the radiation induced defects show three main annealing stages well below this temperature. During annealing, the formation of larger defect complexes can be observed.

Vacancy-Type Defects in Electron and Proton Irradiated II- VI Compounds

1996 ◽  
Vol 439 ◽  
Author(s):  
S. Brunner ◽  
W. Puff ◽  
P. Mascher ◽  
A. G. Balogh ◽  
H. Baumann
Keyword(s):  
Positron Annihilation ◽  
Proton Irradiation ◽  
Basic Properties ◽  
Radiation Induced ◽  
Induced Defects ◽  
Mev Protons

AbstractIn this contribution, we present a study aimed at investigating the basic properties of radiation induced defects in ZnS and ZnO and the influence of the atmosphere on the annealing characteristics of the defects. Positron annihilation experiments (both lifetime and Dopplerbroadening measurements) were performed on both single- and polycrystalline samples, irradiated with 3 MeV protons or 1 MeV electrons. For ZnS it was found that both electron and proton irradiation caused significant changes in the positron annihilation characteristics. The annealing of proton irradiated ZnS in air leads to significant oxidation and eventual transformation into ZnO.

A positron study of plastic deformation of silicon

1983 ◽  
Vol 61 (3) ◽  
pp. 451-459 ◽  
Author(s):  
S. Dannefaer ◽  
N. Fruensgaard ◽  
S. Kupca ◽  
B. Hogg ◽  
D. Kerr
Keyword(s):  
Plastic Deformation ◽  
Room Temperature ◽  
Functional Form ◽  
Isothermal Annealing ◽  
Positron Lifetime ◽  
Activation Enthalpy ◽  
Isochronal Annealing ◽  
Doppler Broadening ◽  
Trapping Rate ◽  
Vacancy Clusters

Positron lifetime and Doppler broadening experiments have been conducted in silicon which was subjected to various degrees of plastic deformation. With increasing plastic deformation (from 2.5 to 38%) the trapping rate per unit dislocation concentration decreased from about 8 × 1015 to 4.5 × 1015 s−1 as measured at room temperature. Two annealing stages were identified by isochronal annealing, one of which had an activation enthalpy of 3.2 to 3.8 eV as determined by isothermal annealing. Measurements in the temperature range 15 to 673 K show that the positron annihiliation parameters (lifetimes, intensities, and S-parameters) depend strongly on temperature and that the functional form of these dependencies is related to the state of annealing of the deformed samples. These results are disscussed in terms of the presence of vacancy clusters and dislocations, and evidence is presented indicating the existence of the hexavacancy.

Vacancy-Type Defects in Electron and Proton Irradiated II- VI Compounds

1996 ◽  
Vol 438 ◽  
Author(s):  
S. Brunner ◽  
W. Puff ◽  
P. Mascher ◽  
A. G. Balogh ◽  
H. Baumann
Keyword(s):  
Positron Annihilation ◽  
Proton Irradiation ◽  
Basic Properties ◽  
Radiation Induced ◽  
Induced Defects ◽  
Mev Protons

AbstractIn this contribution, we present a study aimed at investigating the basic properties of radiation induced defects in ZnS and ZnO and the influence of the atmosphere on the annealing characteristics of the defects. Positron annihilation experiments (both lifetime and Dopplerbroadening measurements) were performed on both single- and polycrystalline samples, irradiated with 3 MeV protons or 1 MeV electrons. For ZnS it was found that both electron and proton irradiation caused significant changes in the positron annihilation characteristics. The annealing of proton irradiated ZnS in air leads to significant oxidation and eventual transformation into ZnO.

scholarly journals MINIMAL VARIATION OF DEFECT STRUCTURE DUE TO THE ORDER OF ROOM TEMPERATURE HYDROGEN ISOTOPE IMPLANTATION AND SELF-ION IRRADIATION IN NICKEL

MRS Advances ◽  
2016 ◽  
Vol 1 (42) ◽  
pp. 2887-2892
Author(s):  
Brittany Muntifering ◽  
Jianmin Qu ◽  
Khalid Hattar
Keyword(s):  
Dislocation Loop ◽  
Hydrogen Isotope ◽  
Room Temperature ◽  
Ion Irradiation ◽  
In Situ Tem ◽  
Loop Formation ◽  
Radiation Induced ◽  
Formation And Evolution ◽  
And Performance ◽  
Induced Defects

ABSTRACTThe formation and stability of radiation-induced defects in structural materials in reactor environments significantly effects their integrity and performance. Hydrogen, which may be present in significant quantities in future reactors, may play an important role in defect evolution. To characterize the effect of hydrogen on cascade damage evolution, in-situ TEM self-ion irradiation and deuterium implantation was performed, both sequentially and concurrently, on nickel. This paper presents preliminary results characterizing dislocation loop formation and evolution during room temperature deuterium implantation and self-ion irradiation and the consequence of the sequence of irradiation. Hydrogen isotope implantation at room temperature appears to have little or no effect on the final dislocation loop structures that result from self-ion irradiation, regardless of the sequence of irradiation. Tilting experiments emphasize the importance of precise two-beam conditions for characterizing defect size and structure.

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