Crystallization of Bulk Zr48Nb8Cu14Ni12Be18Metallic Glass

AbstractThe crystallization of bulk Zr48Nb8Cu14Ni12Be18metallic glass has been investigated by differential scanning calorimetry (DSC) and X-ray powder diffraction. The activation energies of glass transition and crystallization for the glass obtained using Kissinger analysis from the shift of the peak temperature in the DSC curve are 470 and 235 kJ/mol, respectively. The effect of applied pressure on crystallization is studied by in situ high-pressure and high-temperature X-ray powder diffraction using synchrotron radiation. It is found that the crystallization temperature increases with pressure having a slope of 9.5 K/GPa in the range of 0-4.4 GPa.

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Polymorphism of 1,3-X-adamantanes (X = Br, OH, CH3) and the crystal plastic phase formation ability

CrystEngComm ◽

10.1039/c9ce01910c ◽

2020 ◽

Vol 22 (7) ◽

pp. 1230-1238 ◽

Cited By ~ 1

Author(s):

Philippe Negrier ◽

Bacem Ben Hassine ◽

Maria Barrio ◽

Michela Romanini ◽

Denise Mondieig ◽

...

Keyword(s):

Differential Scanning Calorimetry ◽

High Pressure ◽

Phase Formation ◽

Powder Diffraction ◽

Scanning Calorimetry ◽

Density Measurements ◽

X Ray ◽

Plastic Phase

The polymorphism of 1,3-dimethyladamantane (13DMA), 1,3-adamantanediol (13DOHA) and 1,3-dibromoadamantane (13DBrA) has been studied by X-ray powder diffraction, density measurements and differential scanning calorimetry at normal and high-pressure.

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Effects of high pressure and high temperature on cation ordering in magnesioferrite, MgFe2O4, using in situ synchrotron X-ray powder diffraction up to 1430 K and 6 GPa

American Mineralogist ◽

10.2138/am.2005.1797 ◽

2005 ◽

Vol 90 (10) ◽

pp. 1500-1505 ◽

Cited By ~ 14

Author(s):

S. M. Antao

Keyword(s):

High Pressure ◽

High Temperature ◽

Powder Diffraction ◽

Cation Ordering ◽

X Ray

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Researches on Ti-alloy Hydrides under High Pressure and High Temperature with the Aid of In-situ Synchrotron Radiation X-ray Diffraction Measurements

Materia Japan ◽

10.2320/materia.53.94 ◽

2014 ◽

Vol 53 (3) ◽

pp. 94-99

Author(s):

Naruki Endo ◽

Hiroyuki Saitoh ◽

Akihiko Machida ◽

Yoshinori Katayama

Keyword(s):

High Pressure ◽

High Temperature ◽

Synchrotron Radiation ◽

Ti Alloy ◽

X Ray Diffraction ◽

X Ray

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Multichannel detector–collimator for powder diffraction measurements at energy scanning x-ray absorption spectroscopy synchrotron radiation beamlines for high-pressure and high-temperature applications

Review of Scientific Instruments ◽

10.1063/1.1568553 ◽

2003 ◽

Vol 74 (5) ◽

pp. 2654-2663 ◽

Cited By ~ 20

Author(s):

Adriano Filipponi ◽

Valentina M. Giordano ◽

Simone De Panfilis ◽

Andrea Di Cicco ◽

Emiliano Principi ◽

...

Keyword(s):

High Pressure ◽

High Temperature ◽

Synchrotron Radiation ◽

Absorption Spectroscopy ◽

Powder Diffraction ◽

X Ray ◽

X Ray Absorption ◽

Temperature Applications

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High-pressure and high-temperature transformation of Pb(ii)-natrolite to Pb(ii)-lawsonite

Dalton Transactions ◽

10.1039/c5dt03695j ◽

2016 ◽

Vol 45 (4) ◽

pp. 1622-1630 ◽

Cited By ~ 3

Author(s):

Junhyuck Im ◽

Yongmoon Lee ◽

Douglas A. Blom ◽

Thomas Vogt ◽

Yongjae Lee

Keyword(s):

High Pressure ◽

High Temperature ◽

Powder Diffraction ◽

Real Space ◽

Ex Situ ◽

Chemical Transformations ◽

X Ray ◽

Temperature Transformation

We report on high-pressure and high-temperature chemical transformations of Pb2+-exchanged natrolite (Pb-NAT, Pb8Al16Si24O80·16H2O) using a combination ofin situsynchrotron X-ray powder diffraction andex situHAADF-STEM real space imaging.

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In situ synchrotron radiation X-ray diffraction measurements of Fe–Mo alloy hydrides formed under high pressure and high temperature

Journal of Alloys and Compounds ◽

10.1016/j.jallcom.2021.162300 ◽

2021 ◽

pp. 162300

Author(s):

R. Utsumi ◽

M. Morimoto ◽

H. Saitoh ◽

T. Watanuki ◽

T. Sato ◽

...

Keyword(s):

High Pressure ◽

High Temperature ◽

Synchrotron Radiation ◽

X Ray Diffraction ◽

X Ray

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Recent advances in high pressure and high temperature in-situ x-ray studies using sintered diamond and synchrotron radiation

10.1063/1.46397 ◽

1994 ◽

Cited By ~ 1

Author(s):

Takehiko Yagi

Keyword(s):

High Pressure ◽

High Temperature ◽

Synchrotron Radiation ◽

X Ray ◽

Recent Advances ◽

Sintered Diamond

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PHYSICAL PROPERTIES OF TELLURITE GLASSES PREPARED UNDER DIFFERENT THERMAL HISTORIES

Modern Physics Letters B ◽

10.1142/s0217984910022585 ◽

2010 ◽

Vol 24 (06) ◽

pp. 527-537

Author(s):

E. B. ARAÚJO ◽

E. IDALGO ◽

A. P. A. MORAES ◽

A. G. SOUZA FILHO ◽

J. MENDES FILHO

Keyword(s):

Differential Scanning Calorimetry ◽

Raman Spectroscopy ◽

Glass Transition ◽

Tellurite Glasses ◽

X Ray Diffraction ◽

Scanning Calorimetry ◽

X Ray ◽

In Situ Crystallization ◽

Thermal Histories

Tellurite glasses were prepared with identical 20 Li 2 O -80 TeO 2 nominal compositions but with different thermal histories. Differential scanning calorimetry (DSC), X-ray diffraction (XRD) and Raman spectroscopy techniques were used to understand the effects of the thermal histories on the thermal and structural properties of these glasses. It was observed that investigated properties depend strongly on the thermal histories. DSC results suggested that annealing immediately after quenching at temperatures around the glass transition temperature (Tg) and for longer times is favorable for producing local ordered regions in the glass without necessarily increasing the number of nuclei. XRD results revealed the crystallization of the γ- TeO 2, α- TeO 2 and α- Li 2 Te 2 O 5 phases in both studied glasses. Raman spectroscopy revealed the mestastable character of the γ- TeO 2 crystalline phase, while the α- TeO 2 and α- Li 2 Te 2 O 5 crystalline phases persisted up to the final stages of the in-situ crystallization.

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