Slip trace characterisation of Ni3Al by atomic force microscopy.

2000 ◽  
Vol 646 ◽  
Author(s):  
Christophe Coupeau ◽  
Tomas Kruml ◽  
Joël Bonneville

ABSTRACTWe examined by atomic force microscope the slip traces produced on Ni3Al single crystals pre-deformed up to nearly 1% plastic strain at three temperatures in the anomaly domain: 293K, 500K and 720K. It is observed that, whatever the deformation temperature, the slip traces essentially belong to the primary octahedral slip system. The lengths of the slip lines become shorter and shorter with increasing temperature, while the number of dislocations that constitutes the lines is approximately constant. These results are interpreted in terms of a decreasing mean free path of the mobile dislocations when the temperature is raised. The implications of these results in the understanding of the flow stress anomaly are underscored.

2011 ◽  
Vol 465 ◽  
pp. 403-406 ◽  
Author(s):  
Joël Bonneville ◽  
Christophe Coupeau ◽  
Dimitri Charrier

The positive temperature dependence of flow stress in Ni3Al is examined through fine slip trace analysis performed by atomic force microscopy. Slip traces, which result from dislocation movements, constitute outstanding markers for investigating the elementary dislocation mechanisms that control plasticity. The experiments were performed on two Ni3Al-base alloys, with Ta or Hf as additional elements. The results give evidence that the anomaly domain is accompanied by a drastic exhaustion of mobile dislocations and very short cross-slip distances on the cube cross-slip plane.


1988 ◽  
Vol 133 ◽  
Author(s):  
B. Tounsia ◽  
P. Beauchamp ◽  
Y. Mishima ◽  
T. Suzuki ◽  
P. Veysslière

ABSTRACTIn order to correlate the flow stress anomaly of Ni3Si with dislocation properties, a weakbeam study ofpolycrystalline samples deformed between ambient and the peak temperature was carried out. Samples with two extreme Ni/Si ratios were tested.The most frequently activated slip system changes progressively from octahedral to cubic with increasing temperature. The transformation of superdislocations into Kear-Wilsdorf configurations gives rise to screw dislocations that are rectilinear only after deformation at room temperature. The effect of temperature is to gradually promote bending of Kear-Wisdorf configurations in the cube plane, from a few nanometers at 230°C to several tenths of micrometers at intermediate temperature. Cube slip begins to be massively activated a little below the peak temperature. It is suggested that the flow stress anomaly is controlled by progressive exhaustion of octahedral slip by thermally-activated expansion of superdislocations on the cube cross-slip plane.


1997 ◽  
Vol 68 (12) ◽  
pp. 4492-4497 ◽  
Author(s):  
W. F. Oele ◽  
J. W. J. Kerssemakers ◽  
J. Th. M. De Hosson

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