scholarly journals STRUCTURAL-PHASE STATE OF UFG TITANIUM IMPLANTED WITH ALUMINUM IONS

2019 ◽  
Vol 21 (4) ◽  
pp. 17-25
Author(s):  
Alisa Nikonenko ◽  
Nataliya Popova ◽  
Elena Nikonenko ◽  
Mark Kalashnikov ◽  
Efim Oks ◽  
...  
Keyword(s):  
Phase State ◽  
Structural Phase ◽  
Structural Phase State ◽  
Aluminum Ions

Structural-Phase State of UFG-Titanium Implanted with Aluminum Ions

2020 ◽  
Vol 303 ◽  
pp. 161-168
Author(s):  
Alisa V. Nikonenko ◽  
Natalya A. Popova ◽  
E.L. Nikonenko ◽  
M.P. Kalashnikov ◽  
I.A. Kurzina
Keyword(s):  
Grain Size ◽  
Yield Stress ◽  
Phase State ◽  
Structural Phase ◽  
Ion Source ◽  
Anisotropy Factor ◽  
Structural Phase State ◽  
Aluminum Ions ◽  
Average Grain Size ◽  
Before And After

Transmission electron microscopy investigations were carried out to study the structural-phase state of ultra-fine grain (UFG) titanium with the average grain size of ~0.2 μm, implanted with aluminum ions. Implantation was carried out on MEVVA-V.RU ion source at room temperature, exposure time of 5.25 h and ion implantation dosage of 1⋅1018 ion/cm2. UFG-titanium was obtained by a combined multiple uniaxial compaction with rolling in grooved rolls and further annealing at 573 К for 1h. The specimens were investigated before and after implantation at a distance of 70-100 nm from the specimen surface. Concentration profile of aluminum implanted with α-Ti was obtained. It was revealed that the thickness of implanted layer was 200 nm, while maximum aluminum concentration was 70 at.%. Implantation of aluminum into titanium has resulted in formation of the whole number of phases having various crystal lattices, like β-Ti, TiAl3, Ti3Al, TiC and TiO2. The areas of their localization, the sizes, distribution density and volume fractions were determined. Grain distribution functions by their sizes were built, and the average grain size was defined. The paper investigates the influence of implantation on the grain anisotropy factor. It was revealed that implantation leads to the decrease in the average transverse and longitudinal grain size of α-Ti and decrease in the anisotropy factor by three times. The yield stress and contributions of separate strengthening mechanisms before and after implantation were calculated. The implantation has resulted in increase in the yield stress by two times.

scholarly journals VT6 TITANIUM ALLOY WEARABILITY INCREASE VIA IMPLANTATION OF COPPER AND ALUMINUM IONS

2019 ◽  
Vol 16 (32) ◽  
pp. 945-966
Author(s):  
V. V. OVCHINNIKOV ◽  
N. V. UCHEVATKINA ◽  
I. A. KURBATOVA ◽  
E. V. LUKYANENKO ◽  
S. V. YAKUTINA
Keyword(s):  
Titanium Alloy ◽  
Phase State ◽  
Copper Ions ◽  
Structural Phase ◽  
Intermetallic Phases ◽  
Surface Layers ◽  
Structural Phase State ◽  
Mechanical And Tribological Properties ◽  
Aluminum Ions ◽  
Implantation Process

The relevance of the article is due to the fact that the use of titanium alloys within friction joints is restrained by their low resistance to wear while traditional methods of increasing their wear resistance are ineffective. The objective of this work was to study the processes occurring on the surface of VT6 titanium alloy samples when implanting with copper and aluminum ions, as well as in friction. Elemental composition, structural-phase state, mechanical and tribological properties of VT6 titanium alloy surface layers modified by aluminum and copper ions during the high-intensity ion-implantation process was being researched. As can be seen from the undertaken studies, the mode of the high-intensity ion-implantation process makes it possible to obtain ion doped surface layers of VT6 alloy containing TiAl, Ti3Al, Ti3Cu, Ti2Cu, TiCu finely dispersed intermetallic phases and a solid solution of aluminum and copper in titanium of composition varying in depth. The thickness of the ion-doped layer, the average grain size of the intermetallic phases (from 18 to 55nm) and their conglomerates (from 45 to 280 nm) increases with the increase in implantation dose from 2⋅1017 to 1.2⋅1019 ion/cm2 while aluminum implantation (from 0.42 to 2.1 μm) is in progress. It has been shown that the implantation of aluminum and copper ions into VT6 alloy leads to a considerable increase in its microhardness and wearability. Based on the research results, a conclusion on the positive effect of a structural-phase state of ion-doped titanium layers on their mechanical and tribological properties of VT6 titanium alloy has been drawn.

Influence of composition on the structural-phase state, electrophysical and magnetotransport properties of alloy thin films based on Co and Cu

Vacuum ◽  
2021 ◽  
Vol 187 ◽  
pp. 110141
Author(s):  
I.O. Shpetnyi ◽  
I.Yu Protsenko ◽  
S.I. Vorobiov ◽  
V.I. Grebinaha ◽  
L. Satrapinskyy ◽  
...  
Keyword(s):  
Thin Films ◽  
Phase State ◽  
Structural Phase ◽  
Structural Phase State

Influence of ball milling duration on the morphology, features of the structural-phase state and microhardness of 3Ni-Al powder mixture

2021 ◽  
Author(s):  
Ivan A. Ditenberg ◽  
Denis A. Osipov ◽  
Michail A. Korchagin ◽  
Ivan V. Smirnov ◽  
Konstantin V. Grinyaev ◽  
...  
Keyword(s):  
Ball Milling ◽  
Powder Mixture ◽  
Phase State ◽  
Structural Phase ◽  
Structural Phase State ◽  
Milling Duration ◽  
Al Powder

Effect of Alloying Elements on the Structural Phase State of Hadfield Steel

2021 ◽  
Vol 33 (11) ◽  
pp. 04021324
Author(s):  
Almira Zhilkashinova ◽  
Mazhyn Skakov ◽  
Madi Abilev ◽  
Dossym Yerbolatuly
Keyword(s):  
Phase State ◽  
Structural Phase ◽  
Alloying Elements ◽  
Hadfield Steel ◽  
Structural Phase State ◽  
Effect Of Alloying

scholarly journals Influence of electrolytic plasma nitriding mode on structural phase state of pearlitic steel

2018 ◽  
Vol 143 ◽  
pp. 03004
Author(s):  
Natalya Popova ◽  
Lyudmila Erygina ◽  
Elena Nikonenko ◽  
Mazhin Skakov
Keyword(s):  
Phase State ◽  
Plasma Nitriding ◽  
Water Solution ◽  
Lath Martensite ◽  
Structural Phase ◽  
Pearlitic Steel ◽  
Parallel Plates ◽  
Structural Phase State ◽  
Original State ◽  
Α Phase

The paper describes results of studies of phase transitions in structural phase state occurring in the type 0.34C-1Cr-1Ni-1Mo-Fe steel under electrolytic plasma nitriding in nitrogen-containing water solution. The nitriding voltages considered in the given study were 550 and 600 V. The research was conducted by means of X-ray diffraction electron microscopy. The specimens were studied in two states : 1) before modification (original state) and 2) after nitriding in the surface layer of the specimen. The study was conducted on thin foils. It was found that nitriding lead to significant changes in the structure of steel, namely in its phase composition and in the number of existing phases. In the original state the structure of steel was given as lamellar pearlite, ferritic carbide mix and fragmented ferrite. After 550 V nitriding it was lath martensite, plates of α-phase, with colonies of thin parallel plates of γ-phase and coarse grains of α-phase, containing γ-phase grains which were different in size and shape and were various-directional. Increase in nitriding voltage up to 600 V lead to change in the structure given as a lamellar non-fragmented pearlite and fragmented ferrite. The original state was marked by presence of particles of M3C cementite, after nitriding irrespective of the voltage it had the particles of M3C alloyed cementite, Fe3Mo3N nitride and Cr2C0.61N0.39 carbonitride. The sizes, volume fractions and locations of particles were dependent on nitriding voltage.

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