scholarly journals Methods of potassium contents evaluation in the substrate solution and gerbera leaves

2019 ◽  
Vol 25 (3) ◽  
pp. 238-246 ◽  
Author(s):  
Fernanda Ludwig ◽  
Dirceu Maximino Fernandes ◽  
Amaralina Celoto Guerrero ◽  
Guilherme Amaral Ferreira ◽  
Valeria Pohlmann

Abstract Several authors report that potassium (K) is the nutrient absorbed in greater amounts by gerbera plants. Thus, objective of determining the concentration of Kin the solution of substrates for growing potted gerbera, quantified by the Cardy Horiba C-131 and an atomic absorption spectrophotometer, correlating them with each other and with the plant leaf content. The experiment was carried out in a greenhouse. The experimental design was in randomized complete blocks using a 5×2 factorial scheme (5 substrates/2 cultivars) and four replications. Cherry and Red gerbera cultivar seedlings with four final leaves were transplanted into pots, filled with the substrates and acclimated for 30 days. After acclimation, the K content in the substrate solution extracted by the “PourThru” methodology was evaluated every two weeks using the Cardy Horiba C-131 portable ion meter and an atomic absorption spectrophotometer, as well as the K content in the leaves of gerbera plants. The solution of the commercial substrate had higher concentrations of K in relation to the others in the two forms of measurement, which is directly related to the high initial contents of the nutrient in this substrate. This is directly related to the high initial K contents in the substrate. Greater values of K were obtained for the cultivar Red, both in the solution and in the leaves. The K concentration of the substrate solution cultured with gerbera plants quantified by the Cardy Horiba C-131 and atomic absorption spectrophotometry correlated significantly with each other and showed a low correlation with the content of this nutrient in the plant tissue.

1978 ◽  
Vol 24 (2) ◽  
pp. 344-347 ◽  
Author(s):  
C H McMurray ◽  
W J Blanchflower

Abstract We describe an integrated automated system for the atomic absorption spectrophotometer. The system makes use of a light-dependent resistor to detect the presence of a marker ion which is present along with the sample ion in the flame. An electronic circuit has been developed which enables the marker ion to trigger the read signal of the spectrophotometer. The system has been tested by determining magnesium and calcium in serum. Alternative modes of operation and different potential applications are discussed.


1975 ◽  
Vol 58 (3) ◽  
pp. 436-440 ◽  
Author(s):  
Robert A Isaac ◽  
William C Johnson

Abstract Seven laboratories participated in a collaborative study of wet ashing of plant material with a nitric-perchloric acid mixture and dry ashing at 500°C in order to determine the elements calcium, copper, iron, magnesium, manganese, potassium, and zinc by atomic absorption spectrophotometry. Five different homogeneous leaf tissue samples were analyzed and a synthetic standard solution containing all of the elements studied was included to evaluate sample preparation errors independent of instrument errors. The results indicated that plant tissue preparation by either wet or dry ashing gave similar elemental composition results for the tissues analyzed. The wet and dry ashing techniques have been adopted as official first action.


1989 ◽  
Vol 35 (6) ◽  
pp. 1031-1033 ◽  
Author(s):  
N N Rehak ◽  
B T Chiang

Abstract Bilirubin interferes with the Du Pont magnesium method in the aca at 510 nm. We determined that bilirubin concentrations in serum samples up to 380 mg/L did not affect the absorbance measured in the aca III at 540 nm, and therefore we modified the Du Pont setting of spectrophotometer for the magnesium method to 540 and 600 nm. Accuracy and precision of the modified method were comparable with the unmodified method and with atomic absorption spectrophotometry. For comparison, we analyzed serum samples with normal (n = 37) and increased (n = 22) bilirubin concentration with the modified method in the aca III (y) and in the atomic absorption spectrophotometer (x). The results (range 0.56-1.25 mmol/L) were in good agreement (x = y = 0.84 mmol/L, D(x - y) = -0.001, SD = 0.004, t = 0.238, P greater than 0.50) and bilirubin did not interfere with the modified method.


ALCHEMY ◽  
2015 ◽  
Vol 4 (1) ◽  
Author(s):  
Eny Rahmawati ◽  
Diana Candra Dewi ◽  
Ahmad Ghanaim Fasya ◽  
Begum Fauziyah

<p class="BodyAbstract">Candy sold in the market could be containing a heavy metals like copper. In this study, candy was destructed with HNO3, HNO3/H2SO4 (3:1) dan HNO3/H2SO4/H2O2 (6:2:1) to know the best matter oxidixer for copper. Then, evaluated the levels of copper using Atomic Absorption Spectrophotometer (AAS). The one way anove result with F test showed that the best oxidizer for copper in candy is HNO3/H2SO4. The average concentration of Copper in candy coded A, B, C, D, and E were 1. 72 mg/Kg; 1.69 mg/Kg; 1.57 mg/Kg; 1.71 mg/Kg; and 1.69 mg/Kg respectively. The content of copper in candies were the under daily dietary recommended limit based on SNI regulation.</p><p class="BodyAbstract"> </p><p class="BodyAbstract"><em><strong>Key Words:</strong> Atomic Absorption Spectrophotometry, candy, matter oxidizer, time stability, wet destruction</em></p><p class="BodyAbstract"><em> </em></p>


2019 ◽  
Vol 5 (3) ◽  
pp. 185
Author(s):  
Regina Andayani ◽  
Siti Yulia Rahma ◽  
Martinus Martinus

ABSTRAKKromium merupakan logam berat yang dilarang penggunaannya dalam sediaan kosmetik. Efek logam kromium apabila terpapar pada kulit dapat menyebabkan dermatitis, oedema dan borok yang dapat meluas pada kulit. Analisis logam kromium (Cr) pada sediaan perona pipi (Blush On) secara Spektrofotometri Serapan Atom telah dilakukan. Masing-masing sampel didestruksi terlebih dahulu dengan cara destruksi kering, kemudian sampel dilarutkan dengan asam nitrat 6 N, larutan sampel diukur serapannya dengan alat Spektrofotometer Serapan Atom menggunakan lampu katoda berongga kromium pada panjang gelombang 357,9 nm. Hasil dari penelitian ini adalah sampel merek IZ, VV, KS, MC terdeteksi mengandung logam kromium dengan kadar berturut-turut adalah 10,05 ± 0,05 µg/g; 6,74 ± 0,02 µg/g; 28,95 ± 0,19 µg/g; 13,52 ± 0,63 µg/g. Data menunjukan bahwa adanya kromium pada semua sampel.Kata kunci: logam; kromium; perona pipi; spektrofotometri serapan atom ABSTRACTChromium is a heavy metal which is prohibited from using it in cosmetic preparations. Effects of chromium metal, when exposed to the skin, can cause dermatitis, oedema and ulcers that can extend to the skin. Analysis of chromium (Cr) metal in blush preparations by Atomic Absorption Spectrophotometry was carried out. Each sample was first destructed by dry destruction, then the sample was dissolved with 6 N nitric acid, the absorption of the sample solution was measured by an atomic absorption spectrophotometer using a chromium hollow cathode lamp at a wavelength of 357.9 nm. The results showed that all samples under the IZ, VV, KS and MC brands were detected containing chromium metal with levels of 10.05 ± 0.05 μg/g respectively; 6.74 ± 0.02 µg/g; 28.95 ± 0.19 µg/g; 13.52 ± 0.63 µg/g. Data shows that the presence of chromium in all samples.Keywords: metal; chromium; blush; atomic absorption spectrophotometry. 


1973 ◽  
Vol 19 (5) ◽  
pp. 521-522 ◽  
Author(s):  
H J Gitelman ◽  
C Soucek ◽  
J F Owen

Abstract Diluting continuous-flow circuits that incorporate a jet mixer with conventional AutoAnalyzer equipment provide a convenient technique for supplying diluted samples to an atomic absorption spectrophotometer at rates up to 90 per hour.


2019 ◽  
Vol 4 (1) ◽  
pp. 41-44
Author(s):  
M.A. Hanny Ferry Fernanda ◽  
Devi Elidya ◽  
Novianti Ayu Manaheda ◽  
Nurul Qomaryah ◽  
Muhammad Khotibul Umam ◽  
...  

ABSTRAKLipstik merupakan salah satu kosmetik yang paling banyak dan hampir setiap hari digunakan oleh wanita. Timbal adalah salah satu cemaran logam berat yang terdapat dalam lipstik. Penelitian ini bertujuan untukmengetahui kandungan logam berat timbal dalam lipstik yang teregistrasi dan tidak teregistrasi mengguanakan Spektrofotometer Serapan Atom (SSA). Preparasi sampel menggunakan destruksi basah dengan aqua regia. Sampel lipstik yang digunakan sebanyak 24 sampel lipstik yang diambil di wilayah Kota Surabaya, dimana 12 sampel memiliki nomor registrasi BPOM dan 12 sampel tidak memiliki nomor registrasi BPOM. Hasil penelitian menunjukkan adanya kandungan logam berat yang melebihi persyaratan BPOM pada semua sampel lipstikdengan rata-rata kadar 108.9517 ppm untuk lipstik yang teregistrasi dan 102.7183 ppm untuk lipstik yang tidak teregistrasi. Berdasarkan uji Mann-Whitney U diketahui bahwa tidak ada beda antara kadar Pb pada lipstik yang teregistrasi dengan lipstik yang tidak teregistrasi dengan nilai α= 0,05.Kata kunci: Timbal (Pb), Lipstik, Surabaya, Registrasi, Spektrofotometri Serapan Atom. ABSTRACTLipstick is one of the most widely used cosmetics every day by women. Lead is one of the heavy metal contaminants found in lipstick. This study aims to determine the heavy metal content of lead in registered lipstickand not registered using Atomic Absorption Spectrophotometer (AAS). Sample preparation using wet destruction with aqua regia. Lipstick samples were used as many as 24 lipstick samples taken in the Surabaya area, where 12 samples had BPOM registration numbers and 12 samples did not have BPOM registration numbers. The results showed that there was a heavy metal content that exceeded BPOM requirements for all lipstick samples with an average level of 108.9517 ppm for registered lipstick and 102.7183 ppm for unregistered lipstick. Basedon the Mann-Whitney U test it is known that there is no difference between Pb levels on lipstick registered with lipstick which was not registered with a value of α = 0.05.Keywords: Lead (Pb), Lipstick, Surabaya, Registration, Atomic Absorption Spectrophotometry..


2020 ◽  
Vol 2 (1) ◽  
Author(s):  
Rizki Andalia ◽  
Mulia Aria Suzanni ◽  
Rini Rini

Lipstick or lip dye is a cosmetic dose that serves to coloring, decorative the lips, as a moisturizing material and protect the lips from exposure the sun to provide optimum results. Lipstick should not contain chemicals such as lead (Pb) because the Pb is a heavy metal that is very dangerous when continuously used on the skin, because it will be absorbed into the blood and attack the body organ causing the onset of disease. According to BPOM that the lead rate on the lipstick does not exceed the permissible limit of 20 mg/kg or 20 ppm.This research aims to know the levels contained in the samples are 4 brands of matte lipstick that are sold in the Aceh market in Banda Aceh City with the method of atomic absorption spectrophotometry (AAS). The results showed that on the 4 brands of lipstick matte contain heavy metal lead (Pb) with a rate still qualified allowed by BPOM  is samples A, B, C, and D, respectively at 0.24 ppm; 0.10 ppm; 2.87 ppm and 1.32 ppm, so that the 4 brands of lipstick matte are still used.


Sign in / Sign up

Export Citation Format

Share Document