X-RAY AND SINGLE CRYSTAL VALUES OF THE ELASTIC CONSTANTS AND DETERMINATION OF MACHINING RESIDUAL STRESSES IN ALN

1998 ◽  
Vol 2 (3) ◽  
pp. 309-326 ◽  
Author(s):  
A. Kampfe ◽  
B. Eigenmann ◽  
O. Vohringer ◽  
D. Lohe
Keyword(s):  
Residual Stresses ◽  
Single Crystal ◽  
Elastic Constants ◽  
X Ray

Determination of single-crystal elastic constants from a cubic polycrystalline aggregate

1985 ◽  
Vol 18 (6) ◽  
pp. 513-518 ◽  
Author(s):  
M. Hayakawa ◽  
S. Imai ◽  
M. Oka
Keyword(s):  
Single Crystal ◽  
Young’S Modulus ◽  
Elastic Constants ◽  
Young's Modulus ◽  
Polycrystalline Aggregate ◽  
X Ray ◽  
Cubic Stiffness

A method for determining cubic stiffness constants from polcrystalline Young's modulus and X-ray elastic constants is described. The relations used among these elastic constants are those based on Kröner's quasiisotropic model. The X-ray elastic constants required [S1(hkl)] are obtained by measuring various (hkl) d spacings of a stressed specimen under symmetric θ–2θ scan mode. An application to an Fe–31Ni alloy has given the results: C 11 = 1.47, C 12 = 1.05 and C 44 = 1.24 × 1011 Pa.

Determination of X-Ray Elastic Constants of Isotropic Materials With Non-Linear Sin2ϕ Diagrams

1993 ◽  
Vol 37 ◽  
pp. 299-304
Author(s):  
Toshihiko Sasaki ◽  
Yukio Hirose
Keyword(s):  
Residual Stresses ◽  
Stress Analysis ◽  
Elastic Constants ◽  
Axial Stress ◽  
Stress Evaluation ◽  
X Ray ◽  
Stress Components ◽  
Non Linear ◽  
Zinc Nickel

As known well, non-linear sin2ϕ diagrams are observed from materials having either steep gradients of residual stresses paralell to the surface normal of the specimen or tri-axial stress components. Many authors have reported on this problem for several processing such as polishing and grinding etc. The authors also obtained such non-linear data from an electro-plated zinc—nickel alloy. For these cases, the sin2ϕ method is inadequate for the stress evaluation. Much attention has been given to the stress analysis from about 1970s as compared to the X-ray elastic constants for this phenomenon.

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

Synthesis of 4-(3-coumarinyl)-3-benzyl-4-thiazolin-2-one 4-methylbenzylidenehydrazone and determination of the isomeric structure by X-ray analysis

2003 ◽  
Vol 218 (12) ◽  
Author(s):  
Süheyla Özbey ◽  
Nilgün Karalı ◽  
Aysel Gürsoy
Keyword(s):  
Single Crystal ◽  
Diffraction Analysis ◽  
Spectral Data ◽  
X Ray Diffraction ◽  
X Ray ◽  
Isomeric Structure ◽  
Elemental Analyses

AbstractIn this study 4-(3-coumarinyl)-3-benzyl-4-thi azolin-2-one 4-methylbenzylidenehydrazone 3 was synthesised. An independent proof of the thiazolylhydrazone structure of 3 was achieved by single crystal X-ray diffraction analysis. Elemental analyses and spectral data (IR,

Lattice-constant and stress measurement in single crystals: a new method

2005 ◽  
Vol 38 (4) ◽  
pp. 678-684 ◽  
Author(s):  
Balder Ortner
Keyword(s):  
Single Crystal ◽  
Single Crystals ◽  
Lattice Constant ◽  
Stress Measurement ◽  
New Method ◽  
Lattice Plane ◽  
X Ray ◽  
Advantages And Disadvantages

A method for the X-ray determination of lattice-plane distances is given. Similar to Bond's method, it is based on the measurement of rocking curves, with some advantages and disadvantages compared with the former method. The new method is especially designed for single-crystal stress measurement. Its usefulness is demonstrated in two examples of lattice-constant and stress measurement.

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