scholarly journals Microshear bond strength of conventional and self-adhesive resin cements to feldsphatic ceramic

2018 ◽  
Vol 17 ◽  
pp. 1-7
Author(s):  
Estéfani Maminis Soares Couto ◽  
Bruna de Oliveira Reis ◽  
Thaís Yumi Umeda Suzuki ◽  
Wirley Gonçalves Assunção ◽  
André Luiz Fraga Briso ◽  
...  

Aim: The aim of this study was to verify the microshear bond strength of conventional and self-adhesive resin cements to feldsphatic ceramic. Methods: Twenty discs of Starlight ceramic (Degudent) were made (15mm x 2mm). The bonding procedure was accomplished by insertion of resin cements into tubes of 0.7mm internal diameter in contact with the ceramic. The resin cements used were: RelyX ARC (3M Espe), Panavia F (Kuraray), RelyX Unicem (3M Espe) and seT (SDI). Total of six tubes of each material on each ceramic disc. The specimens were tested for microshear in a universal testing machine, 24hours and 6months after bonding procedure. Values of microshear bonding strength (MPa) were subjected to ANOVA and Fisher PLSD test (p<0.05). Results: For 24hours analysis, RelyX ARC showed the highest microshear bonding strength without statistical difference to RelyX Unicem and seT. Panavia F showed the lowest values of microshear bonding strength in both periods. In the analysis after 6months there was a significant increase in the microshear bonding strength values for all cements compared to 24hours. Only for RelyX ARC, the increase was not statistically significant. Conclusion: In conclusion, the bond strength depends mainly on the type of resin cement used, and the self-adhesive cements behave similarly to conventional resin cement.

2021 ◽  
Vol 46 (1) ◽  
pp. 107-115
Author(s):  
DM De Paula ◽  
AD Loguercio ◽  
A Reis ◽  
S Sauro ◽  
AH Alves ◽  
...  

Clinical Relevance Use of zirconia primers with a low pH and a high acidic monomer concentration should be employed in combination with dual-cure resin cements that are less sensitive to an acidic environment. Primers with lower 10-MDP concentrations attain better outcomes. SUMMARY Objective: To assess the effects of different concentrations of 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) included in experimental ceramic primers on the degree of conversion (DC) and microshear bond strength (μSBS) of a dual-cure resin cement, and on the acidity neutralization potential of zirconia (ZrO2) in comparison to hydroxyapatite (HAp). Methods: Experimental ceramic primers were formulated using 5 wt%, 10 wt%, 20 wt%, or 40 wt% 10-MDP as an acidic functional monomer and camphorquinone (CQ)/amine or 1-phenyl-1,2-propanedione (PPD) as a photoinitiator system. Clearfil Ceramic Primer (Kuraray Dental, Tokyo, Japan) was used as the commercial control. Micro-Raman spectroscopy was used to assess the DC of uncured and light-cured resin cements applied onto primer-treated ZrO2 surfaces. The μSBS and pH of primers were assayed in a universal testing machine and by a digital pH meter (Tec-3MP; Tecnal, Piracicaba, Brazil), respectively. Statistical analysis was performed by one-way analysis of variance (ANOVA) and Tukey’s test (p&lt;0.05). Results: DC was not affected until a concentration of 10% 10-MDP in CQ primer and 5% 10-MDP in PPD primer was reached, when compared with the positive control (p&gt;0.05). Groups 10-MDP 5% in CQ and PPD primers showed the highest μSBS compared with the positive control (p&gt;0.05); however, higher concentrations of 10-MDP induced significant DC and μSBS reduction (p&lt;0.05). HAp neutralized 10-MDP primers, but ZrO2 provided higher acidity to the primers’ pH. Conclusion: 10-MDP monomer should be used in low concentrations in ZrO2 primers to avoid reduction of the polymerization and bond strength of resin cement.


2013 ◽  
Vol 14 (4) ◽  
pp. 675-680
Author(s):  
Khalil Aleisa

ABSTRACT Statement of the problem Post retention is crucial factor in restoration survival. Posts are commonly failed due to loss of retention. It is unknown which luting agents would provide the maximum bond strength for Locator overdenture posts. Aim The aim of this study was to evaluate the bond retentive strengths of Locator overdenture posts cemented with 7 luting agents. Materials and methods One hundred and five single rooted human teeth were decoronated and randomly assigned to 7 groups (n = 15). Post spaces were prepared with Locator post drills to the depth of 6 mm. The Locator posts were cemented with Variolink II, RelyX ARC, Multilink N, RelyX Unicem, ParaCore, or MultiCore Flow resin luting agents. Zinc phosphate cement was served as control group. Specimens were stored in water at 37°C for 24 hours. Each specimen was loaded in tension in an Instron universal testing machine. The maximum force required to dislodge each Locator post was recorded. Means and standard deviations were calculated and data were statistically analyzed with one-way analysis of variance (ANOVA). Results The highest mean bond strength value for Locator posts was recorded for MultiCore® Flow group (mean = 550.1 N), while the lowest mean value was for RelyX Unicem™ resin cement group (mean = 216.8 N). A statistically significant difference in mean locator overdenture post bond strength was observed between the 7 cement types (p < 0.0001). ParaCore™ and MultiCore® Flow groups had significantly higher bond strength than all other groups, but they were not differed from each other. Conclusion Bond strength of Locator overdenture posts were influenced by the type of luting agents. MultiCore Flow and ParaCore resin cements offered the greatest retention. Clinical significance The type of luting agents had a significant effect on the retention of Locator posts. The use of Core buildup resin cements as luting agent with Locator post demonstrated the greatest retention. How to cite this article Aleisa K. Bond Strength of Overdenture Locator Posts Cemented with Seven Luting Agents. J Contemp Dent Pract 2013;14(4):675-680.


2019 ◽  
Vol 44 (4) ◽  
pp. 379-385 ◽  
Author(s):  
EJ Go ◽  
Y Shin ◽  
JW Park

SUMMARY Objectives: The purpose of this study was to measure the microshear bond strength (μSBS) of four different self-adhesive resin cements with/without 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primer to zirconium ceramics and to evaluate the effect of zirconia primers on these self-adhesive resin cements (SARCs). Methods and Materials: Zirconia blocks (20 × 20 × 8 mm3) were prepared and divided into eight groups (n=20). They were sandblasted (50 μm Al2O3) and treated as follows: no primer or primer (Z-Primer Plus). Four self-adhesive resin cements (MDP-containing: Permacem 2.0 [PC], Clearfil SA luting [CS]; non–MDP-containing: Rely-X U200 [RU], Maxcem Elite [ME]) were bonded to the zirconia surface. After thermocycling, a μSBS test was performed. The failure mode was analyzed using light microscopy. Statistical analysis of μSBS was performed using one-way analysis of variance and two-sample t-test with post hoc Tukey test. The loss rate was evaluated using the Fisher's exact test and χ2 test with post hoc Tukey test (p&lt;0.05). Results: Within the no primer groups, the PC and CS groups showed higher bond strength than the RU and ME groups. Comparing the μSBS of the no primer and primer groups in the same SARCs, the RU/P group was higher than the RU group, and the ME/P group was higher than the ME group. No significant difference was observed between the PC and PC/P groups and between the CS and CS/P groups. Conclusions: Non–MDP-containing SARC showed the increased bonding value with MDP-containing primer to zirconia ceramics. The bond strength of MDP-containing SARCs was not affected significantly by the use of zirconia primer.


2015 ◽  
Vol 40 (5) ◽  
pp. 524-532 ◽  
Author(s):  
DP Lise ◽  
J Perdigão ◽  
A Van Ende ◽  
O Zidan ◽  
GC Lopes

SUMMARY Objectives To investigate the effect of hydrofluoric acid (HF) etching, silane solution, and adhesive system application on the microshear bond strength (μSBS) of lithium disilicate glass-ceramic (LD) to three resin cements. Materials and Methods Circular bonding areas were delimited on the lithium disilicate surfaces using a perforated adhesive tape. Specimens were assigned to 18 subgroups (n=12) according to surface treatment: NT = no treatment; HF = 4.8% HF for 20 seconds; silane solution: (1) no silane; (2) Monobond Plus, a silane/10-methacryloyloxydecyl dihydrogen phosphate solution for 60 seconds; (3) Monobond Plus+ExciTE F DSC, a dual-cure adhesive; and resin cement: (1) Variolink II, a bisphenol A diglycidyl ether dimethacrylate (bis-GMA)–based, hand-mixed, dual-cure resin cement; (2) Multilink Automix, a bis-GMA–based, auto-mixed, dual-cure resin cement; (3) RelyX Unicem 2, a self-adhesive, auto-mixed, dual-cure resin cement. Tygon tubes (Ø=0.8 mm) were used as cylinder matrices for resin cement application. After 24 hours of water storage, the specimens were submitted to the μSBS test. Mode of failure was evaluated under an optical microscope and classified as adhesive, mixed, cohesive in resin cement, or cohesive in ceramic. Data were statistically analyzed with three-way analysis of variance and Dunnett test (p&lt;0.05). Results When means were pooled for the factor surface treatment, HF resulted in a significantly higher μSBS than did NT (p&lt;0.0001). Regarding the use of a silane solution, the mean μSBS values obtained with Monobond Plus and Monobond Plus+ExciTE F DSC were not significantly different but were higher than those obtained with no silane (p&lt;0.001). Considering the factor resin cement, Variolink II resulted in a significantly higher mean μSBS than did RelyX Unicem 2 (p&lt;0.03). The mean μSBS for Multilink Automix was not significantly different from those of Variolink II and RelyX Unicem 2. According to Dunnett post hoc test (p&lt;0.05), there was no significant difference in μSBS between the different resin cements for HF-etched and silanized (with or without adhesive application) LD surfaces. Conclusion LD may benefit from pretreatment of the inner surface with HF and silanization, regardless of the resin cement used.


2014 ◽  
Vol 39 (3) ◽  
pp. E118-E127 ◽  
Author(s):  
A Erdem ◽  
GC Akar ◽  
A Erdem ◽  
T Kose

SUMMARY This study compares the bond strength of resin cement and yttrium-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramic with different surface conditioning methods. Two hundred presintered Y-TZP ceramic specimens were prepared, sintered (4 × 4 × 4 mm), and randomly assigned to four equal groups as control (C, no conditioning); airborne particle abraded (APA, air abrasion with 11 μm Al2O3); tribochemical silica coating/silane coupling system (TSC, Rocatec, air abrasion with 110 μm Al2O3, 30 μm silica-coated Al2O3 and silane); and laser (L, Er:YAG laser irradiation treated at a power setting of 200 mJ). After specimen preparation, composite resin cylinders were prepared and cemented with resin cements (Clearfil Esthetic, Panavia F 2.0, Rely X-U100, Super Bond C&B, and Multilink Automix) on the ceramic surfaces and kept in an incubator at 37°C for 60 days. All specimens were tested for shear bond strength with a universal testing machine, and fractured surfaces were evaluated by environmental scanning electron microscopy. Statistical analysis was performed using Kruskal-Wallis and Mann-Whitney U-tests (α=0.05). The bond strengths for C and L groups were not significantly different according to adhesive resin cement. APA and TSC resulted in increased bond strength for Panavia F 2.0 and Rely X-U100 resin cements. Additionally, TSC presented higher bond strength with Multilink Automix. Adhesive fracture between the ceramic and resin cement was the most common failure. Complete cohesive fracture at the ceramic or composite cylinders was not observed. Regardless of the adhesive resin cement used, laser treatment did not improve resin bond strength.


2021 ◽  
pp. 232020682110527
Author(s):  
Mehmet Uğur ◽  
I˙dris Kavut ◽  
Şafak Külünk ◽  
Mehmet Şerif Akdeniz ◽  
Özgür Ozan Tanrıkut

Aim: The aim of this study was to evaluate the effect of desensitizer, temporary cements, dentin cleaning methods on shear bond strength (SBS) of self-etch and self-adhesive resin cements to dentin. Materials and Methods: Four hundred eighty buccal or lingual/palatine coronal portions of human molar teeth were mounted in the acrylic blocks. Teeth surfaces were prepared until the dentin was exposed. Specimens were divided into four groups. One group separated as control and three groups of teeth were treated with a desensitizing agent containing calcium-phosphate desensitizer (Teethmate Desensitizer, TMD), resin-based self-reinforcing monomer (Shield Force Plus, SFP) and 2-hydroxyethyl methacrylate and glutaraldehyde (Gluma Desensitizer). Two different temporary cement containing calcium hydroxide (Dycall) and zinc oxide based (Rely X Temp NE) temporary cement were applied to the dentin surfaces. Temporary cement was removed with one of three cleansing techniques: 2% chlorhexidine digluconate and glass particles containing agent (Consepsis Scrub), cleansing bur (OptiClean), and ıntra/extracoronal rotary brush (Starbrush). All groups were further divided into two cementation subgroups (Panavia V5 and Panavia SA). The SBS (MPa) was measured using a universal testing machine at 0.5 mm/min crosshead speed. The data were analyzed statistically with a four-way analysis of variance and Tukey’s Honest Significant Difference test ( α = 0.05). Results: Although SFP showed higher SBS, there was no statistically significant difference between other groups ( P > .05). There were no significant differences between temporary cements ( P > .05). OptiClean rotary bur showed higher mean SBS values in all groups. The dual-polymerized Panavia V5 showed the highest SBS values in all groups ( P <.05). Conclusion: Cleaning of dentin surface from temporary cement remnants with a silicon bur and dual-cure resin cement showed the highest bond strength values.


2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.


2015 ◽  
Vol 16 (2) ◽  
pp. 147-153 ◽  
Author(s):  
Mateus Rodrigues Tonetto ◽  
Rudys Rodolfo de Jesus Tavarez ◽  
Omar El-Mowafy ◽  
Matheus Coelho Bandeca ◽  
Thiago Soares Porto ◽  
...  

ABSTRACT Purpose The purpose of this study was to evaluate the effect of self-adhesive and self-etching resin cements on the bond strength of nonmetallic posts in different root regions. Materials and methods Sixty single-rooted human teeth were decoronated, endodontically treated, post-space prepared, and divided into six groups. Glass-fiber (GF) posts (Exacto, Angelus) and fiber-reinforced composite (FRC) posts (EverStick, StickTeck) were cemented with self-adhesive resin cement (Breeze) (SA) (Pentral Clinical) and self-etching resin cement (Panavia-F) (SE) (Kuraray). Six 1-mm-thick rods were obtained from the cervical (C), middle (M), and apical (A) regions of the roots. The specimens were then subjected to microtensile testing in a special machine (BISCO; Schaumburg, IL, USA) at a crosshead speed of 0.5 mm/min. Microtensile bond strength data were analyzed with two-way ANOVA and Tukey's tests. Results Means (and SD) of the MPa were: GF/SA/C: 14.32 (2.84), GF/SA/M: 10.69 (2.72), GF/SA/A: 6.77 (2.17), GF/SE/C: 11.56 (4.13), GF/SE/M: 6.49 (2.54), GF/SE/A: 3.60 (1.29), FRC/SA/C: 16.89 (2.66), FRC/SA/M: 13.18 (2.19), FRC/SA/A: 8.45 (1.77), FRC/SE/C: 13.69 (3.26), FRC/SE/M: 9.58 (2.23), FRC/SE/A: 5.62 (2.12). The difference among the regions was statistically significant for all groups (p < 0.05). The selfadhesive resin cement showed better results than the selfetching resin cement when compared to each post (p < 0.05). No statistically significant differences in bond strengths of the resin cements when comparable to each post (p > 0.05). Conclusion The bond strength values were significantly affected by the resin cement and the highest values were found for self-adhesive resin cement. How to cite this article da Silva MB, de Jesus Tavarez RR, de Assis FS, Tonetto MR, Porto TS, Bhandi SH, El-Mowafy O, de Toledo Porto Neto S, Bandeca MC. The Effect of Self-adhesive and Self-etching Resin Cements on the Bond Strength of Nonmetallic Posts in Different Root Thirds. J Contemp Dent Pract 2015;16(2):147-153.


2017 ◽  
Vol 15 (4) ◽  
pp. 258
Author(s):  
Marcelo Giannini ◽  
Andreia Assis Carvalho ◽  
Ariovaldo Stefani ◽  
Wladimir Franco de Sá Barbosa ◽  
Lawrence Gonzaga Lopes

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.


2020 ◽  
Vol 45 (5) ◽  
pp. 484-495
Author(s):  
LL Miotti ◽  
AC Follak ◽  
AF Montagner ◽  
RT Pozzobon ◽  
BL da Silveira ◽  
...  

Clinical Relevance Conventional multistep resin cements presented higher adhesive performance to dentin than simplified self-adhesive cements, which is an important criterion for indirect restoration prognosis. SUMMARY This study aimed to conduct a systematic review of the literature on laboratory studies assessing bonding performance to dentin of conventional and self-adhesive resin cements, in cementing indirect restorations. This review was reported according to the PRISMA Statement. Of a total of 518 studies, 36 were screened full text and reviewed according to exclusion criteria. Nineteen papers were included in the systematic review and meta-analyses, according to the following inclusion criteria: studies that evaluated the bond strength to dentin of indirect restorations cemented with dual conventional or self-adhesive resin cements and those that presented bond strength data in MPa as an outcome. Statistical analyses were conducted using Rev-Man 5.1. Comparisons were performed with random effects models at 5% significance level. A global analysis comparing conventional and self-adhesive cements and three subgroup analyses comparing immediate and long-term results were performed. Global analysis showed a difference between groups, with conventional resin cements presenting higher bond strength results than self-adhesive resin cements, in immediate and long-term time periods (both p=0.03). Immediate and longterm bond strength results were different for self-adhesive cements, favoring immediate bond strength (p=0.03), but immediate and long-term bond strength results for conventional resin cements were not different (p=0.06). Medium or high risk of bias was found in all studies. Conventional multistep resin cements showed superior overall adhesive performance compared with simplified self-adhesive resin cements when used to cement indirect restorations to dentin.


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