scholarly journals Corrosion Studies of Carbon Steel Immersed in NACE Brine by Weight Loss, EIS and XRD Techniques

2016 ◽  
pp. 10185-10198
Author(s):  
Román Cabrera-Sierra ◽  
Keyword(s):  
Weight Loss ◽  
Carbon Steel ◽  
Corrosion Studies ◽  
Xrd Techniques

Influence of interface‐related parameters on some heat stable salts in the corrosion studies of carbon steel for post‐combustion CO 2 capture

2021 ◽  
Vol 52 (11) ◽  
pp. 1185-1200
Author(s):  
W. Emori ◽  
S.L. Jiang ◽  
Y.G. Zheng ◽  
P. C. Okonkwo ◽  
A. I. Obike ◽  
...  
Keyword(s):  
Carbon Steel ◽  
Heat Stable ◽  
Corrosion Studies

Reaction Synthesis and Oxidation Behaviours of Ludwigite

2010 ◽  
Vol 146-147 ◽  
pp. 475-480 ◽  
Author(s):  
Ran Liu ◽  
Xing Juan Wang ◽  
Yong Liang Gao ◽  
Qing Lu ◽  
Xiang Xin Xue
Keyword(s):  
Weight Loss ◽  
Mass Loss Rate ◽  
Mass Gain ◽  
Raw Material ◽  
X Ray Diffraction ◽  
Blast Furnace Smelting ◽  
Isothermal Tg ◽  
Lower Temperature ◽  
Xrd Techniques ◽  
Furnace Smelting

Using ludwigite as raw material, the phase transformation and mass loss rate of ludwigite in the process of oxidizing roasting are investigated by DTA, isothermal TG, scanning electron microscopy (SEM), X-ray diffraction (XRD) techniques. The results showed that magnetite is transformed into hematite, serpentine is decomposed into forsterite at lower temperature (T＜700°C). The weight of ludwigite has a small loss below 600°C. The decomposed of szaibelyite dehydrated and formed into suanite about 700°Cis the main reason of causing ludwigite mass losses. By comparing the curves of ludwigite at different temperature from 700 to 900°C, the process of oxidizing roasting can be divided into three phases: characterized by a period of fast weight loss, and then followed by a mass gain. Finally, weight of sample is no longer change with prolongation of time. The final weight loss is 6.062%, 6.658% and 7.442% respectively for test temperature. Suanite can not be decomposed to form B2O3 and volatilized when the temperature of oxidizing roasting is below 1142 °C. It is found by XRD that paigeite and magnoferrite are the most stable composition without deterioration on oxidizing roasting. The experiment results can provide theoretical references for agglomeration and blast furnace smelting of ludwigite.

scholarly journals Electrochemical and Surface Morphological Studies of Carbon Steel Corrosion by a Novel Polynuclear Schiff Base in HCl Solution

2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
K. S. Shaju ◽  
K. Joby Thomas ◽  
Vinod P. Raphael ◽  
Aby Paul
Keyword(s):  
Weight Loss ◽  
Schiff Base ◽  
Carbon Steel ◽  
Hydrochloric Acid ◽  
Adsorption Isotherm ◽  
Acid Solution ◽  
Corrosion Inhibition ◽  
Hydrochloric Acid Solution ◽  
Inhibition Efficiency ◽  
Morphological Studies

The corrosion inhibition efficiency of a potential polynuclear Schiff base, (s)-2-(anthracene-9 (10H)-ylidene amino)-5-guanidinopentanoic acid (A9Y5GPA), on carbon steel (CS) in 1 M hydrochloric acid solution has been investigated using weight loss measurements, electrochemical impedance spectroscopy (EIS), and potentiodynamic polarization studies. The corrosion inhibition efficiencies of parent amine [(s)-2-amino-5-guanidinopentanoic acid] and parent ketone (anthracene-9 (10H)-one) on carbon steel in 1.0 M hydrochloric acid solution have also been investigated using weight loss studies. The electrochemical and weight loss data established that the inhibition efficiency on CS increases with the increase in the concentration of inhibitor, A9Y5GPA. The adsorption of A9Y5GPA obeys the Langmuir adsorption isotherm. Thermodynamic parameters (Kads, ΔGads0) were calculated using the adsorption isotherm. Activation parameters of the corrosion process (Ea, ΔH* and ΔS*) were also calculated from the corrosion rates obtained from temperature studies. Tafel plot analysis revealed that A9Y5GPA acts as a mixed-type inhibitor. A probable inhibition mechanism was also proposed. Surface morphology of the carbon steel specimens in the presence and absence of the inhibitor was evaluated by SEM analysis.

Microstructural and Corrosion Studies by Immersion in 3.5% NaCl Solution on Aged Mg-9Al-1Zn-XCa Alloy

2019 ◽  
Vol 969 ◽  
pp. 93-97
Author(s):  
S. Manivannan ◽  
B. Narenthiran ◽  
A. Sivanantham ◽  
S.P. Kumaresh Babu
Keyword(s):  
Corrosion Behaviour ◽  
Nacl Solution ◽  
X Ray Diffraction ◽  
Corrosion Attack ◽  
X Ray ◽  
Α Phase ◽  
Corrosion Studies ◽  
Different Temperatures ◽  
Xrd Techniques ◽  
Scanning Electron

The experimatal alloys were aged at different temperatures of 180°C, 200°C, 220°C, and 240º C with calcium addition levels of (X=0.5, 1, 1.5, 2%) on Mg-6Al-1Zn-XCa alloy were investigated in 3.5% NaCl solution. All the experimatal alloys were immersed in 3.5% NaCl solutions and the resulted surface were analyzed to study the corrosion behaviour and its surface topography by optical microscopy (OM), scanning electron microscopy (SEM), energy dispersed spectroscopy (EDS) and X-ray diffraction (XRD) techniques. The result shows that corrosion attack occurred predominantly on ß phase and α phase exhibit relatively minor corrosion. In addition to that the increased aging temperature coarsens the intermetallic as well as α- Mg grains, which shows adverse effect to corrosion resistances and the best result were obtained at composition of 0.5wt.% Ca aged at 200°C.

Adsorption Behavior and Corrosion Inhibition of S-Benzyl o-Phenylenedioxydithiophosphate for Carbon Steel in Hydrochloric Acid Solution

2014 ◽  
Vol 937 ◽  
pp. 109-112
Author(s):  
Xiu Lan Zhang ◽  
Xiao Lin ◽  
Bin Xie ◽  
Li Ke Zou ◽  
Sha Sha Zhu ◽  
...  
Keyword(s):  
Weight Loss ◽  
Carbon Steel ◽  
Hydrochloric Acid ◽  
Acid Solution ◽  
Corrosion Inhibition ◽  
Hydrochloric Acid Solution ◽  
Hydrochloric Acid Concentration ◽  
Carbon Steel Surface ◽  
Effects Of Temperature ◽  
Mixed Type Inhibitor

The corrosion inhibition of S-benzyl o-phenylenedioxydithiophosphate (BPOTP), for carbon steel in hydrochloric acid solution was studied by electrochemical measurements and weight loss measurements. Polarization curves indicate BPOTP is a mixed-type inhibitor, and the effects of temperature, hydrochloric acid concentration and immersion time were also studied. The studies of weight loss measurement show that the inhibition efficiency was up to 92.82 % at the BPOTP concentration of 40 mg·L-1 in 1.0 M hydrochloric acid solution at 30°C. The adsorption of BPOTP on carbon steel surface obeys the Langmuir isotherm.

scholarly journals UAE Neem Extract as a Corrosion Inhibitor for Carbon Steel in HCl Solution

2010 ◽  
Vol 2010 ◽  
pp. 1-9 ◽  
Author(s):  
Ayssar Nahlé ◽  
Ideisan Abu-Abdoun ◽  
Ibrahim Abdel-Rahman ◽  
Maysoon Al-Khayat
Keyword(s):  
Weight Loss ◽  
Carbon Steel ◽  
Adsorption Isotherm ◽  
Corrosion Inhibitor ◽  
Room Temperature ◽  
Tannin Content ◽  
Neem Extract ◽  
Neem Leaves ◽  
Temkin Adsorption Isotherm ◽  
Hcl Solution

The effect of aqueous extract of UAE Neem (Azadirachta Indica) on the corrosion inhibition of carbon steel in 1.0 M HCl solution was investigated electrochemically, and by weight-loss experiments at temperatures ranging from 303 to 343 K. The percentage inhibition increased with the increase of the concentration of the inhibitor. At a concentration of 2.0 g/L, the percentage inhibition reached about 87% at room temperature and 80% at 303 K. The percentage inhibition decreased with the increase of temperature. The thermodynamic parameters for the adsorption of this inhibitor on the metal surface were calculated using the Temkin adsorption isotherm. The aqueous Neem leaves extract was found to be an excellent potential corrosion inhibitor because of the high content of tannin content as well as the presence of a series of complex triterpene glycosides.

scholarly journals New Aromatic Azo-Schiff as Carbon Steel Corrosion Inhibitor in 1 M H2SO4

2018 ◽  
Vol 34 (5) ◽  
pp. 2471-2476 ◽  
Author(s):  
Hamida Edan Salman ◽  
Asim A. Balakit ◽  
Ali Ahmed Abdulridha
Keyword(s):  
Weight Loss ◽  
Carbon Steel ◽  
Corrosion Inhibitor ◽  
Corrosion Inhibition ◽  
Potentiodynamic Polarization ◽  
Inhibition Efficiency ◽  
Steel Corrosion ◽  
Spectroscopic Techniques ◽  
Different Temperatures ◽  
Corrosion Inhibition Efficiency

A new aromatic Schiff base with azo linkage (AS) has been synthesized and characterized by FT-IR, 1H NMR and 13C NMR spectroscopic techniques. The new compound (AS) has been evaluated as carbon steel corrosion inhibitor at different concentrations (0.005, 0.01, 0.02, 0.04 and 0.08 mM) and different temperatures (303 – 333 K). The corrosion inhibition efficiency was studied by potentiodynamic polarization and weight loss measurements. The effects of concentration and temperature on the inhibition efficiency were studied by potentiodynamic polarization studies, the results showed that increasing concentration of AS increases the inhibition efficiency while increasing the temperature decreases it, the highest corrosion inhibition efficiency, 93.9% was recorded with 0.08 mM of AS at 313 K in 1 M H2SO4. Weight loss measurements showed that the inhibition efficiency reached 97.1% in the presence of AS (0.08 mM) at 313 K. The adsorption process was found to obey Langmuir isotherm, and the adsorption thermodynamic parameters were studied. Scanning electron microscope (SEM) was used to confirm the results.

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