The Scenario of Pharmaceuticals and Development of Microwave Assisted Extraction Techniques

2019 ◽  
Author(s):  
AYUSH KUMAR ◽  
mohammad gayoor khan
Keyword(s):  
Microwave Assisted Extraction ◽  
Extraction Techniques ◽  
Microwave Assisted ◽  
Assisted Extraction

scholarly journals Evaluation of Microwave-Assisted Extraction for the Analysis of Polychlorinated Biphenyls and Organochlorine Pesticides in Fish

2008 ◽  
Vol 91 (5) ◽  
pp. 1124-1129 ◽  
Author(s):  
Takamitsu Otake ◽  
Yoshie Aoyagi ◽  
Masahiko Numata ◽  
Takashi Yarita
Keyword(s):  
Polychlorinated Biphenyls ◽  
Organochlorine Pesticides ◽  
Soxhlet Extraction ◽  
Liquid Extraction ◽  
Isotope Dilution Method ◽  
Dilution Method ◽  
Microwave Assisted Extraction ◽  
Extraction Techniques ◽  
Microwave Assisted ◽  
Assisted Extraction

Abstract The efficiency of microwave-assisted extraction (MAE) was evaluated for the analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in fish. An isotope dilution method was used for quantification via analysis of the samples by gas chromatography and mass spectrometry. MAE solvent, temperature, and time were optimized, and observed concentrations were compared. The MAE results were also compared to those of other extraction techniques (Soxhlet extraction, pressurized liquid extraction, saponification, and homogenization). Concentrations of PCBs and OCPs obtained by MAE at 120C for 10 min were comparable to those by the other techniques. The results suggest that MAE can be used for the analysis of PCBs and OCPs in fish.

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