Top-down delayering by low energy, broad-beam, argon ion milling — A solution for microelectronic device process control and failure analyses

Author(s):  
Pawel Nowakowski ◽  
Mary Ray ◽  
Paul Fischione ◽  
James Sagar
Author(s):  
P. Nowakowski ◽  
M.L. Ray ◽  
P.E. Fischione

Abstract Conventional mechanical sample preparation is a difficult and uncontrolled process that does not allow targeting of a specific depth or layer. Because of the difficulties presented by mechanical sample preparation, there has been an emergence of beam-based techniques for device delayering applications. Cross-sectioning is another commonly used technique used in microelectronics industry investigations; when combined with delayering, one can gain complete knowledge about a device's faults. This paper presents a development in semiconductor device investigation using low energy, broad-beam argon ion milling. The results highlight that broad-beam Ar ion milling produces excellent surface quality, which allows high resolution scanning electron microscope observation and energy dispersive spectrometry analyses, even at low energy.


2009 ◽  
Vol 15 (S2) ◽  
pp. 170-171 ◽  
Author(s):  
H Stegmann ◽  
Y Ritz ◽  
D Utess ◽  
H-J Engelmann ◽  
E Zschech
Keyword(s):  

Extended abstract of a paper presented at Microscopy and Microanalysis 2009 in Richmond, Virginia, USA, July 26 – July 30, 2009


2009 ◽  
Author(s):  
Heiko Stegmann ◽  
Yvonne Ritz ◽  
Dirk Utess ◽  
René Hübner ◽  
Ehrenfried Zschech ◽  
...  

2021 ◽  
Vol 27 (S1) ◽  
pp. 426-429
Author(s):  
Cecile Bonifacio ◽  
Pawel Nowakowski ◽  
Mary Ray ◽  
Paul Fischione
Keyword(s):  

Author(s):  
J.Y. Lee

In the oxidation of metals and alloys, microstructural features at the atomic level play an important role in the nucleation and growth of the oxide, but little is known about the atomic mechanisms of high temperature oxidation. The present paper describes current progress on crystallographic aspects of aluminum oxidation. The 99.999% pure, polycrystalline aluminum was chemically polished and oxidized in 1 atm air at either 550°C or 600°C for times from 0.5 hr to 4 weeks. Cross-sectional specimens were prepared by forming a sandwich with epoxy, followed by mechanical polishing and then argon ion milling. High resolution images were recorded in a <110>oxide zone-axis orientation with a JE0L JEM 200CX microscope operated at 200 keV.


2018 ◽  
Author(s):  
C.S. Bonifacio ◽  
P. Nowakowski ◽  
M.J. Campin ◽  
M.L. Ray ◽  
P.E. Fischione

Abstract Transmission electron microscopy (TEM) specimens are typically prepared using the focused ion beam (FIB) due to its site specificity, and fast and accurate thinning capabilities. However, TEM and high-resolution TEM (HRTEM) analysis may be limited due to the resulting FIB-induced artifacts. This work identifies FIB artifacts and presents the use of argon ion milling for the removal of FIB-induced damage for reproducible TEM specimen preparation of current and future fin field effect transistor (FinFET) technologies. Subsequently, high-quality and electron-transparent TEM specimens of less than 20 nm are obtained.


2021 ◽  
Vol 27 (S1) ◽  
pp. 20-22
Author(s):  
Chengge Jiao ◽  
Jeremy Graham ◽  
Xu Xu ◽  
Timothy Burnett ◽  
Brandon van Leer

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