scholarly journals Wetting properties of titanium oxides, oxynitrides and nitrides obtained by DC and pulsed magnetron sputtering and cathodic arc evaporation

2019 ◽  
Vol 37 (2) ◽  
pp. 173-181 ◽  
Author(s):  
Božana Čolović ◽  
Danilo Kisić ◽  
Bojan Jokanović ◽  
Zlatko Rakočević ◽  
Ilija Nasov ◽  
...  
Keyword(s):  
Magnetron Sputtering ◽  
Oxygen Vacancies ◽  
Titanium Nitrides ◽  
Titanium Oxides ◽  
High Concentration ◽  
Wetting Properties ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc ◽  
Pulsed Magnetron

AbstractThin films of titanium oxides, titanium oxynitrides and titanium nitrides were deposited on glass substrates by the methods of direct current (DC) and pulsed magnetron sputtering and cathodic arc evaporation. Phase analysis of the deposited films by X-ray diffraction (XRD) and Fourier-transform infrared spectroscopy (FT-IR) showed the presence of phases with various Ti oxidative states, which indicated a high concentration of oxygen vacancies. The films morphology was investigated by scanning electron microscopy (SEM). Investigations of the films wettability, either with water or ethylene glycol, showed that it depends directly on the concentration of oxygen vacancies. The wettability mechanism was particularly discussed.

Hybrid technology combining electrospark alloying, cathodic arc evaporation and magnetron sputtering for hard wear-resistant coating deposition

2018 ◽  
pp. 92-103 ◽  
Author(s):  
A. N. Sheveyko ◽  
K. A. Kuptsov ◽  
Ph. V. Kiryukhantsev-Korneev ◽  
E. A. Levashov ◽  
D. V. Shtansky
Keyword(s):  
Magnetron Sputtering ◽  
Multilayer Coating ◽  
The Novel ◽  
Coating Deposition ◽  
Novel Technology ◽  
Porous Graphite ◽  
Cathodic Arc Evaporation ◽  
Mechanical And Tribological Characteristics ◽  
Arc Evaporation ◽  
Cathodic Arc

The novel technology of multilayer coating deposition combining electric-spark alloying (ESA), pulsed arc evaporation (PAE), and magnetron sputtering (MS) in one vacuum process is presented. Layers can be deposited using a single electrode material at operating pressures from 0,1 Pa to atmospheric pressure. The lower ESA layer provides increased substrate toughness, perfect adhesion and a relatively high (up to 100 μm) coating thickness. The upper PAE or MS layer up to 10 μm in thickness provides high mechanical and tribological characteristics. The technology of double-layer PAE–ESA and MS–ESA coating deposition was tested on substrates made of structural and tool steels, titanium alloys using electrodes of cemented carbides (WC–Co, TiCNiAl) and carbon (low-porous graphite).

scholarly journals Detailed characterization of the Ti-O based thin films obtained by cathodic arc evaporation

2021 ◽  
Vol 62 (1) ◽  
pp. 41-50
Author(s):  
Vukoman Jokanović ◽  
Nenad Bundaleski ◽  
Božana Čolović ◽  
Manuela Ferarra ◽  
Bojan Jokanović ◽  
...  
Keyword(s):  
Thin Films ◽  
Titanium Oxides ◽  
Xps Analysis ◽  
Detailed Characterization ◽  
Extinction Coefficients ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc ◽  
Oxidative State

Physicochemical properties of thin films on the base of titanium oxides, obtained by a cathodic arc evaporation on the surface of glass substrate are analysed in details. The analysis of these films was made by using XRD, FTIR, SEM, XPS analysis and ellipsometry. On the basis of these analyses, particularly analysis obtained by XPS, the oxidative state Ti and corresponding phases are determined through various film layers from the surface to the substrate. The depth of the various levels and their extinction coefficients and refractory indexes are estimated by ellipsometry.

Investigation of ZrN Hard Coatings Obtained by Cathodic Arc Evaporation

2010 ◽  
Vol 159 ◽  
pp. 113-116 ◽  
Author(s):  
Roumen Kakanakov ◽  
H. Bahchedjiev ◽  
Lilyana Kolaklieva ◽  
T. Cholakova ◽  
Svetla Evtimova ◽  
...  
Keyword(s):  
Hard Coatings ◽  
Crystallographic Structure ◽  
Titanium Nitrides ◽  
X Ray Diffraction ◽  
Force Microscopy ◽  
Atomic Force ◽  
Cathodic Arc Evaporation ◽  
Steel Substrates ◽  
Arc Evaporation ◽  
Cathodic Arc

Zirconium nitrides (ZrN) coatings have shown better quality in comparison to titanium nitrides (TiN) ones regarding the application in the mechanical processing of aluminum and titanium alloys. This work presents the results from investigation on properties of ZrN-based coatings intended for industrial application. The ZrN and ZrTiN hard coatings in a thickness of (3 5) m were obtained on stainless steel substrates by cathodic arc evaporation method. The coating hardness in the range of 25-32 GPa was evaluated using the Vickers measurement technique. The coating properties were studied in relation to the surface morphology by Atomic force microscopy (AFM) and Scanning electron microscopy (SEM). The analyses showed that the number and size of the macroparticles decrease when N2 pressure increases in the deposition chamber. X-ray diffraction analysis (XRD) was performed to identify the crystallographic structure, preferred orientation and stress of the ZrN coatings.

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