scholarly journals Adhesion Strength of Hydroxyapatite Coating on Titanium Materials (Ti-6Al-4V ELI) for Biomedical Application

MESIN ◽  
2020 ◽  
Vol 11 (2) ◽  
Author(s):  
Gunawarman Gunawarman ◽  
Jon Affi ◽  
Agus Sutanto ◽  
Dian Mustika Putri ◽  
Dian Juliadmi ◽  
...  

Implantasi menggunakan material titanium Ti-6Al-4V ELI masih memiliki keterbatasan yaitu osseointegrasi yang rendah karena bersifat kurang bioaktif. Hidroksiapatit digunakan sebagai bahan pelapisn meningkatkan bioaktivitas material dan ikatan material dengan jaringan tulang. Material Ti-6AL-4V ELI (kepingan) dilapisi dengan hidroksiapatit menggunakan metode electrophoretic deposition, dengan variasi voltase (5,8, dan 11 volt) selama 5 menit dan variasi waktu deposisi (5,8, dan 11 menit) dengan voltase 8 volt. Pengujian kekasaran dan kekuatan adhesi lapisan hidroksiapatit pada permukaan material dilakukan secara kualitatif. Hasil penelitian yang diperoleh menunjukkan bahwa metode EPD dapat digunakan untuk melapisi material Ti-6Al-4V ELI dengan hidroksiapatit. Massa partikel penyusun lapisan hidroksiapatit relatif dipengaruhi oleh perlakuan waktu deposisi karena terdapat perubahan ketebalan lapisan. Akan tetapi, susunan partikel relatif dipengaruhi oleh daya yang mengakibatkan migrasi partikel yang akan berpengaruh terhadap ikatan lapisan pada permukaan material. Perlakuan voltase 8 volt selama 5 menit menghasilkan kekasaran pemukaan material dilapisi hidroksiapatit Ra 0,88 dan kerusakan lapisan setelah cross cut tape test adalah 2,25% yang berarti lapisan mengalami adhesi dengan baik pada permukaan material. Dengan masa hidroksiapatit relatif tinggi (0,3 mg), lapisan tersebut menutupi permukaan material titanium dengan baik (surface coverage 82,1%) memiliki ketebalan rata-rata (73,3 μm). Hasil yang diperoleh diharapkan sesuai untuk aplikasi biomedis.

2021 ◽  
Vol 1062 (1) ◽  
pp. 012031
Author(s):  
Gunawarman ◽  
Jon Affi ◽  
Agus Sutanto ◽  
Dian Mustika Putri ◽  
Dian Juliadmi ◽  
...  

2020 ◽  
Vol 1000 ◽  
pp. 97-106
Author(s):  
Dian Juliadmi ◽  
Nuzul Ficky Nuswantoro ◽  
Hidayatul Fajri ◽  
Irma Yulia Indriyani ◽  
Jon Affi ◽  
...  

Research about the utilization of titanium alloy (Ti-6Al-4V ELI) as implant material in the treatment of orthopedic cases had been increasing. Health problems appear due to the drawbacks of using titanium. The lack of titanium using is bio-inertness characteristic, which decreasing its bioactivity and results in low bone growth and effect for implant failure. The titanium can be modified with coating on the surface using a bioactive substance that is natural-source hydroxyapatite. Bovine-source hydroxyapatite (bovineHA) contains apatite component that is similar to human bone apatite. The coating process was carried out using particle size variation (25 μm, 63 μm, and 125 μm) of bovineHA. The electrophoretic deposition (EPD) method was applied to coat hydroxyapatite with 10 volt for 5 minutes onto the titanium surface. The result showed that different size particles have an effect on coating properties. The coating composed by particle-sized 25 μm has better surface coverage (95.89%), indicating more particle mass (particle weight 6.97x103 μg) attached to surface material, thus resulting thick coating. The good coating characteristic using bovine-source hydroxyapatite with small particle size was expected can be used in biomedical applications due to fulfill the prerequisite of the bone implant.


2019 ◽  
Vol 36 (9) ◽  
pp. 908-918 ◽  
Author(s):  
Ahmad Saadati ◽  
Hamid Hesarikia ◽  
Mohammad Reza Nourani ◽  
Ramezan Ali Taheri

2018 ◽  
Vol 56 (1) ◽  
pp. 94 ◽  
Author(s):  
Vo Thi Hanh ◽  
Pham Thi Nam ◽  
Nguyen Thu Phuong ◽  
Dinh Thi Mai Thanh

Hydroxyapatite (HAp) co-doped by magnesium (Mg), strontium (Sr), sodium (Na) and fluorine (F) were deposited on the 316L stainless steel (316L SS) substrate by electrodeposition method. The influences of scanning potential ranges, scanning times, scanning rates to form MgSrFNaHAp coating were investigated. The analytical results FTIR, SEM, Xray, EDX, thickness and adhension of the obtained coating at scanning potential ranges of 0 ÷ -1.7 V/SCE; scaning times of 5, scanning rate of 5 mV/s showed that MgSrFNaHAp coatings were single phase crystals of HAp, rod shape with the thickness 8.9 µm and the adhesion strength reached 8.38 MPa.


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